Solvothermal synthesis of Cr-doped MS(M=Zn, Cd) nanostructures with room-temperature ferromagnetic property

2019 ◽  
Vol 114 ◽  
pp. 113643
Author(s):  
Yinshuan Ren ◽  
Zhufeng Zhang ◽  
Hai Hu ◽  
Wanguo Liu
2012 ◽  
Vol 1479 ◽  
pp. 95-100
Author(s):  
Oscar A. Jaramillo ◽  
Reshmi Raman ◽  
Marina E. Rincón

ABSTRACTTiO2 nanoflowers were obtained on modified ITO substrates by solvothermal synthesis. Surface modification was achieved with a layer of TiO2 seeds/nucleus obtained by dip-coating at various pH and dip cycles. Field emission scanning electron microscopy results indicated that at all nucleation conditions there was a dual population of TiO2 nanoparticles and nanoflowers. For a particular pH, the effect of increasing the number of dips was to increase the size and number of the nanoflowers, whereas for a fixed number of dips, the increase in pH causes a decrease in nanoflower population. The comparison with solvothermal films obtained on unmodified substrates indicates that TiO2 nanoflowers grew up on the nucleation sites. These microstructural changes determine the active surface area and sensing properties of the solvothermal films. At room temperature, no evidence of superior ethanol sensing properties was found for TiO2 nanoflowers, which show larger resistivity than TiO2 nanoparticles.


RSC Advances ◽  
2019 ◽  
Vol 9 (39) ◽  
pp. 22232-22239 ◽  
Author(s):  
Ashwani Kumar Singh ◽  
Jagdees Prasad ◽  
Uday Pratap Azad ◽  
Ashish Kumar Singh ◽  
Rajiv Prakash ◽  
...  

In this paper, we demonstrate a facile solvothermal synthesis of a vanadium(v) doped MoS2-rGO nanocomposites for highly efficient electrochemical hydrogen evolution reaction (HER) at room temperature.


2017 ◽  
Vol 727 ◽  
pp. 996-1000 ◽  
Author(s):  
Ning An ◽  
Hai Tao Zhang ◽  
Cheng Zhi Liu ◽  
Cun Bo Fan ◽  
Xue Dong ◽  
...  

In order to improve the structural and ferromagnetic property of BiFeO3, the effects of Ho3+ doping is systematically investigated. Pure BiFeO3 and Ho-doped BiFeO3 thin films are fabricated by sol-gel method, and the phase structure, morphology, crystalline structure, ferromagnetic are characterized by XRD, SEM, Raman spectra and VSM, respectively. The XRD patterns of the samples indicate that all the compounds crystallize in rhombohedral distorted perovskite structure with space group R3c and the Ho substitution can suppress the intrinsic formation of the miscellaneous phase. The SEM proves that along with the increasing of Ho concentration, the surface roughness of BiFeO3 is decreased due to the reduction of defects in the preparation. From the Raman spectroscopy, it is found that the peak intensity of 8 modes in Bi1-xHoxFeO3 are increased and the modes shift to higher wave number. Besides, the VSM results show that the ferromagnetic of the samples is enhanced with increasing of Ho concentration. When x=0.1, Ms is improved to be 4.8emu/g. The results can prove that the Ho3+ doping can reduce the volatilization of Bi3+, decrease the concentration of oxygen vacancies and improve the room-temperature ferromagnetic of BiFeO3.


2010 ◽  
Vol 55 (33) ◽  
pp. 3838-3841 ◽  
Author(s):  
YongZhen Yang ◽  
XuGuang Liu ◽  
WenFang Ren ◽  
Li Qiu ◽  
BingShe Xu

2014 ◽  
Vol 602-603 ◽  
pp. 19-22 ◽  
Author(s):  
Lin Qiang Gao ◽  
Hai Yan Chen ◽  
Zhen Wang ◽  
Xin Zou

Nanoscale LiTaO3 powders with perovskite structure were synthesized using the solvothermal technique with glycol as solvent at 240°C for 12h. The powders were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM). XRD was used to elucidate room temperature structures using Rietveld refinement. The powders were pure single pervoskite phase with high crystallinity. FESEM and TEM were used to determine particle size and morphology. The average LiTaO3 grain size was estimated to be < 200nm, and TEM images indicated that LiTaO3 particles had a brick-like morphology. In addition, the effect of the temperature on the LiTaO3 power characterisitics was also detailed studied.


2020 ◽  
Vol 33 (8) ◽  
pp. 2469-2481
Author(s):  
S. Senthil ◽  
S. Srinivasan ◽  
T. Thangeeswari ◽  
M. Silambarasan ◽  
V. Ratchagar

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