Characterization of a confocal three-dimensional micro X-ray fluorescence facility based on polycapillary X-ray optics and Kirkpatrick–Baez mirrors

2008 ◽  
Vol 63 (1) ◽  
pp. 76-80 ◽  
Author(s):  
Tianxi Sun ◽  
Xunliang Ding ◽  
Zhiguo Liu ◽  
Guanghua Zhu ◽  
Yude Li ◽  
...  
Keyword(s):  
2007 ◽  
Vol 40 (6) ◽  
pp. 1169-1173 ◽  
Author(s):  
Tianxi Sun ◽  
Meirong Zhang ◽  
Xunliang Ding ◽  
Zhiguo Liu ◽  
Xiaoyan Lin ◽  
...  

A confocal technology based on polycapillary X-ray optics is proposed to perform three-dimensional energy-dispersive micro X-ray diffraction. A three-dimensional energy-dispersive micro X-ray diffractometer based on a polycapillary focusing X-ray lens (PFXRL) in the excitation channel and a polycapillary parallel X-ray lens (PPXRL) in the detection channel has been designed. At 2\theta = 90^ \circ, the lateral resolution l_X \times l_Y of this diffractometer is 49.7 \times 49.9 \rm \micro m at 7.5 keV, and its depth resolution d_Z is 48.1 \rm \micro m at 8.0 keV. The total resolution of this diffractometer in \Delta d/d is 6.5% at 6.4 keV and 2\theta = 140.2^ \circ.


2021 ◽  
Vol 127 ◽  
pp. 388-397
Author(s):  
Rani Puthukulangara Ramachandran ◽  
Chyngyz Erkinbaev ◽  
Sandeep Thakur ◽  
Jitendra Paliwal

2018 ◽  
Vol 139 ◽  
pp. 75-82 ◽  
Author(s):  
A.H. Galmed ◽  
A. du Plessis ◽  
S.G. le Roux ◽  
E. Hartnick ◽  
H. Von Bergmann ◽  
...  

2000 ◽  
Vol 33 (4) ◽  
pp. 1023-1030 ◽  
Author(s):  
M. Ohler ◽  
M. Sanchez del Rio ◽  
A. Tuffanelli ◽  
M. Gambaccini ◽  
A. Taibi ◽  
...  

Section topographs recorded at different spatial locations and at different rocking angles of a highly oriented pyrolytic graphite (HOPG) crystal allow three-dimensional maps of the local angular-dependent scattering power to be obtained. This is performed with a direct reconstruction from the intensity distribution on such topographs. The maps allow the extraction of information on local structural parameters such as size, form and internal mosaic spread of crystalline domains. This data analysis leads to a new method for the characterization of mosaic crystals. Perspectives and limits of applicability of this method are discussed.


Author(s):  
Claudio Ferrari ◽  
Riccardo Lolli ◽  
Bianca Salmaso ◽  
Giovanni Pareschi ◽  
Gianpiero Tagliaferri ◽  
...  
Keyword(s):  
X Ray ◽  

Author(s):  
Anatoly Frenkel

We discuss methods of Extended X-ray Absorption Fine-Structure (EXAFS) analysis that provide three-dimensional structural characterization of metal nanoparticles, both mono- and bi-metallic. For the bimetallic alloys, we use short range order measurements to discriminate between random and non-random inter-particle distributions of atoms. We also discuss the application of EXAFS to heterogeneous nanoparticle systems.


2007 ◽  
Vol 330-332 ◽  
pp. 503-506
Author(s):  
Xiao Wei Fu ◽  
Jie Huang ◽  
E.S. Thian ◽  
Serena Best ◽  
William Bonfield

A Bioglass® reinforced polyethylene (Bioglass®/polyethylene) composite has been prepared, which combines the high bioactivity of Bioglass® and the toughness of polyethylene. The spatial distribution of Bioglass® particles within the composite is important for the performance of composites in-vivo. Recent developments in X-ray microtomography (XμT) have made it possible to visualize internal and microstructural details with different X-ray absorbencies, nondestructively, and to acquire 3D information at high spatial resolution. In this study, the volume fraction and 3D spatial distribution of Bioglass® particles has been acquired quantitatively by XμT. The information obtained provides a foundation for understanding the mechanical and bioactive properties of the Bioglass®/polyethylene composites.


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