Microstructural analysis of La2/3−xLi3xTiO3 single crystals and quenched samples observed by high resolution transmission electron microscopy

2009 ◽  
Vol 180 (6-8) ◽  
pp. 607-611 ◽  
Author(s):  
Takao Tsurui ◽  
Tetsuhiro Katsumata ◽  
Yoshiyuki Inaguma
1992 ◽  
Vol 270 ◽  
Author(s):  
P. Häussler ◽  
H. Bestgen ◽  
H.-U. ter Meer

ABSTRACTWe report on the preparation of C60/C70 by the arc method. Evidence of monofunctional C60O, and C60-CH2 has been observed by mass spectrometry. Dependent on their preparation conditions, high resolution transmission electron microscopy of crystals consisting of mixtures of C60/C70 show different structure. Needle-like crystals grown from toluene show superlattice formation while single crystals obtained by sublimation have fcc structure. UV-VIS-absorption spectra in toluene are compared to those of films of various thickness and crystallinity.


2001 ◽  
Vol 16 (7) ◽  
pp. 1960-1966 ◽  
Author(s):  
K. Miyazawa ◽  
H. Satsuki ◽  
M. Kuwabara ◽  
M. Akaishi

The structure and hardness of C60 bulk specimens compressed under 5.5 GPa at room temperature to 600 °C are investigated by high-resolution transmission electron microscopy, x-ray diffraction, and micro-Vickers hardness tests. A strong accumulation of the [1 1 0]tr orientation of high-pressure-treated C60 specimens was developed along the compression axis, and stacking faults and nano-sized deformation twins were introduced into the C60 specimens compressed at 450–600 °C. Curved lattice planes indicating a polymerization of C60 were observed by high resolution transmission electron microscopy (HRTEM). The polymerization of the high-pressure-compressed C60 is also supported by the computer simulation of HRTEM images.


2021 ◽  
Vol 21 (1) ◽  
pp. 765-771
Author(s):  
Xiaoli Zhang ◽  
Jinxian He ◽  
Zeqiang Ren ◽  
Taotao Zhou ◽  
Wenjie Cao ◽  
...  

Deformed amphibole in the plagioclase amphibolite mylonite of the Guandi Complex, Xishan, Beijing, is the research object in this study. The amphibole nanodeformation under the middle crust was analyzed using microstructural analysis and high-resolution transmission electron microscopy (TEM). Microscope observations show that the amphibolite deformations in the plagioclase amphibolite mylonite are δ and σ type porphyroclasts, and the porphyroclast tail is composed of new long-columnar crystals. Using transmission electron microscopy (TEM, and this acronyms would be defined only once), the authors observed the nanodeformation characteristics of the amphibole porphyroclast core and mantle. Dislocation tangles are dominant in the porphyroclast core, and inside the new crystal, there is little or no dislocation. Swelled new crystals surrounded by dislocation can be observed in the transition zone between the porphyroclasts and new crystals. The deformed amphibole microstructure and submicrostructure represent typical brittle–ductile transitional deformation. The deformation process can be divided into two stages: the disordered dislocation increment stage and the dislocation reduction and ordering stage. Crystalline plastic deformation occurs in the amphibole in the plagioclase amphibolite mylonite of the Xishan area, Beijing. The crystalline plastic deformation temperature in amphiboles is higher than that in plagioclase.


Author(s):  
C. M. Jantzen ◽  
D. G. Howitt

The mullite-SiO2 liquidus has been extensively studied, and it has been shown that the flattening of the liquidus is related to the existence of a metastable region of liquid immiscibility at sub-liquidus temperatures which is detectable by transmission electron microscopy (TEM) (Fig. 1).


Author(s):  
R. Gronsky

The phenomenon of clustering in Al-Ag alloys has been extensively studied since the early work of Guinierl, wherein the pre-precipitation state was characterized as an assembly of spherical, ordered, silver-rich G.P. zones. Subsequent x-ray and TEM investigations yielded results in general agreement with this model. However, serious discrepancies were later revealed by the detailed x-ray diffraction - based computer simulations of Gragg and Cohen, i.e., the silver-rich clusters were instead octahedral in shape and fully disordered, atleast below 170°C. The object of the present investigation is to examine directly the structural characteristics of G.P. zones in Al-Ag by high resolution transmission electron microscopy.


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