Analysis of the Submicrostructural Deformation of Amphibole in a Ductile Shear Zone Based on the TEM Technique

2021 ◽  
Vol 21 (1) ◽  
pp. 765-771
Author(s):  
Xiaoli Zhang ◽  
Jinxian He ◽  
Zeqiang Ren ◽  
Taotao Zhou ◽  
Wenjie Cao ◽  
...  

Deformed amphibole in the plagioclase amphibolite mylonite of the Guandi Complex, Xishan, Beijing, is the research object in this study. The amphibole nanodeformation under the middle crust was analyzed using microstructural analysis and high-resolution transmission electron microscopy (TEM). Microscope observations show that the amphibolite deformations in the plagioclase amphibolite mylonite are δ and σ type porphyroclasts, and the porphyroclast tail is composed of new long-columnar crystals. Using transmission electron microscopy (TEM, and this acronyms would be defined only once), the authors observed the nanodeformation characteristics of the amphibole porphyroclast core and mantle. Dislocation tangles are dominant in the porphyroclast core, and inside the new crystal, there is little or no dislocation. Swelled new crystals surrounded by dislocation can be observed in the transition zone between the porphyroclasts and new crystals. The deformed amphibole microstructure and submicrostructure represent typical brittle–ductile transitional deformation. The deformation process can be divided into two stages: the disordered dislocation increment stage and the dislocation reduction and ordering stage. Crystalline plastic deformation occurs in the amphibole in the plagioclase amphibolite mylonite of the Xishan area, Beijing. The crystalline plastic deformation temperature in amphiboles is higher than that in plagioclase.

2001 ◽  
Vol 16 (7) ◽  
pp. 1960-1966 ◽  
Author(s):  
K. Miyazawa ◽  
H. Satsuki ◽  
M. Kuwabara ◽  
M. Akaishi

The structure and hardness of C60 bulk specimens compressed under 5.5 GPa at room temperature to 600 °C are investigated by high-resolution transmission electron microscopy, x-ray diffraction, and micro-Vickers hardness tests. A strong accumulation of the [1 1 0]tr orientation of high-pressure-treated C60 specimens was developed along the compression axis, and stacking faults and nano-sized deformation twins were introduced into the C60 specimens compressed at 450–600 °C. Curved lattice planes indicating a polymerization of C60 were observed by high resolution transmission electron microscopy (HRTEM). The polymerization of the high-pressure-compressed C60 is also supported by the computer simulation of HRTEM images.


Author(s):  
C. M. Jantzen ◽  
D. G. Howitt

The mullite-SiO2 liquidus has been extensively studied, and it has been shown that the flattening of the liquidus is related to the existence of a metastable region of liquid immiscibility at sub-liquidus temperatures which is detectable by transmission electron microscopy (TEM) (Fig. 1).


Author(s):  
R. Gronsky

The phenomenon of clustering in Al-Ag alloys has been extensively studied since the early work of Guinierl, wherein the pre-precipitation state was characterized as an assembly of spherical, ordered, silver-rich G.P. zones. Subsequent x-ray and TEM investigations yielded results in general agreement with this model. However, serious discrepancies were later revealed by the detailed x-ray diffraction - based computer simulations of Gragg and Cohen, i.e., the silver-rich clusters were instead octahedral in shape and fully disordered, atleast below 170°C. The object of the present investigation is to examine directly the structural characteristics of G.P. zones in Al-Ag by high resolution transmission electron microscopy.


Author(s):  
S. Mahajan

The evolution of dislocation channels in irradiated metals during deformation can be envisaged to occur in three stages: (i) formation of embryonic cluster free regions, (ii) growth of these regions into microscopically observable channels and (iii) termination of their growth due to the accumulation of dislocation damage. The first two stages are particularly intriguing, and we have attempted to follow the early stages of channel formation in polycrystalline molybdenum, irradiated to 5×1019 n. cm−2 (E > 1 Mev) at the reactor ambient temperature (∼ 60°C), using transmission electron microscopy. The irradiated samples were strained, at room temperature, up to the macroscopic yield point.Figure 1 illustrates the early stages of channel formation. The observations suggest that the cluster free regions, such as A, B and C, form in isolated packets, which could subsequently link-up to evolve a channel.


Carbon ◽  
2017 ◽  
Vol 117 ◽  
pp. 174-181 ◽  
Author(s):  
Chang’an Wang ◽  
Thomas Huddle ◽  
Chung-Hsuan Huang ◽  
Wenbo Zhu ◽  
Randy L. Vander Wal ◽  
...  

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