Utilization of solid phase spectrophotometry for determination of trace amounts of beryllium in natural water

2001 ◽  
Vol 437 (2) ◽  
pp. 265-272 ◽  
Author(s):  
Alaa S Amin
2001 ◽  
Vol 137 (1-2) ◽  
pp. 29-33 ◽  
Author(s):  
Leonardo Sena Gomes Teixeira ◽  
Ant�nio Celso Sp�nola Costa ◽  
J�lio C�sar Rosa Assis ◽  
S�rgio Luis Costa Ferreira ◽  
Mauro Korn

The Analyst ◽  
1995 ◽  
Vol 120 (9) ◽  
pp. 2421-2424 ◽  
Author(s):  
L. F. Capitán-Vallvey ◽  
Maria D. Fernández ◽  
Ignacio de Orbe ◽  
Ramiro Avidad

2009 ◽  
Vol 25 (12) ◽  
pp. 1445-1450 ◽  
Author(s):  
Sulistyo SAPUTRO ◽  
Kazuhisa YOSHIMURA ◽  
Shiro MATSUOKA ◽  
Kô TAKEHARA

2008 ◽  
Vol 91 (6) ◽  
pp. 1459-1466 ◽  
Author(s):  
Ji-Ye Hu ◽  
Yu-Chao Zhang ◽  
Hai Yan

Abstract A method for high-performance liquid chromatographic (HPLC) determination of flumorph residues in cucumber, tomato, soil, and natural water was developed and validated. Primary secondary amine or octadecylsilyl (C18) solid-phase extraction cartridges were used for sample preparation. Reversed-phase HPLC with UV detection was used for separation and quantification of the pesticide. The combined cleanup and chromatographic method steps were sensitive and reliable for simultaneous determination of residues of the 2 isomers of flumorph in the studied samples. This method is characterized by recovery >97.9, coefficient of variation <6.2, and limit of quantification of 0.01 mg/kg, in agreement with directives for method validation in residue analysis. Flumorph residues in the samples were further confirmed by HPLC/mass spectrometry. The proposed method is fast, easy to perform, and could be used for monitoring of pesticide residues.


2002 ◽  
Vol 35 (1) ◽  
pp. 153-166 ◽  
Author(s):  
M. Inés Toral ◽  
Nelson Lara ◽  
Javier Gómez ◽  
Pablo Richter

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