Anomalous reaction of d-gluconamide with benzoyl chloride in anhydrous pyridine

1970 ◽  
Vol 14 (1) ◽  
pp. 103-107 ◽  
Author(s):  
Jorge O. Deferrari ◽  
Rosa M. de Lederkremer ◽  
Betty Matsuhiro ◽  
Marta I. Litter
Keyword(s):  
Benzoyl Chloride ◽  
Anhydrous Pyridine ◽  
Anomalous Reaction

scholarly journals Microwave Assisted Synthesis of Some Biologically Active Benzothiazolotriazine Derivatives

2006 ◽  
Vol 3 (4) ◽  
pp. 307-312 ◽  
Author(s):  
Prashant Kriplani ◽  
Pawan Swarnkar ◽  
Rinku Maheshwari ◽  
K. G. Ojha
Keyword(s):  
Antibacterial Activity ◽  
Microwave Irradiation ◽  
Spectral Data ◽  
Elemental Analysis ◽  
Benzoyl Chloride ◽  
Biologically Active ◽  
Anhydrous Pyridine ◽  
Microwave Assisted Synthesis ◽  
Standard Drug ◽  
Microwave Assisted

Synthesis of some biologically active benzothiazolotriazine derivatives by microwave irradiation is reported. 2-Amino-6-substituted benzothiazoles1on treatment with benzaldehyde in anhydrous ethanol afforded 2-benzylidenoimino-6-substitutedbenzothiazoles2which underwent cyclisation with ammoniumthiocyanate in dioxane to give 2-phenyl benzothiazolo [3,2-α]-s-triazine-4-[3H] thiones3.These both steps were carried out in microwave. Compound3with benzoyl chloride in anhydrous pyridine gave 2-phenyl-3-(benzoyl) benzothiazolo [3,2-α]-s-triazine-4-thiones4in good yields. The structure of all these compounds have been supported by their elemental analysis and their spectral data. All synthesized compounds were tested for their antibacterial activity using standard drug.

Analysis of Bioactive Chemical Compounds of Trogoderma granarium (Insecta: Coleoptera: Dermestidae) Using Gas Chromatography – Mass Spectrometry

2017 ◽  
Vol 9 (03) ◽  
Author(s):  
Jenan Mohammed Ubaid ◽  
Abeer Fauzi Al-Rubaye ◽  
Imad Hadi Hameed
Keyword(s):  
Acetic Acid ◽  
Benzoyl Chloride ◽  
Methanolic Extract ◽  
Biological Activities ◽  
Chemical Compounds ◽  
Gas Chromatography Mass Spectrometry ◽  
Pentanoic Acid ◽  
Trogoderma Granarium ◽  
Trans Methyl ◽  
Phenacyl Thiocyanate

Methanolic extract of bioactive compounds of Trogoderma granarium was assayed. GC-MS analysis of Trogoderma granarium revealed the existence of the Pentanoic acid , 1,1-dimethylpropyl ester , (1H)-Pyrimidinone , 5-chloro-4,6- diphenyl, Cyclobutanemethanol , α-methyl- , Nitro-2-methyl-1,3-propanediol , Hydroxylamine ,O-(2-methylpropyl)- , Uridine , 2',3'-O-(phenylmethylene)- ,Acetic acid ,2-benzoylthio-,2-oxo-2-phenylethyl ester , methylpropyl)- , Uridine , 2',3'-O-(phenylmethylene)- , 5'-(4-methylbenzenesulfo , Indolinol , 1-benzoyl-, Benzeneethanol , β-methyl-,(s)- , Acetic acid ,2-benzoylthio-,2-oxo-2-phenylethyl ester , Phenacyl thiocyanate , Deoxy-L-ribose-2,5-dibenzoate , Methenamine , Alanine , N-methyl-n-propargyloxycarbonyl-, decyl ester , Benzoyl chloride , Thiophene-2-ol , benzoate , Ethanone , -(5- nitrotetrazol-2-yl)-1-phenyl- , 2,5-Dimethylhexane-2,5-dihydroperoxide , Benzamide , N-(3-benzylthio-1,2,4-thiadiazol- 5-yl)- , Methyl p-(2-phenyl-1-benzimidazolyl)benzoate , Methyl-2-phenoxyethylamine , Pentaborane(11) , cis-Methoxy- 5-trans-methyl-1R-cyclohexanol , Nitro-1-phenyl-3-(tetrahydropyran-2-yloxy)propan-1-one , cis-Methoxy-5-transmethyl-1R-cyclohexanol. Trogoderma granarium produce many important secondary metabolites with high biological activities.

ChemInform Abstract: ANOMALOUS REACTION OF 3-METHYL-2-CYCLOPENTEN-1-ONE WITH N-BUTYL NITRITE

1978 ◽  
Vol 9 (13) ◽  
Author(s):  
V. L. NOVIKOV ◽  
O. P. SHESTAK ◽  
G. B. ELYAKOV
Keyword(s):  
Anomalous Reaction

scholarly journals N-(5-Chloro-1,3-thiazol-2-yl)-2,4-difluorobenzamide

2012 ◽  
Vol 68 (6) ◽  
pp. o1857-o1857 ◽  
Author(s):  
Xi-Wang Liu ◽  
Jian-Yong Li ◽  
Han Zhang ◽  
Ya-Jun Yang ◽  
Ji-Yu Zhang
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonds ◽  
Benzene Ring ◽  
Dihedral Angle ◽  
Title Compound ◽  
Benzoyl Chloride ◽  
Bond Lengths ◽  
Compound C

The title compound, C10H5ClF2N2OS, was obtained by linking an amino heterocycle and a substituted benzoyl chloride. The dihedral angle between the two rings is 41.2 (2)° and the equalization of the amide C—N bond lengths reveals the existence of conjugation between the benzene ring and the thiazole unit. In the crystal, pairs of N—H...N hydrogen bonds link molecules into inversion dimers. Non-classical C—H...F and C—H...O hydrogen bonds stabilize the crystal structure.

scholarly journals Anomalous reaction mean free paths of nuclear projectile fragments from heavy ion collisions at2AGeV

1983 ◽  
Vol 27 (4) ◽  
pp. 1489-1520 ◽  
Author(s):  
E. M. Friedlander ◽  
R. W. Gimpel ◽  
H. H. Heckman ◽  
Y. J. Karant ◽  
B. Judek ◽  
...  
Keyword(s):  
Heavy Ion Collisions ◽  
Heavy Ion ◽  
Ion Collisions ◽  
Anomalous Reaction

scholarly journals Effect of Pyridine and Tribenzylamine on the Hydrolysis Kinetics of Benzoyl Chloride in Water-Dioxane System

2017 ◽  
Vol 29 (9) ◽  
pp. 1888-1890
Author(s):  
Mohammad A. Batiha ◽  
Elena A. Chizhova ◽  
Marwan M. Batiha ◽  
Leema A. Al-Makhadmeh ◽  
Saleh Rawadieh ◽  
...  
Keyword(s):  
Benzoyl Chloride ◽  
Hydrolysis Kinetics ◽  
Kinetics Of

scholarly journals 2-Aminocyclohexan-1-aminium thiocyanate

2012 ◽  
Vol 68 (6) ◽  
pp. o1732-o1732 ◽  
Author(s):  
Halima F. Salem ◽  
Siti Aishah Hasbullah ◽  
Bohari M. Yamin
Keyword(s):  
Title Compound ◽  
Benzoyl Chloride ◽  
Ammonium Thiocyanate ◽  
Chair Conformation ◽  
Cyclohexane Ring ◽  
Two Dimensional ◽  
Thiocyanate Anion ◽  
Compound C

The title compound, C6H15N2 +·NCS−, was obtained unexpectedly from the reaction mixture of benzoyl chloride, ammonium thiocyanate and cyclohexane-1,2-diamine. The cyclohexane ring adopts a chair conformation. In the crystal, N—H...S and N—H...N interactions involving the thiocyanate anion and both the amine and the aminium N atoms link the molecules, forming two-dimensional networks parallel to (001).

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