Effect of drying on cement-based materials pore structure as identified by mercury intrusion porosimetry

2001 ◽  
Vol 31 (10) ◽  
pp. 1467-1477 ◽  
Author(s):  
C. Gallé
2010 ◽  
Vol 168-170 ◽  
pp. 615-618
Author(s):  
Zhi Qin Du ◽  
Wei Sun

The effect of different quantity of air-entraining agent on the impermeability of cement-based materials are studied in this paper. Impermeability test and mercury intrusion porosimetry (MIP) method were used to characterize the impermeability and pore structures. The fractal dimension is used to describe the characteristic of pore structure and calculated by the data of MIP experiment. The result shows that owing to the improvement of pore structure, the impermeability performance of the cement-based composites is noticeably enhanced when air-entraining agent is added with appropriate quantity.


2012 ◽  
Vol 517 ◽  
pp. 403-410
Author(s):  
Jia Xiao ◽  
Bao Guo Ma ◽  
Rong Zhen Dong ◽  
Cai Yun Xu

The effect of ground limestone fineness on the properties and mechanism of cement-based composite materials was investigated. The setting times, fluidity and strength of cement mortar were measured. In order to identify the mechanism effect of ground limestone fineness on the microstructure of the hardened cement pastes, microstructure analyses such as calorimetry analysis and Mercury Intrusion Porosimetry (MIP) were also performed. Experimental results indicated that the setting times are shortened, and the fluidity and strength of cement mortar are improved with the ground limestone fineness increases. The increase of the ground limestone fineness can effectively inhibit the pore structure of hardened paste, which due to mortar and paste samples incorporating replacement levels of ground limestone, and improve the pore structure of hardened paste.


Materials ◽  
2019 ◽  
Vol 12 (14) ◽  
pp. 2220 ◽  
Author(s):  
Xiaohu Wang ◽  
Yu Peng ◽  
Jiyang Wang ◽  
Qiang Zeng

Mercury intrusion porosimetry (MIP) is questioned for possibly damaging the micro structure of cement-based materials (CBMs), but this theme still has a lack of quantitative evidence. By using X-ray computed tomography (XCT), this study reported an experimental investigation on probing the pore structure damages in paste and mortar samples after a standard MIP test. XCT scans were performed on the samples before and after mercury intrusion. Because of its very high mass attenuation coefficient, mercury can greatly enhance the contrast of XCT images, paving a path to probe the same pores with and without mercury fillings. The paste and mortar showed the different MIP pore size distributions but similar intrusion processes. A grey value inverse for the pores and material skeletons before and after MIP was found. With the features of excellent data reliability and robustness verified by a threshold analysis, the XCT results characterized the surface structure of voids, and diagnosed the pore structure damages in terms of pore volume and size of the paste and mortar samples. The findings of this study deepen the understandings in pore structure damages in CBMs by mercury intrusion, and provide methodological insights in the microstructure characterization of CBMs by XCT.


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