Solid-state synthesis and X-ray diffraction studies of Na2S

Mechanical alloying (MA) was used to prepare pseudobinary high Pr-content Tb0.7Pr0.3Fex alloys. The structural and magnetoelastic properties were in investigated by means of x-ray diffraction and a standard strain technique. A single (Tb,Pr)Fe2 Laves phase with MgCu2-type structure for the composition Tb0.7Pr0.3Fe1.80 was synthesized by MA and subsequent annealing process. The high magnetostriction of 600 ppm was achieved at 10 kOe for the epoxy-bonded Tb0.7Pr0.3Fe1.8 composite.

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Preparation of Forsterite by Solid State Synthesis Process and its Dielectric Properties

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.534.110 ◽

2012 ◽

Vol 534 ◽

pp. 110-113 ◽

Cited By ~ 1

Author(s):

Fei Shi ◽

Peng Cheng Du ◽

Jing Xiao Liu ◽

Ji Wei Wu ◽

Chun Yuan Luo

Keyword(s):

Dielectric Properties ◽

Solid State ◽

Single Phase ◽

Raw Materials ◽

Magnesium Carbonate ◽

Solid State Synthesis ◽

Molar Ratio ◽

Synthesis Process ◽

X Ray Diffraction ◽

X Ray

Using basic magnesium carbonate (Mg(OH)2•4MgCO3•6H2O) and SiO2 as raw materials, forsterite (Mg2SiO4) was prepared by solid state synthesis process. The optimal process for synthesizing Mg2SiO4 was obtained by adjusting Mg/Si molar ratio and sintering temperature. The crystal phase of the obtained Mg2SiO4 powder was determined by X-ray diffraction (XRD). The results indicate that the single-phase Mg2SiO4 powder can be obtained when the mixtures with Mg/Si molar ratio of 2.05～2.01 were sintered at 1350°C for 3h in the air. The as-prepared Mg2SiO4 ceramic samples which were sintered at 1300～1360°C showed better dielectric properties with εr=7.4 and tanδ =7.5×10-4.

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Ammonium fluorolanthanates: solid state synthesis, infrared spectral and X-ray diffraction data

Canadian Journal of Chemistry ◽

10.1139/v77-363 ◽

1977 ◽

Vol 55 (14) ◽

pp. 2620-2627 ◽

Cited By ~ 12

Author(s):

Krishnan Rajeshwar ◽

Etalo A. Secco

Keyword(s):

Solid State ◽

Absorption Spectra ◽

Diffraction Data ◽

Decomposition Product ◽

Solid State Synthesis ◽

Synthesis Reaction ◽

X Ray Diffraction ◽

X Ray ◽

Final Decomposition Product ◽

Infrared Spectral

Solid state synthesis of thirteen ammonium fluorolanthanates is reported. Two main types of fluorolanthanates appeared in the primary synthesis reaction, viz. NH4LnF4 and (NH4)3Ln2F9.The final decomposition product of the fluorolanthanates is LnF3 with NH4Ln2F7 appearing as an intermediate in (NH4)3Ln2F9 decomposition.Infrared absorption spectra and X-ray diffraction data for the stable fluorolanthanates are presented.

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Solid state synthesis of layered sodium manganese oxide for sodium-ion battery by in-situ high energy X-ray diffraction and X-ray absorption near edge spectroscopy

Journal of Power Sources ◽

10.1016/j.jpowsour.2016.11.022 ◽

2017 ◽

Vol 341 ◽

pp. 114-121 ◽

Cited By ~ 12

Author(s):

Tianyuan Ma ◽

Gui-Liang Xu ◽

Xiaoqiao Zeng ◽

Yan Li ◽

Yang Ren ◽

...

Keyword(s):

Solid State ◽

Manganese Oxide ◽

High Energy ◽

Solid State Synthesis ◽

Sodium Ion ◽

Sodium Ion Battery ◽

X Ray Diffraction ◽

X Ray ◽

X Ray Absorption

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Low temperature solid state synthesis of Li5FeO4 and CO2 capture mechanism via real time in situ synchrotron X-ray diffraction

Chemical Engineering Journal ◽

10.1016/j.cej.2018.08.017 ◽

2018 ◽

Vol 354 ◽

pp. 370-377 ◽

Cited By ~ 5

Author(s):

María Valeria Blanco ◽

Katja Kohopää ◽

Irina Snigireva ◽

Federico Cova

Keyword(s):

Solid State ◽

Low Temperature ◽

Real Time ◽

Co2 Capture ◽

Solid State Synthesis ◽

X Ray Diffraction ◽

X Ray ◽

Capture Mechanism

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Stoichiometrically Controlled Solid State Synthesis and Crystal Growth of C60H2

MRS Proceedings ◽

10.1557/proc-349-151 ◽

1994 ◽

Vol 349 ◽

Cited By ~ 1

Author(s):

B. Morosin ◽

Joshua Jacobs ◽

Craig Henderson ◽

James E. Schirber

Keyword(s):

Crystal Growth ◽

Solid State ◽

Main Product ◽

Structural Parameters ◽

Solid State Synthesis ◽

Complex Nature ◽

X Ray Diffraction ◽

X Ray ◽

Structure Determinations ◽

Direct Solid

ABSTRACTWe have demonstrated the direct solid state synthesis of C60H2 by controlling the amount of hydrogen introduced into the reaction with C60. Palladium hydride has been used as the source of hydrogen. The main product 1,2-C60H2 is the isomer previously predicted by computational studies to be the lowest in energy of the possible 23 isomers; in addition, small amounts of the thermodynamically most stable isomer of C60H2, 1,2,3,4-C60H2, has also been obtained. To determine structural parameters by x-ray diffraction, crystal growth from various solvents yielded complex solventcontaining crystals which were examined; however, the complex nature of these crystals have so far precluded detailed crystal structure determinations.

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