Determination of the steel axial stresses in memory mode by the exponential law of magnetoelastic demagnetization

Magnetic and magnetoelastic methods of stress control are based on changes in the magnetic parameters of steel upon deformation. However, the magnetic properties of different steel grades, and even of the same grade in different heats may differ noticeably. The inhomogeneity of the magnetic and magnetoelastic properties of steel attributed to variations in the chemical composition, as well as in the modes of rolling and heating during manufacture affects the accuracy of stress control being a common disadvantage of magnetoelastic methods used for monitoring the stress-strain state of steel structures. The goal of the study is to consider the possibility of monitoring uniaxial mechanical stresses in steel structures in the «magnetoelastic memory» mode, based on H(σ) dependence of the strength of magnetic field of scattering local remanent magnetization of steel on the uniaxial stresses. The exponential function is shown to provide a satisfactory description of the experimental dependence of the strength of the magnetic field of scattering of the permanently magnetized 17G1S and 15KhSND steels on the stresses induced in steels by tension, compression, and impact. To improve the accuracy of the control, we propose to introduce the magnetoelastic sensitivity of steel (MSS) into the accepted form of the exponential dependence H(σ). A way to MSS determination not only on laboratory samples under ideal conditions, but directly on the construction under control (which reduces the errors of the control attributed to variations in the magnetic and magnetoelastic properties of steels) is considered. To implement the proposed procedure, prototypes of the devices for static and dynamic local loading of metal structure elements have been developed and manufactured. The devices have undergone a pilot test when monitoring the stress-strain state of the load-bearing beams of an automobile overpass. Using the developed devices, a local dosed loading with a hemispherical indenter was carried out through shock or static loading of a pre-magnetized region of the structure resulted in a decrease in the intensity of the magnetic field of scattering. A procedure for monitoring uniaxial stresses in steel structure elements by the method of magnetoelastic «memory» is proposed taking into account the measured magnetoelastic sensitivity of their material.

Microstructure and Its Effect on the Magnetic, Magnetocaloric and Magnetostrictive Properties of Tb55Co30Fe15 Glassy Ribbons

In the present work, the microstructure and its effect on the magnetic, magnetocaloric, and magnetoelastic properties of the Tb55Co30Fe15 melt-spun ribbon were investigated. The ribbon exhibits typical amorphous characteristics in its X-ray diffraction examination and differential scanning calorimetry measurement. However, the magnetic properties of the ribbon indicate that the ribbon is inhomogeneous in the nanoscale, as ascertained by a high-resolution electron microscope. Compared to the Tb55Co45 amorphous alloy, the Tb55Co30Fe15 ribbon shows poor magnetocaloric properties but outstanding magnetostriction. A rather high value of reversible magnetostriction up to 788 ppm under 5 T was obtained. The mechanism for the formation of nanoparticles and its effect on the magnetocaloric and magnetostrictive properties were investigated.

Enhancing Properties of Soft Magnetic Materials: A Study into Hot Isostatic Pressing and Sintering Atmosphere Influences

Soft magnetic materials are characterized by achieving a high magnetic induction value in the presence of a small magnetic field. Common applications of these materials, such as transformers or sensors, are in constant evolution and new requirements are becoming more demanding. Nickel and its alloys are employed as smart materials taking advantage of their superior magnetoelastic properties. A metal injection molding (MIM) technique provides high-quality complex-shaped parts with a good density and controlled impurity levels, which are necessary for these applications, by carefully adjusting the sintering stage. Previous investigations have established a sintering cycle for pure nickel consisting of 1325 ∘C for 12 h within an N2-5%H2 atmosphere. Nevertheless, microstructural, mechanical and magnetoelastic responses can still be greatly enhanced. In this context, the effects of hot isostatic pressing (HIP), and sintering atmosphere have been investigated. The application of an adequate HIP treatment leads to significant improvements in comparison to the reference sintering process. It achieves almost complete densification while increasing field-dependent elastic modulus from 8.1% up to 9.6%. Additionally, the sintering atmosphere has been proven to be a key factor in reducing impurities and hence facilitating magnetic domain motion. Three different atmospheres have been studied: N2-5%H2 (with a higher gas flow), N2-10%H2-0.1%CH4 and low vacuum. Minimum carbon contents have been registered using more reducing atmospheres (N2-5%H2 and N2-10%H2-0.1%CH4) which has led to values of field-dependent elastic modulus higher than 10%. This value is 2.5 times higher than that obtained when nickel parts are processed via conventional techniques. Moreover, although minimizing carbon content has been shown to be easier and more beneficial than achieving complete densification, both strategies could be used in combination to improve and maximize magnetoelastic performance.

Enhanced magnetoelastic performance in Pr/Mn-doped Laves phase (Tb,Ho)Fe2 compounds

Magnetostrictive TbxHo0.8−xPr0.2Fe1.8Mn0.1 (0 ⩽ x ⩽ 0.20) alloys are prepared by arc-melting and subsequent annealing. The dopant of Pr/Mn introduced into RFe2 compounds effectively stabilizes the forming of single C15 Laves phase at ambient pressure. The easy magnetization direction (EMD) varies when Tb content increases, which is accompanied by a crystal-structural transition. EMD lies along ‹1 0 0› axis for x ⩽ 0.05, rotating to ‹1 1 1› axis for x ⩽ 0.12, with a tetragonal symmetry changing to a rhombohedral one. Magnetocrystalline-anisotropy compensation is obtained with the optimized composition of x = 0.12, shifting to the Tb-poor side in comparison to Pr/Mn-free counterpart. An enhanced effect on magnetoelastic properties is achieved in Tb0.12Ho0.68Pr0.2Fe1.8Mn0.1, which simultaneously possesses a low anisotropy and high magnetostriction performance, i.e. λS ~ 420 ppm, λ111 ~ 970 ppm, and a large low-field λa ~ 390 ppm/2 kOe, being 30 % higher than that of Pr/Mn-free compound. Combining low-cost light rare earth Pr with the lower Tb content, Tb0.12Ho0.68Pr0.2Fe1.8Mn0.1 may make it promising solution in magnetostrictive applications.

Магнитострикция в сплавах Fe-=SUB=-75-=/SUB=-Ga-=SUB=-25-x-=/SUB=-Z-=SUB=-x-=/SUB=- (Z=Al, Ge, Si): расчет методом магнитного вращающего момента

This work presents an ab initio study of the effect of a small addition of the third element of III and IV groups on the elastic and magnetoelastic properties of Fe75Ga25 alloy. The dependencies of the tetragonal elastic modulus C', magnetoelastic constant –b1, and the tetragonal magnetostrictive constant λ001 on the concentration of the Z-element in the cubic crystal structures A2 and D03 were obtained with the help of the density functional theory and the magnetic torque method in Fe75Ga25-xZx (Z = Al, Ge, Si) alloys (0≤x≤6 at.%). It is shown that the addition of Al and Si atoms leads to an increase in the tetragonal elastic modulus compared to the Fe75Ga25 binary alloy. A correlation was established in the dependence equilibrium lattice constants a0(x) and λ001(x) in the studied ternary alloys for the A2 structure.