Appendix I The Determination Of Adsorption-Desorption Efficiency Of Chromatographic Traps

2014 ◽  
Vol 13 (4-8) ◽  
pp. 147-155
Author(s):  
N. Alifar ◽  
A.R. Zaharah ◽  
C.F. Ishak ◽  
Y. Awang ◽  
B. Khayambash

1982 ◽  
Vol 65 (1) ◽  
pp. 24-27
Author(s):  
Michel Galoux ◽  
Jean-C Van Damme ◽  
Albert Bernes

Abstract This colorimetric method for the determination of 3-amino-l,2,4-triazole in grain or meal is a modification of the Storherr and Burke method. The herbicide is extracted from grain with methanol, and purified by adsorption-desorption on resin. The extract is cleaned by digestion with sulfuric acid and clarified with charcoal. The colored complex formed by coupling with N-(1-naphthyl)ethylenediammonium dichloride is measured spectrophotometrically at 455 nm. The limit of detection is 0.05 ppm.


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