Austenite Grain Growth in Heat Affected Zone of Zr-Ti Bearing Microalloyed Steel

2012 ◽  
Vol 19 (2) ◽  
pp. 73-78 ◽  
Author(s):  
Lei Zheng ◽  
Ze-xi Yuan ◽  
Shen-hua Song ◽  
Tian-hui Xi ◽  
Qian Wang
2021 ◽  
Vol 118 (4) ◽  
pp. 409
Author(s):  
Xiaoqian Pan ◽  
Jian Yang ◽  
Yinhui Zhang ◽  
Joohyun Park ◽  
Hideki Ono

The submicrometre and nanometre particle characteristics, soluble element contents, and austenite grain growth behaviors in heat-affected zone of offshore engineering steels with 0.0002 (2Mg) and 0.0042 (42Mg) wt.% Mg during the simulated welding process were studied. With increasing the Mg content in steel from 0.0002 to 0.0042 wt.%, the submicron particles are decreased in number and size with their compositions evolved from TiN to TiN + MgO capped with Mo carbides, and the number density of small-sized nanoparticles increases and large-sized nanoparticles decreases. When the temperature is below 1250 °C, the grain growth rate of two steels is not much different due to the larger Mo solute drag effect in 2Mg and larger pinning force in 42Mg. When the temperature is 1250–1300 °C, the small-sized nanoparticles in 42Mg is more than that in 2Mg, resulting in the larger pinning force and smaller grain growth rate in 42Mg. When heated to 1300–1350 °C and soaked at 1350 °C for 300 s, since large quantities of particles smaller than the critical size (dcr) are dissolved, the grain growth rate in 2Mg is smaller than that in 42Mg due to the greater amount of the effective pinning particles and larger pinning force in 2Mg.


2011 ◽  
Vol 47 (2) ◽  
pp. 199-209 ◽  
Author(s):  
D. Priadi ◽  
R.A.M. Napitupulu ◽  
E.S. Siradj

Modeling of microstructural evolution has become a powerful tool for materials and process design by providing quantitative relationships for microstructure, composition and processing. Insufficient attention has been paid to predicting the austenite grain growth of microalloyed steel and the effect of undissolved microalloys. In this research, we attempted to calculate a mathematical model for austenite grain growth of 0.028% Nb steel, which can account for abnormal grain growth. The quantitative calculation of austenite grain growth generated from this model fit well with the experimental grain growth data obtained during reheating of niobium steels. The results of this study showed that increasing the temperature increases the austenite grain size, with a sharp gradient observed at higher temperatures.


Author(s):  
Nicolas Romualdi ◽  
Matthias Militzer ◽  
Warren Poole ◽  
Laurie Collins ◽  
Robert Lazor

Abstract Pipelines are the safest and most cost-effective method of oil and gas transportation to storage and processing facilities. Large diameter welded pipes fabricated by submerged arc welding (SAW) are the preferred product in many cases for pipeline construction. Furthermore, pipelines are constructed by welding segments of pipe, typically by single or dual torch Gas Metal Arc Welding (GMAW). During welding, both during pipe fabrication and girth welding, the Heat Affected Zone (HAZ) experiences rapid thermal cycles with peak temperatures up to the melting temperature of the base metal. Controlling the microstructure evolution in the HAZ during welding of line pipe steels is critical to ensure that these products meet the Charpy impact testing and CTOD requirements imposed by clients and specifications. In particular, the Coarse Grain Heat Affected Zone (CGHAZ) is of concern. Here, austenite grain growth occurs readily due to the combination of high temperature and precipitate dissolution. Controlling the CGHAZ austenite grain size is critical to obtain final microstructures with acceptable impact properties. In this study, austenite grain growth has been measured and modeled for thermal conditions relevant for the CGHAZ in 27 steels, including industrial as well as laboratory steels with systematic variations of alloying element content. Austenite grain size was measured using a Laser Ultrasonics for Metallurgy (LUMet) sensor attached to a Gleeble 3500 Thermomechanical Simulator, which enables high-throughput in-situ monitoring of austenite grain growth. A classical grain growth model has been developed based on a standard test. The grain growth kinetics are described by combining curvature driven grain growth with pinning due to TiN precipitates. A phenomenological relationship has been developed for the grain boundary mobility that decreases with C, Nb and Mo alloying which is consistent with their expected grain boundary segregation. The pinning parameter is rationalized in terms of volume fraction and size of TiN particles. The proposed model has been validated for CGHAZ heat treatment cycles including an industrial welding trial. The results of this study provide a model to predict the austenite grain size in the CGHAZ as a function of steel chemistries and heat treatment paths, i.e. welding parameters. Austenite grain size maps have been constructed as a function of peak local temperature and line pipe steel chemistry. The model can be used both for steel chemistry design and for optimizing welding of steels with known chemical composition to minimize the CGHAZ austenite grain size both during pipe fabrication and girth welding.


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