Angle-energy analyzers of back-scattered electrons for layer-by-layer diagnostics of microelectronics devices in Scanning Electron Microscope

Author(s):  
S.K. Likharev

In previous work it was shown that it was possible to visualize depth microstructure of solidstate samples in layer-by-layer form using some modifications of the back-scattered electron (BSE) detector system in the scanning electron microscope. The approach is based on the idea to detect not all of the BSE current, but only the part of it with the directions of velocities close to inverse to the primary beam and energies within a small window in the high-energy part of the whole spectrum. The fact is that when primary electrons scatter in sample, consisting only of light elements, the process of their elastic scattering can be formally divided on two-parts: small-angle scattering and large-angle scattering. In this case the probability of small-angle scattering is approximately five orders higher than large-angle scattering. Taking into account that energy of an electron can be considered as decreasing continuously, if an electron scatters in a sample and comes out with the velocity mentioned above, one can say, that it most probably passed exactly one large-angle scattering in a sample media.

Polymer ◽  
1998 ◽  
Vol 39 (13) ◽  
pp. 2733-2744 ◽  
Author(s):  
Christopher Harrison ◽  
Miri Park ◽  
P.M. Chaikin ◽  
Richard A. Register ◽  
Douglas H. Adamson ◽  
...  

2000 ◽  
Vol 07 (05n06) ◽  
pp. 533-537 ◽  
Author(s):  
ICHIRO SHIRAKI ◽  
TADAAKI NAGAO ◽  
SHUJI HASEGAWA ◽  
CHRISTIAN L. PETERSEN ◽  
PETER BØGGILD ◽  
...  

For in-situ measurements of surface conductivity in ultrahigh vacuum (UHV), we have installed micro-four-point probes (probe spacings down to 4 μm) in a UHV scanning electron microscope (SEM) combined with scanning reflection–high-energy electron diffraction (RHEED). With the aid of piezoactuators for precise positioning of the probes, local conductivity of selected surface domains of well-defined superstructures could be measured during SEM and RHEED observations. It was found that the surface sensitivity of the conductivity measurements was enhanced by reducing the probe spacing, enabling the unambiguous detection of surface-state conductivity and the influence of surface defects on the electrical conduction.


2006 ◽  
Vol 48 (1) ◽  
pp. 76-80 ◽  
Author(s):  
Masanori INUI ◽  
Kazuhiro MATSUDA ◽  
Kozaburo TAMURA ◽  
Daisuke ISHIKAWA

2019 ◽  
Vol 52 (4) ◽  
pp. 783-790 ◽  
Author(s):  
Satoshi Koizumi ◽  
Satoru Ueda ◽  
Yukihiro Nishikawa ◽  
Takeshi Terao ◽  
Norio Kubo

An attempt has been made to combine small-angle scattering of X-rays or neutrons with scanning electron microscopy in reciprocal space, in order to establish a structural analysis method covering a wide range of sizes from micro- to macro-scales. A system with a binary contrast, in which scattering objects with a homogeneous density are dispersed in vacuum (or air), is considered. A topological surface image, detected by secondary electron emission, is converted by means of a Fourier transform into a two-dimensional scattering amplitude in reciprocal space. The method was first tested by studying a dilute system of monodisperse SiO2 particles, with respect to calibrations for brightness inversion, noise reduction and two-dimensional Fourier transform, to obtain a scattering amplitude that agrees well with the analytical amplitude for a spherical particle. Secondly, the microstructure of a carbon-supported Pt catalyst for polymer electrolyte fuel cell applications was examined with the combined method, covering length scales from 10 µm down to nanometres. After two-dimensional Fourier transformation, the secondary electron emission images with low magnification are able to overcome the limitation of the minimum wavenumber (q min) detectable by ultra-small-angle scattering.


Paleobiology ◽  
1976 ◽  
Vol 2 (2) ◽  
pp. 122-130 ◽  
Author(s):  
Susan C. Oldfield

A scanning electron microscope survey of the regular echinoid test reveals that the outer surface of its component coronal plates may be sculptured with a fine-relief ornament that is species-characteristic for those species presently surveyed. Structural resemblances in surface ornamentation are more marked in species living in similar habitats than in those species that are apparently phyletically related. Plate ornament is related to skeletal magnesium levels. It is tentatively suggested that low growth rate echinoids that inhabit “low-energy” environments (and exhibit low total skeletal magnesium levels) and “high-energy” habitat-exploiting species with high growth rates (and relatively high skeletal magnesium levels) may have differential patterns of plate growth that can be distinguished by the degree of ornamentation of the plate surface.


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