Relationship Between High-Strain-Rate Superplasticity and Interface Microstructure in Aluminum Alloy Composites
The Al alloy composites reinforced with Si3N4 or SiC have been reported to exhibit superplasticity at high strain rate of faster than 1x10−2 s−1. It has been shown in many aluminum alloy composites that the optimum superplastic temperature coincides with an incipient melting temperature. The coincidence suggests a contribution of the liquid phase to the superplasticity mechanism. This paper shows a direct evidence of partial melting along matrix grain boundaries and matrix-reinforcement interfaces. Based on the obtained results, the role of the liquid phase in the high-strain-rate superplasticity is discussed.The sample was Al-Mg (5052) alloy reinforced with 20vol% Si3,N4 particles, fabricated by a powder metallurgy process. The sample showed an excellent superplasticity under the conditions given in Table 1. Partial melting was confirmed to occur at 821 K by differentail scanning calorimetry. The microstructural changes during heating were observed in situ by TEM using a heating stage. The structure of interfaces and grain boundaries was observed by HREM. Chemical analysis was performed with EDS attached to VG-STEM.