scholarly journals Relationship Between High-Strain-Rate Superplasticity and Interface Microstructure in Aluminum Alloy Composites

1999 ◽  
Vol 5 (S2) ◽  
pp. 772-773
Author(s):  
J. Koike ◽  
K.E. Sickafus ◽  
T.E. Mitchell

The Al alloy composites reinforced with Si3N4 or SiC have been reported to exhibit superplasticity at high strain rate of faster than 1x10−2 s−1. It has been shown in many aluminum alloy composites that the optimum superplastic temperature coincides with an incipient melting temperature. The coincidence suggests a contribution of the liquid phase to the superplasticity mechanism. This paper shows a direct evidence of partial melting along matrix grain boundaries and matrix-reinforcement interfaces. Based on the obtained results, the role of the liquid phase in the high-strain-rate superplasticity is discussed.The sample was Al-Mg (5052) alloy reinforced with 20vol% Si3,N4 particles, fabricated by a powder metallurgy process. The sample showed an excellent superplasticity under the conditions given in Table 1. Partial melting was confirmed to occur at 821 K by differentail scanning calorimetry. The microstructural changes during heating were observed in situ by TEM using a heating stage. The structure of interfaces and grain boundaries was observed by HREM. Chemical analysis was performed with EDS attached to VG-STEM.

2001 ◽  
Vol 16 (8) ◽  
pp. 2429-2435 ◽  
Author(s):  
Woo-Jin Kim ◽  
Dong-Wha Kum ◽  
Ha-Guk Jeong

Interface structure and solute-segregation behavior in the high-strain-rate superplastic SiCp/2124 and SiCp/6061 Al composites were investigated. Evidence for interfacial reaction between reinforcement and Al matrix, which was evident in the superplastic Si3N4p,w/2124 Al and Si3N4p,w/6061 Al composites, could not be detected in the current SiC-reinforced Al composites. Instead, strong solute segregation was observed at SiC/Al interfaces. Extensive formation of whiskerlike fibers was observed at the fractured surface of tensile samples above the critical temperature where particle weakening began to be seen. These results suggest that partial melting occurs at the solute-enriched region near SiC interfaces and is responsible for the particle weakening. The absence of reaction phase in the SiC-reinforced composite may explain why no endothermic peak for partial melting appears in its differential scanning calorimetry curve and why its optimum temperature for superplasticity is generally higher than that of the Si3N4-reinforced composite.


1997 ◽  
Vol 12 (9) ◽  
pp. 2332-2336 ◽  
Author(s):  
Mamoru Mabuchi ◽  
Hajime Iwasaki ◽  
Ha-Guk Jeong ◽  
Kenji Hiraga ◽  
Kenji Higashi

A liquid phase serves to relax stress concentrations caused by sliding at interfaces and grain boundaries in high-strain-rate superplasticity for aluminum matrix composites. However, the presence of a liquid phase does not always lead to high-strain-rate superplasticity because too much liquid causes decohesion at a liquid phase. The critical conditions of the optimum distribution, thickness, and volume in a liquid phase are discussed based on the observation results by differential scanning calorimetry and transmission electron microscopy. As a result, a very thin and discontinuous liquid phase is required both to assist relaxation of the stress concentrations and to limit decohesion at a liquid phase.


2008 ◽  
Vol 584-586 ◽  
pp. 164-169 ◽  
Author(s):  
Krystof Turba ◽  
Premysl Malek ◽  
Edgar F. Rauch ◽  
Miroslav Cieslar

Equal-channel angular pressing (ECAP) at 443 K was used to introduce an ultra-fine grained (UFG) microstructure to a Zr and Sc modified 7075 aluminum alloy. Using the methods of TEM and EBSD, an average grain size of 0.6 1m was recorded after the pressing. The UFG microstructure remained very stable up to the temperature of 723 K, where the material exhibited high strain rate superplasticity (HSRSP) with elongations to failure of 610 % and 410 % at initial strain rates of 6.4 x 10-2 s-1 and 1 x 10-1 s-1, respectively. A strain rate sensitivity parameter m in the vicinity of 0.45 was observed at temperatures as high as 773 K. At this temperature, the material still reached an elongation to failure of 430 % at 2 x 10-2 s-1. These results confirm the stabilizing effect of the Zr and Sc additions on the UFG microstructure in a 7XXX series aluminum alloy produced by severe plastic deformation.


JOM ◽  
2011 ◽  
Vol 63 (2) ◽  
pp. 53-56 ◽  
Author(s):  
Dung D. Luong ◽  
Nikhil Gupta ◽  
Atef Daoud ◽  
Pradeep K. Rohatgi

2021 ◽  
Vol 35 (12) ◽  
pp. 5405-5413
Author(s):  
Keguo Zhang ◽  
Yang Cao ◽  
Jianlin An ◽  
Keyi Wang

Author(s):  
Atsumichi Kushibe ◽  
Yorinobu Takigawa ◽  
Kenji Higashi ◽  
Kazuo Aoki ◽  
Koichi Makii ◽  
...  

2005 ◽  
pp. 3055-3060
Author(s):  
Atsumichi Kushibe ◽  
Koichi Makii ◽  
L.F. Chiang ◽  
Tsutomu Tanaka ◽  
Masahide Kohzu ◽  
...  

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