AFM-in-SEM as a Tool for Comprehensive Sample Surface Analysis

Texts on electron diffraction recommend that the camera constant of the electron microscope be determine d by calibration with a standard crystalline specimen, using the equation

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Atomic orientation effects in proton stopping at low velocity

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100077116 ◽

1983 ◽

Vol 41 ◽

pp. 708-709

Author(s):

Kin Lam

Keyword(s):

Polycrystalline Material ◽

Charged Particles ◽

Target Material ◽

Stopping Power ◽

Low Velocity ◽

Electronic Density ◽

Interatomic Distances ◽

Frame Work ◽

Image Position ◽

Atomic Orientation

The energy of moving ions in solid is dependent on the electronic density as well as the atomic structural properties of the target material. These factors contribute to the observable effects in polycrystalline material using the scanning ion microscope. Here we outline a method to investigate the dependence of low velocity proton stopping on interatomic distances and orientations.The interaction of charged particles with atoms in the frame work of the Fermi gas model was proposed by Lindhard. For a system of atoms, the electronic Lindhard stopping power can be generalized to the formwhere the stopping power function is defined as

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A Magnetic Spectrometer for a Scanning Transmission Electron Microscope

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100052195 ◽

1974 ◽

Vol 32 ◽

pp. 436-437

Author(s):

A. Kosiara ◽

J. W. Wiggins ◽

M. Beer

Keyword(s):

Scanning Transmission Electron Microscope ◽

Magnetic Spectrometer ◽

Fringe Field ◽

Curvature Radius ◽

Magnetic Pole ◽

Quadrupole Field ◽

Transmission Electron ◽

Scanning Transmission ◽

Under Construction ◽

Image Position

A magnetic spectrometer to be attached to the Johns Hopkins S. T. E. M. is under construction. Its main purpose will be to investigate electron interactions with biological molecules in the energy range of 40 KeV to 100 KeV. The spectrometer is of the type described by Kerwin and by Crewe Its magnetic pole boundary is given by the equationwhere R is the electron curvature radius. In our case, R = 15 cm. The electron beam will be deflected by an angle of 90°. The distance between the electron source and the pole boundary will be 30 cm. A linear fringe field will be generated by a quadrupole field arrangement. This is accomplished by a grounded mirror plate and a 45° taper of the magnetic pole.

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Optimizing conditions for x-ray microchemical analysis in analytical electron microscopy

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100109884 ◽

1978 ◽

Vol 36 (1) ◽

pp. 548-549 ◽

Cited By ~ 2

Author(s):

N. J. Zaluzec

Keyword(s):

Solid Angle ◽

Analytical Electron Microscopy ◽

Incident Beam ◽

Thin Foil ◽

Experimental Conditions ◽

X Ray ◽

Microchemical Analysis ◽

Analytical Electron ◽

Image Position ◽

Incident Beam Energy

The ultimate sensitivity of microchemical analysis using x-ray emission rests in selecting those experimental conditions which will maximize the measured peak-to-background (P/B) ratio. This paper presents the results of calculations aimed at determining the influence of incident beam energy, detector/specimen geometry and specimen composition on the P/B ratio for ideally thin samples (i.e., the effects of scattering and absorption are considered negligible). As such it is assumed that the complications resulting from system peaks, bremsstrahlung fluorescence, electron tails and specimen contamination have been eliminated and that one needs only to consider the physics of the generation/emission process.The number of characteristic x-ray photons (Ip) emitted from a thin foil of thickness dt into the solid angle dΩ is given by the well-known equation

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X-ray microanalysis of thin specimens in the transmission electron microscope at voltages up to 1000 Kv.

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100109847 ◽

1978 ◽

Vol 36 (1) ◽

pp. 540-541

Author(s):

G. Cliff ◽

M.J. Nasir ◽

G.W. Lorimer ◽

N. Ridley

Keyword(s):

Electron Microscope ◽

Transmission Electron Microscope ◽

Weight Fraction ◽

Present Series ◽

Constant Independent ◽

X Ray ◽

Transmission Electron ◽

Series Of Experiments ◽

Image Position ◽

X Ray Absorption

In a specimen which is transmission thin to 100 kV electrons - a sample in which X-ray absorption is so insignificant that it can be neglected and where fluorescence effects can generally be ignored (1,2) - a ratio of characteristic X-ray intensities, I1/I2 can be converted into a weight fraction ratio, C1/C2, using the equationwhere k12 is, at a given voltage, a constant independent of composition or thickness, k12 values can be determined experimentally from thin standards (3) or calculated (4,6). Both experimental and calculated k12 values have been obtained for K(11<Z>19),kα(Z>19) and some Lα radiation (3,6) at 100 kV. The object of the present series of experiments was to experimentally determine k12 values at voltages between 200 and 1000 kV and to compare these with calculated values.The experiments were carried out on an AEI-EM7 HVEM fitted with an energy dispersive X-ray detector.

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SEM analysis of the change in the reaction rates with deposit structures in the copper-iron cementation system

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100109422 ◽

1978 ◽

Vol 36 (1) ◽

pp. 456-457

Author(s):

V. Annamalai ◽

L.E. Murr

Keyword(s):

Structural Characteristics ◽

Secondary Electron Emission ◽

Copper Deposit ◽

Reaction Rates ◽

Sem Analysis ◽

Experimental Conditions ◽

Major Drawback ◽

Emission Mode ◽

Scrap Iron ◽

Image Position

Economical recovery of copper metal from leach liquors has been carried out by the simple process of cementing copper onto a suitable substrate metal, such as scrap-iron, since the 16th century. The process has, however, a major drawback of consuming more iron than stoichiometrically needed by the reaction.Therefore, many research groups started looking into the process more closely. Though it is accepted that the structural characteristics of the resultant copper deposit cause changes in reaction rates for various experimental conditions, not many systems have been systematically investigated. This paper examines the deposit structures and the kinetic data, and explains the correlations between them.A simple cementation cell along with rotating discs of pure iron (99.9%) were employed in this study to obtain the kinetic results The resultant copper deposits were studied in a Hitachi Perkin-Elmer HHS-2R scanning electron microscope operated at 25kV in the secondary electron emission mode.

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Field ion microscopy

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100104236 ◽

1988 ◽

Vol 46 ◽

pp. 434-435

Author(s):

Gert Ehrlich

Keyword(s):

Low Temperature ◽

Sample Surface ◽

Low Pressure ◽

Radius Of Curvature ◽

Field Ion Microscopy ◽

Phosphor Screen ◽

Ion Microscopy ◽

Field Ion Microscope

The field ion microscope, devised by Erwin Muller in the 1950's, was the first instrument to depict the structure of surfaces in atomic detail. An FIM image of a (111) plane of tungsten (Fig.l) is typical of what can be done by this microscope: for this small plane, every atom, at a separation of 4.48Å from its neighbors in the plane, is revealed. The image of the plane is highly enlarged, as it is projected on a phosphor screen with a radius of curvature more than a million times that of the sample. Müller achieved the resolution necessary to reveal individual atoms by imaging with ions, accommodated to the object at a low temperature. The ions are created at the sample surface by ionization of an inert image gas (usually helium), present at a low pressure (< 1 mTorr). at fields on the order of 4V/Å.

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