Analysis of Liquid Distribution in a Packed Column on a Pilot Scale

1998 ◽  
Vol 37 (7) ◽  
pp. 2844-2849 ◽  
Author(s):  
S. M. Pizzo ◽  
D. Moraes ◽  
F. A. N. Fernandes ◽  
M. S. Kobayasi ◽  
R. J. Pazini
Processes ◽  
2018 ◽  
Vol 6 (12) ◽  
pp. 266 ◽  
Author(s):  
J. Padilla de la Rosa ◽  
Priscilla Ruiz-Palomino ◽  
Enrique Arriola-Guevara ◽  
Jorge García-Fajardo ◽  
Georgina Sandoval ◽  
...  

The processing of Mexican limes generates great amounts of peel as a by-product. Lime peel is mainly rich in the flavonoid hesperidin, whose bioactivity is oriented mainly to cardiovascular diseases and cancer. The purpose of this work was to develop a green process for the extraction and purification of hesperidin from Mexican lime peel. The extraction of hesperidin was investigated on a laboratory scale by varying the solvent composition and the solid-to-solvent ratio, and then scaling this process (volume: 20 L). Next, a purification process using adsorption resins was assessed: first through static tests to determine the adsorption efficiency with two resins (FPX66, EXA118), and then on a packed column with 80 mL of resin at 25 °C. Lab-scale extraction showed that the best conditions were a solid-to-solvent ratio of 0.33 g/mL and 60% ethanol. After using these conditions at pilot scale and concentrating the solution, the hesperidin content of the extract was 0.303 mg/mL. Through static tests, higher adsorption efficiencies were achieved with the EXA-118 resin and diluted extract (4:6 ratio with 10% dimethylsulfoxide, (DMSO)). Finally, the purification process on a packed column from the diluted extract (hesperidin concentration of 0.109 mg/mL) had a mean recovery efficiency of almost 90%.


1973 ◽  
Vol 28 (9) ◽  
pp. 1677-1683 ◽  
Author(s):  
Kakusaburo Onda ◽  
Hiroshi Takeuchi ◽  
Yoshiro Maeda ◽  
Noboru Takeuchi

1980 ◽  
Vol 35 (3) ◽  
pp. 759-761 ◽  
Author(s):  
K.J.R Ter Veer ◽  
H.W. Van Der Klooster ◽  
A.A.H. Drinkenburg

2018 ◽  
Vol 62 ◽  
pp. 176-185 ◽  
Author(s):  
A.F. Velo ◽  
D.V.S. Carvalho ◽  
M.M. Hamada

2021 ◽  
Author(s):  
Nazar Aoda

The aim of this research is to use Electrical Resistance Tomography technique (ERT) to measure factors that affect local mass transfer at various axial locations in a random packed column with diameter 0.3m and bed height 150cm filled with 2 cm plastic spheres. These factors are: liquid maldistribution, velocity profiles, and flow pattern. The system was designed to run in a trickling down-flow mode and a full liquid up-flow mode. Experiments were performed at flow rates of 3, 6, and 9 gpm (or 0.27 x 10⁻², 0.54 x 10⁻² and 0.8 x 10⁻² m³/m² s) and under normal operating conditions of 25C° and atmospheric pressure. The liquid maldistribution factors were measured via ERT technique and the conventional liquid collection method. Both measurements were conducted at various fluid flow rates at different bed heights. The results of ERT were in very good agreement with the conventional method. The standard deviation values were 17% and 21% at flow rates 3 and 6 gpm respectively. The numerical values of velocity for full liquid up flow at 3 gpm were 0.83cm/s, 1.2cm/s, 1.2 cm/s and 1.11 cm/s for different heights of 30, 60 and 90 cm respectively and the numerical values of velocity for trickle down flow at 3 gpm were 16.5 cm/s, 22.5 cm/s and 24 cm/ for different heights of 30, 60 and 90 cm respectively. The values of the liquid maldistribution factor for flow rate 3 gpm were 0.43 (30cm), 0.33(60cm) and 0.30 (90cm) and for flow rate 6 gpm were 0.33(30cm), 0.27(60cm) and 0.22 (90cm). By comparison with findings of many studies conducted on liquid distribution in packed bed column, a good agreement was observed on the relation of Mf and flow rates and bed heights.


2018 ◽  
Vol 1 (1) ◽  
pp. 19
Author(s):  
Daniela Boyanova Dzhonova-Atanasova ◽  
Krum Semkov ◽  
Tatyana Petrova ◽  
Simeon Darakchiev ◽  
Konstantina Stefanova ◽  
...  

The scientific interest in the efficiency of packed bed columns is part of the world-wide pursuit of sustainability of processes. The maldistribution of the phases in the apparatus reduces the efficiency and makes difficult the prediction of process performance and scaling up. In the present work the operation of liquid distribution devices and high performance packings are investigated addressing the reasons for hydrodynamic non-uniformity of the liquid phase, including the formation and development of wall flow. Data are obtained from semi-industrial size experimental studies and mathematical modeling of the liquid flow through a layer of random Raschig Super-Ring packing. The effect of measures for ensuring uniform initial liquid distribution in the column apparatus is evaluated and the parameters in the mathematical model are identified.  


2014 ◽  
Vol 625 ◽  
pp. 369-372
Author(s):  
Ali Qasim ◽  
M. Zamri Abdullah ◽  
K.K. Lau ◽  
Nor Adilla

The following study involves the investigation of hydrodynamics inside the packed column both at laboratory scale which is HPVA high pressure adsorption analyzer chamber and pilot scale. The simulations are performed in ANSYS FLUENT14. Velocity variation due to porous media along with the pressure gradient for different adsorbent particle sizes and varying flow rates are obtained and compared for both the scales. Simulation is based on the criterion which identifies the emergence of non-Darcy flow.


Sign in / Sign up

Export Citation Format

Share Document