Two energetic complexes incorporating 3,5-dinitrobenzoic acid and azole ligands: microwave-assisted synthesis, favorable detonation properties, insensitivity and effects on the thermal decomposition of RDX

2016 ◽  
Vol 40 (9) ◽  
pp. 7779-7786 ◽  
Author(s):  
Qi Yang ◽  
Jing Ge ◽  
Qibing Gong ◽  
Xiaxia Song ◽  
Jinwen Zhao ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Microwave Assisted Synthesis ◽  
Detonation Properties ◽  
Microwave Assisted ◽  
Green Propellants

The two energetic complexes reported may act as attractive candidates for green propellants.

scholarly journals Microwave-assisted synthesis of layered basic zinc acetate nanosheets and their thermal decomposition into nanocrystalline ZnO

2014 ◽  
Vol 9 (1) ◽  
pp. 11 ◽  
Author(s):  
Afshin Tarat ◽  
Chris J Nettle ◽  
Daniel T J Bryant ◽  
Daniel R Jones ◽  
Mark W Penny ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Zinc Acetate ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted

MICROWAVE-ASSISTED SYNTHESIS AND CATALYTIC PERFORMANCE OF HIERARCHICAL Cu2O NANOSTRUCTURES

NANO ◽  
2013 ◽  
Vol 08 (05) ◽  
pp. 1350047 ◽  
Author(s):  
XUE-YUN GONG ◽  
YU-PENG GAO ◽  
LI-BO WANG ◽  
PENG-FEI GUO
Keyword(s):  
Thermal Decomposition ◽  
Large Scale ◽  
Copper Acetate ◽  
Great Influence ◽  
Catalytic Performance ◽  
Decomposition Temperature ◽  
Microwave Assisted Synthesis ◽  
X Ray Diffraction ◽  
Experimental Conditions ◽  
Microwave Assisted

Hierarchical Cu 2 O nanostructures have been successfully fabricated on a large scale using copper acetate and glucose as starting reactants, CTAB as an additive via a microwave-assisted process. The influences of CTAB dosage and reaction time on the morphology of the products were investigated. The resulting Cu 2 O nanostructures were characterized by means of X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM). FESEM images show that the Cu 2 O nanostructures are microsphere, which are composed of nanoparticles. The concentration of CTAB plays a key role in the growth of Cu 2 O nanostructures under experimental conditions. The possible formation mechanism of these hierarchical Cu 2 O nanostructures has been proposed. Meanwhile, the catalytic performances of these Cu 2 O microspheres for thermal decomposition of ammonium perchlorate (AP) were investigated using DSC. The results revealed that Cu 2 O have a great influence on the thermal decomposition of AP. The additions of Cu 2 O powders lower the high decomposition temperature of AP.

Microwave Assisted Synthesis of ZnO Calthrop-Like Nanostructures in Ionic-Liquid

2011 ◽  
Vol 295-297 ◽  
pp. 1397-1401 ◽  
Author(s):  
Ju Gong Zheng ◽  
Ting Yang
Keyword(s):  
Aqueous Solution ◽  
Thermal Decomposition ◽  
Ionic Liquid ◽  
Zno Nanorods ◽  
Reaction Medium ◽  
Wurtzite Structure ◽  
Microwave Assisted Synthesis ◽  
Nano Structure ◽  
Microwave Assisted ◽  
Growth Mechanics

ZnO Calthrop-like framework have been synthesized via a microwave assisted way by thermal decomposition of precursors in the ionic liquid 1-butyl-3-ethyl imidazolium tetrafluoroborate ([Beim]BF4) aqueous solution. The structure of [Beim]BF4were analyzed by means of IR and 1HNMR, The as-samples were characterized by XRD, SEM and UV techniques. The results showed that the as-prepared ZnO have wurtzite structure. nanorods have a diameter of 50 nm to100 nm and lengths of about 3 μm , and the ionic liquid [Beim]BF4can not only act as a reaction medium but also modify ZnO nanorods in the reaction. The growth mechanics of ZnO nano-structure was preliminary studied.

Microwave Assisted Synthesis of Cationic Amino Sugar Surfactants

2020 ◽  
Vol 57 (3) ◽  
pp. 265-272
Author(s):  
Priya S. Singh ◽  
Aizaz Shaikh ◽  
Aditi Deshmukh ◽  
Amit P. Pratap
Keyword(s):  
Amino Sugar ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted
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