Structural analysis of elastically bent organic crystals using in situ indentation and micro-Raman spectroscopy

2017 ◽  
Vol 53 (97) ◽  
pp. 13035-13038 ◽  
Author(s):  
Manish Kumar Mishra ◽  
Kamini Mishra ◽  
S. A. Syed Asif ◽  
Praveena Manimunda
Keyword(s):  
Raman Spectroscopy ◽  
Structural Analysis ◽  
Structural Dynamics ◽  
Bending Test ◽  
Organic Crystals ◽  
Three Point Bending ◽  
Micro Raman Spectroscopy

The structural dynamics of two elastically bendable, halogenated N-benzylideneaniline organic crystals were studied using an in situ three-point bending test and Raman spectroscopy.

scholarly journals Additive Manufacturing-Based In Situ Consolidation of Continuous Carbon Fibre-Reinforced Polycarbonate

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2450
Author(s):  
Andreas Borowski ◽  
Christian Vogel ◽  
Thomas Behnisch ◽  
Vinzenz Geske ◽  
Maik Gude ◽  
...  
Keyword(s):  
Additive Manufacturing ◽  
Carbon Fibre ◽  
Bending Test ◽  
Thermoplastic Composites ◽  
Experimental Investigations ◽  
Material Structure ◽  
Three Point Bending ◽  
Continuous Fibre ◽  
Local Material

Continuous carbon fibre-reinforced thermoplastic composites have convincing anisotropic properties, which can be used to strengthen structural components in a local, variable and efficient way. In this study, an additive manufacturing (AM) process is introduced to fabricate in situ consolidated continuous fibre-reinforced polycarbonate. Specimens with three different nozzle temperatures were in situ consolidated and tested in a three-point bending test. Computed tomography (CT) is used for a detailed analysis of the local material structure and resulting material porosity, thus the results can be put into context with process parameters. In addition, a highly curved test structure was fabricated that demonstrates the limits of the process and dependent fibre strand folding behaviours. These experimental investigations present the potential and the challenges of additive manufacturing-based in situ consolidated continuous fibre-reinforced polycarbonate.

Combined synchrotron x-ray diffraction and micro-Raman for following in situ the growth of solution-deposited YBa2Cu3O7 thin films

2005 ◽  
Vol 20 (12) ◽  
pp. 3270-3273 ◽  
Author(s):  
F. Berberich ◽  
H. Graafsma ◽  
B. Rousseau ◽  
A. Canizares ◽  
R. Ramy Ratiarison ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Additional Information ◽  
Micro Raman Spectroscopy ◽  
High Temperature Process ◽  
Structural Growth ◽  
Metal Organic ◽  
Insight Into

A unique combination of in situ synchrotron x-ray diffraction and in situ micro-Raman spectroscopy was used to study the growth process of YBa2Cu3O6+x films obtained by metal organic decomposition using trifluoroacetate precursor on LaAlO3 substrates. The techniques give complementary information: x-ray diffraction gives insight into the structural growth, whereas micro-Raman spectroscopy gives information of the chemical composition with additional information on the texture. To perform both experiments in situ, a special high-temperature process chamber was designed.

Enhanced yield strength in iron nanocomposite with in situ grown single-wall carbon nanotubes

2006 ◽  
Vol 21 (2) ◽  
pp. 522-528 ◽  
Author(s):  
A. Goyal ◽  
D.A. Wiegand ◽  
F.J. Owens ◽  
Z. Iqbal
Keyword(s):  
Carbon Nanotubes ◽  
Raman Spectroscopy ◽  
Yield Strength ◽  
Vapor Deposition ◽  
Single Wall Carbon Nanotubes ◽  
Iron Matrix ◽  
Single Wall Carbon ◽  
X Ray ◽  
Micro Raman Spectroscopy

The yield strength of iron-carbon nanotube composites fabricated by in situ chemical vapor deposition of 2.2 vol% single-wall carbon nanotubes (SWNTs) inside an iron matrix showed substantial enhancement up to 45%, relative to that of similarly treated pure iron samples without carbon nanotubes of the same piece density. The work hardening coefficient and the Vickers hardness coefficient also significantly increased in these composites relative to the reference samples. X-ray diffraction together with energy dispersive x-ray measurements and micro-Raman spectroscopy indicated no concomitant formation of carbides and very little amorphous carbon during the vapor deposition process. Micro-Raman spectroscopy and scanning and transmission electron microscopy showed spectral signatures and images, respectively, indicating the formation and dispersion of SWNTs within the cavities of the iron matrix. It is suggested that the increased strength of the nanocomposites was due to the mechanical support provided to these cavities by the extremely strong SWNTs.

scholarly journals Investigation of laser-irradiated structure evolution and surface modification by in situ Micro-Raman spectroscopy

Vacuum ◽  
2018 ◽  
Vol 155 ◽  
pp. 376-379
Author(s):  
Chao Li ◽  
Guoxiang Wang ◽  
Xianghua Zhang ◽  
Yawen Zhang
Keyword(s):  
Raman Spectroscopy ◽  
Surface Modification ◽  
Structure Evolution ◽  
Micro Raman Spectroscopy

Analysis of in situ water transport in Nafion® by confocal micro-Raman spectroscopy

2011 ◽  
Vol 196 (2) ◽  
pp. 652-658 ◽  
Author(s):  
Yuichiro Tabuchi ◽  
Rei Ito ◽  
Shohji Tsushima ◽  
Shuichiro Hirai
Keyword(s):  
Raman Spectroscopy ◽  
Water Transport ◽  
Micro Raman Spectroscopy
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