Long-chain α–ω diols from renewable fatty acids via tandem olefin metathesis–ester hydrogenation

2017 ◽  
Vol 19 (7) ◽  
pp. 1678-1684 ◽  
Author(s):  
Angela Gonzalez-de-Castro ◽  
Elena Cosimi ◽  
Mae Joanne B. Aguila ◽  
Piotr Gajewski ◽  
Mike Schmitkamp ◽  
...  

Long chain α–ω diols were readily accessed from renewable fatty acid methyl esters following an orthogonal tandem self-metathesis–ester hydrogenation protocol.

1999 ◽  
Vol 40 (21) ◽  
pp. 4041-4044 ◽  
Author(s):  
Julie Defretin ◽  
Jairo Saez ◽  
Xavier Franck ◽  
Reynald Hocquemiller ◽  
Bruno Figadère

2017 ◽  
Vol 7 (17) ◽  
pp. 3659-3675 ◽  
Author(s):  
S. M. Danov ◽  
O. A. Kazantsev ◽  
A. L. Esipovich ◽  
A. S. Belousov ◽  
A. E. Rogozhin ◽  
...  

The present critical review reports the recent progress of the last 15 years in the selective epoxidation of vegetable oils and their derivatives, in particular unsaturated fatty acids (UFAs) and fatty acid methyl esters (FAMEs).


2010 ◽  
Vol 88 (9) ◽  
pp. 898-905 ◽  
Author(s):  
Liyan Liu ◽  
Ying Li ◽  
Rennan Feng ◽  
Changhao Sun

A method for simultaneous determination of 16 free fatty acids (FFAs) in serum is described. The method involves conversion of FFAs to fatty acid methyl esters (FAMEs) using the heat of ultrasonic waves followed by gas chromatography and mass spectrometry (GC–MS) analysis. Optimum levels of the variables affecting the yield of FAMEs were investigated. The results indicate that the optimal levels are 55 °C, 60 W, 10% H2SO4/CH3OH, and 50 min. Recoveries ranged from 85.32% to 112.11%, with a detection limit ranging from 0.03 to 0.08 μg mL–1. The linearity, using the linear correlation coefficient, was higher than 0.9914.


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