Microstructural evolution and thermal stability of Fe–Zr metastable alloys developed by mechanical alloying followed by annealing

Author(s):  
S. Sooraj ◽  
V. M. Suntharavel Muthaiah ◽  
P. C. Kang ◽  
Carl C. Koch ◽  
Suhrit Mula
1999 ◽  
Vol 14 (5) ◽  
pp. 1760-1770 ◽  
Author(s):  
H. G. Jiang ◽  
H. M. Hu ◽  
E. J. Lavernia

The synthesis of nanocrystalline Fe, Fe–4 wt% Al, and Fe–10 wt% Al solid solutions by SPEX ball milling has been studied. The microstructural evolution during ball milling, as well as subsequent heat treatment, has been characterized. The results demonstrate that ball milling promotes the formation of αFe–4 wt% Al and αFe–10 wt% Al solid solutions by reducing the activation energy of these alloys and generating thermal energy during this process. For Fe–10 wt% Al powders milled for various time intervals up to approximately 20 min, the FeAl intermetallic compound is formed. For alloys annealed at temperatures ranging from 600 to 1000 °C, the addition of 10 wt% Al to Fe significantly enhances the thermal stability of the nanocrystalline Fe–Al alloys. Interestingly, the addition of Al within the range of 4–10 wt% seems to have little effect on the thermal stability of these alloys annealed under the same conditions. Also, the thermal stability improves for alloys milled in air as opposed to those processed using Ar.


2018 ◽  
Vol 101 (7) ◽  
pp. 3205-3221 ◽  
Author(s):  
Daxin Li ◽  
Zhihua Yang ◽  
Dechang Jia ◽  
Delong Cai ◽  
Shengjin Wang ◽  
...  

2011 ◽  
Vol 176 (20) ◽  
pp. 1637-1643 ◽  
Author(s):  
Moni Kanchan Datta ◽  
Da-Tren Chou ◽  
Daeho Hong ◽  
Partha Saha ◽  
Sung Jae Chung ◽  
...  

2007 ◽  
Vol 534-536 ◽  
pp. 233-236 ◽  
Author(s):  
N.T.H. Oanh ◽  
Pyuck Pa Choi ◽  
Ji Soon Kim ◽  
Dae Hwan Kwon ◽  
Young Soon Kwon

Ti-Cu-Ni-Sn quaternary amorphous alloys of Ti50Cu32Ni15Sn3, Ti50Cu25Ni20Sn5, and Ti50Cu23Ni20Sn7 composition were prepared by mechanical alloying in a planetary high-energy ballmill (AGO-2). The amorphization of all three alloys was found to set in after milling at 300rpm speed for 2h. A complete amorphization was observed for Ti50Cu32Ni15Sn3 and Ti50Cu25Ni20Sn5 after 30h and 20h of milling, respectively. Differential scanning calorimetry analyses revealed that the thermal stability increased in the order of Ti50Cu32Ni15Sn3, Ti50Cu25Ni20Sn5, and Ti50Cu23Ni20Sn7.


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