Bulk MgB 2 superconductor with high critical current density synthesized by self-propagating high-temperature synthesis method

2005 ◽  
Vol 14 (11) ◽  
pp. 2325-2328 ◽  
Author(s):  
Feng Wang-Jun ◽  
Xia Tian-Dong ◽  
Liu Tian-Zuo ◽  
Zhao Wen-Jun ◽  
Wei Zhi-Qiang
2017 ◽  
Vol 19 (2) ◽  
pp. 177 ◽  
Author(s):  
S. Tolendiuly ◽  
S. M. Fomenko ◽  
G. C. Dannangoda ◽  
K. S. Martirosyan

<p>Magnesium diboride can be synthesized under argon ambient, elevated or high pressures. High-pressure syntheses are promising methods for manufacturing of the bulk MgB<sub>2</sub> superconductor material. We have been used high pressure of Ar gas in order to investigate its effect on properties of MgB<sub>2</sub> superconductor such as critical temperature and current density. Bulk MgB<sub>2</sub> superconductor was synthesized from elemental Mg–B powders in thermal explosion mode of self-propagating high-temperature synthesis (SHS) under argon pressure of 25 atm. XRD pattern of the as-synthesized product indicates an almost complete conversion of the reactants to the MgB<sub>2</sub> single phase. Most of the diffractions peaks are related to the MgB<sub>2</sub> polycrystalline bulk material. The impurity fraction is less than 24.3% in total sample and identified as MgO and MgB<sub>4</sub> secondary phases. The positive effect of pressure of Ar gas during synthesis of MgB2 on critical current density JC has been confirmed. The critical current density of the sample was achieved in high pressure reactor was 3.8×10<sup>6</sup> A/cm<sup>2</sup>. A superconducting volume fraction of 16% under a magnetic field of 10 Oe was obtained at 5 K, indicating that the superconductivity was bulk in nature. The succeeded level of superconductor parameters of the high-pressure synthesized MgB<sub>2</sub> and the possibility to produce a large bulk products make this technology very promising for practical applications.</p>


2003 ◽  
Vol 18 (8) ◽  
pp. 1842-1848 ◽  
Author(s):  
F. Maglia ◽  
C. Milanese ◽  
U. Anselmi-Tamburini ◽  
Z. A. Munir

Microalloying of MoSi2 to form Mo(1−x)MexSi2 (Me = Nb or V) was investigated by the self-propagating high-temperature synthesis method. With alloying element contents up to 5 at.%, a homogeneous C11b solid solution was obtained. For higher contents of alloying elements, the product contained both the C11b and the hexagonal C40 phases. The relative amount of the C40 phase increases with an increase in the content of alloying metals in the starting mixture. The alloying element content in the hexagonal C40 Mo(1−x)MexSi2 phase was nearly constant at a level of about 12 at.% for all starting compositions. In contrast, the content of the alloying elements in the tetragonal phase is considerably lower (around 4 at.%) and increases slightly as the Me content in the starting mixture is increased.


2003 ◽  
Vol 82 (23) ◽  
pp. 4113-4115 ◽  
Author(s):  
H. Fang ◽  
S. Padmanabhan ◽  
Y. X. Zhou ◽  
K. Salama

2001 ◽  
Vol 689 ◽  
Author(s):  
Shara S. Shoup ◽  
Marvis K. White ◽  
Steve L. Krebs ◽  
Natalie Darnell ◽  
Adam C. King ◽  
...  

ABSTRACTThe innovative Combustion Chemical Vapor Deposition (CCVD) process is a non-vacuum technique that is being investigated to enable next generation products in several application areas including high-temperature superconductors (HTS). In combination with the Rolling Assisted Biaxially Textured Substrate (RABiTS) technology, the CCVD process has significant promise to provide low-cost, high-quality lengths of YBCO coated conductor. The CCVD technology has been used to deposit both buffer layer coatings as well as YBCO superconducting layers. A buffer layer architecture of strontium titanate and ceria have been deposited by CCVD on textured nickel substrates and optimized to appropriate thicknesses and microstructures to provide templates for growing PLD YBCO with high critical current density values. The CCVD buffer layers have been scaled to meter plus lengths with good epitaxial uniformity along the length. A short sample cut from one of the lengths enabled high critical current density PLD YBCO. Films of CCVD YBCO superconductors have been grown on single crystal substrates with critical current densities over 1 MA/cm2. Work is currently in progress to combine both the buffer layer and superconductor technologies to produce high-quality coupons of HTS tape made entirely by the non-vacuum CCVD process.


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