scholarly journals Carboxymethyl cellulose synthesis from durian seed flour: The effect of sodium chloroacetate variation

2021 ◽  
Vol 1122 (1) ◽  
pp. 012094
Author(s):  
MHS Ginting ◽  
A Utama ◽  
H Muhammad ◽  
Maulida ◽  
R Tambun
2021 ◽  
Vol 11 (4) ◽  
pp. 80-88
Author(s):  
Muzakkir Mohammad Zainol ◽  
Nurul Suhada Ab Rasid ◽  
Mohd Asmadi ◽  
Nor Aishah Saidina Amin

The synthesis of carboxymethyl cellulose (CMC) generally uses isolated crude cellulose with alkaline or acid pretreatment followed by bleaching with sodium chlorite. In this study, the simple [BMIM][Cl] ionic liquid was used as a solvent in the pretreatment process before conduct the bleaching process with hydrogen peroxide (H2O2) to isolate cellulose from empty fruit bunch (EFB) for further synthesis of CMC. The isolated crude EFB cellulose obtained was converted to CMC by adding 30 wt.% NaOH and various concentrations of sodium monochloroacetic acid (SMCA) at 55 °C for 3 h. The effects of SMCA concentration on the degree of substitution (DS) and CMC yield were investigated. The physicochemical properties of the CMC products were characterized using proton nuclear magnetic resonance, scanning electron microscope-energy dispersive spectrometry, X-ray diffraction, and thermogravimetric analysis. Based on the results, CMC was demonstrated to be synthesized using ionic liquid pretreatment with H2O2 bleaching. Carboxymethyl cellulose synthesized in this study showed a high DS of 0.82. The CMC synthesized from EFB cellulose through ionic liquid pretreatment presented good chemical and physical properties as that reported in other studies.


2021 ◽  
Vol 9 (2) ◽  
pp. 79-88
Author(s):  
A. Apriantini ◽  
D. Afriadi ◽  
N. Febriyani ◽  
I. I. Arief

Durian seeds are waste products from durian fruit that have not been utilized properly. Durian seedflour contain high starch as well as tapioca flour, therefore, durian seed flour can be combined withtapioca flour as a filler for sausage dough, in order to reduce production costs of sausage products. Theaim of this study was to analyze the physicochemical, microbiological and organoleptic properties of beefsausage with the addition of 0%, 25% and 50% durian seed flour from a maximum 30% of the flour usedin making sausages. The results of physical characteristics showed that the addition of durian seed flourhad a significant effect (P <0.05) on the cohesiveness of sausages and had no significant effect (P>0.05) onother physical characteristics of sausages. The microbiological assay showed that durian seed flour didnot affect the total plate count (TPC) of beef sausages. However, the total plate count of the sausages withthe addition of 25% durian seed flour still met the SNI (Indonesian National Standard) for sausages,instead of sausages with 50% durian seed flour addition. The results of chemical analysis showed that theaddition of durian seed flour had no affect on moisture content, ash content, fat content, protein content,and carbohydrate content of the sausages. The hedonic test values on the parameters of aroma, color,texture and general appearance also showed no significant effect (P> 0.05), except for taste parameters.The hedonic quality test value also showed that the addition of durian seed flour had no different effect(P> 0.05) on the parameters of aroma, color, texture, and general appearance, but had different effect (P<0.05) on the sausage taste. The addition of durian seed flour produced a distinctive taste which coverthe flavor of sausage.


Food Research ◽  
2021 ◽  
Vol 5 (4) ◽  
pp. 374-381
Author(s):  
Siti Faridah M.A. ◽  
Nur Atikah M.R.L. ◽  
Jau-Shya L. ◽  
Hasmadi M. ◽  
Mohd Rosni S. ◽  
...  

This study was aimed at assessing the physicochemical and thermal properties of flour, acquired from the seeds of three native Sabah durian species. The three durian species concerned are the Dalit, Sukang and Pulu. Flour deriving from the seeds of the dalit (DDSF), sukang (DSSF) and pulu (DPSF) durian species, were put through a physicochemical, pasting and thermal characteristics assessment process. The protein content in flours, derived from the seeds of durian native to Sabah, demonstrated a high capacity for the absorption of both water (r = -0.855, p<0.01), and oil (r = 0.921, p<0.01). DPSF, which holds the most protein content at 6.92%, demonstrated the lowest water absorption capacity, and greatest oil absorption capacity (p<0.05). Moreover, DPSF was observed to have the lowest swelling power, solubility and peak viscosity (p<0.05). In terms of pasting temperature, no outstanding disparities were detected between the three durian seed flours (p>0.05), but they were considered to have high pasting temperatures. The lowest setback viscosity (p<0.05) displayed by DPSF, is an indication that the following gelatinization, will quickly dissolve. Additionally, the enthalpy ΔH of DPSF revealed as 0.29 J/g (p<0.05) is deemed significantly low. This undertaking delves into the physicochemical and thermal characteristics of durian seed flour, to its use as composite flour.


Author(s):  
Dewita ◽  
Syahrul ◽  
S Loekman ◽  
Restu ◽  
S W Sidauruk
Keyword(s):  

2016 ◽  
Vol 17 (4) ◽  
pp. 1-8 ◽  
Author(s):  
P Kimani ◽  
P Kareru ◽  
S Madivoli ◽  
P Kairigo ◽  
E Maina ◽  
...  

LWT ◽  
2015 ◽  
Vol 63 (1) ◽  
pp. 184-190 ◽  
Author(s):  
Hamed Mirhosseini ◽  
Nur Farhana Abdul Rashid ◽  
Bahareh Tabatabaee Amid ◽  
Kok Whye Cheong ◽  
Milad Kazemi ◽  
...  

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