Detailed structural characterisation of semiconductors with X-ray scattering

Author(s):  
P.F. Fewster
2009 ◽  
Vol 182 ◽  
pp. 012066 ◽  
Author(s):  
Emil Indrea ◽  
Anca Peter ◽  
Danut T Silipas ◽  
Simina Dreve ◽  
Ramona-Crina Suciu ◽  
...  

2006 ◽  
Vol 253 (1) ◽  
pp. 112-117 ◽  
Author(s):  
C. Renard ◽  
O. Durand ◽  
X. Marcadet ◽  
J. Massies ◽  
O. Parillaud

2003 ◽  
Vol 17 (21) ◽  
pp. 3857-3863 ◽  
Author(s):  
R. Stefan ◽  
V. Simon ◽  
E. Indrea

The effect of silver addition to bismuth-borate glasses with low lime content on their structure is evidenced from X-ray scattering measurements. The radius of the first coordination spheres was determined from the correlation function g(r). The larger radius values obtained for the first coordination spheres by adding silver denotes a diminution of the atom packing in this system. Further atoms from the third and fourth coordination spheres occur in a less distorted configuration than in the precursor CaO-Bi 2 O 3- B 2 O 3 vitreous compound.


2020 ◽  
Author(s):  
Susanne Seibt ◽  
Timothy Ryan

With the advent of new in situ structural characterisation techniques including X-ray scattering, there has been an increased interest in investigations of the reaction kinetics of nucleation and growth of nanoparticles as well as self-assembly processes. In this chapter, we discuss the applications of microfluidic devices specifically developed for the investigation of time resolved analysis of growth kinetics and structural evolution of nanoparticles and nanofibers. We focus on the design considerations required for spectrometry and SAXS analysis, the advantages of using a combination of SAXS and microfluidics for these measurements, and discuss in an applied fashion the use of these devices for time-resolved research.


Author(s):  
Eva-Maria Mandelkow ◽  
Eckhard Mandelkow ◽  
Joan Bordas

When a solution of microtubule protein is changed from non-polymerising to polymerising conditions (e.g. by temperature jump or mixing with GTP) there is a series of structural transitions preceding microtubule growth. These have been detected by time-resolved X-ray scattering using synchrotron radiation, and they may be classified into pre-nucleation and nucleation events. X-ray patterns are good indicators for the average behavior of the particles in solution, but they are difficult to interpret unless additional information on their structure is available. We therefore studied the assembly process by electron microscopy under conditions approaching those of the X-ray experiment. There are two difficulties in the EM approach: One is that the particles important for assembly are usually small and not very regular and therefore tend to be overlooked. Secondly EM specimens require low concentrations which favor disassembly of the particles one wants to observe since there is a dynamic equilibrium between polymers and subunits.


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