Effect of human saliva on surface degradation of composite resins

1991 ◽  
Vol 99 (3) ◽  
pp. 254-261 ◽  
Author(s):  
INGE BIRK LARSEN ◽  
ERIK GHRISTIAN MUNKSGAARD
Author(s):  
Gisseli Bertozzi Ávila ◽  
Sergio Candido Dias ◽  
Mariana Lima da Costa Valente ◽  
José Augusto Marcondes Agnelli ◽  
Andréa Candido dos Reis

Objective: The aesthetics of dental materials is extremely important for the success of oral rehabilitation. Thus, in the present study we evaluated the color stability and the surface degradation of three micro hybrid composite resins after accelerated artificial aging process (AAA). Methods: Were prepared 24 specimens (n=8) for each material: Solidex, Artglass and Cesead, dimensions of Ø 15 mm by 2 mm in thickness. The samples were subjected to color analysis, before and after AAA, in a spectrophotometer according to the CIE L*a*b* parameters, and a sample of each material, was selected for morphological evaluation under scanning electron microscopy (SEM). The data were submitted to one-way ANOVA and Tukey test (α=0.05). Results: Artglass showed higher stability regarding the presence of red and yellow (p<0.05) when subjected to the AAA and fewer of these pigments (p<0.05) when compared to the Cesead and Solidex, which showed the highest luminance stability (p<0.05). ΔE Cesead was the most unstable (p<0.05). All resins analyzed by SEM showed superficial degradation when submitted to the AAA, mainly in resin Cesead. Conclusion: All materials analyzed demonstrate color change and surface degradation, Cesead resin showed the worse results.


2008 ◽  
Vol 16 (4) ◽  
pp. 257-265 ◽  
Author(s):  
Ana Carolina Valinoti ◽  
Beatriz Gonçalves Neves ◽  
Eduardo Moreira da Silva ◽  
Lucianne Cople Maia

2019 ◽  
Vol 14 (1) ◽  
pp. 87-92 ◽  
Author(s):  
Tânia Mara da Silva ◽  
Débora Cristina Barbosa Dantas ◽  
Tainá Teixeira Franco ◽  
Lucas Teixeira Franco ◽  
Maria Filomena Rocha Lima Huhtala

Biomimetics ◽  
2018 ◽  
Vol 3 (3) ◽  
pp. 23 ◽  
Author(s):  
Rasoul Sahebalam ◽  
Alireza Boruziniat ◽  
Fahimeh Mohammadzadeh ◽  
Abdolrasoul Rangrazi

Saliva contamination is a major clinical problem in restorative procedures. The purpose of this study was to evaluate the effect of the time of salivary contamination during light curing on the degree of conversion and the microhardness of a restorative composite resin. Eight groups of 10 samples for measuring the microhardness and eight groups of 5 samples for evaluating the degree of conversion were prepared. The samples of each group were contaminated with human saliva at a certain time. The first group (T0) was contaminated before light curing. The specimens in groups T2–T30 were contaminated at 2, 5, 10, 15, 20 and 30 s after the start of light curing, respectively. The samples of group T40 were contaminated after light curing. The degree of conversion and the microhardness of the specimens were measured by Fourier transform infrared (FTIR) spectroscopy and Vickers hardness testing techniques, respectively. The results of this study revealed that there were no significant differences between the groups in terms of the degree of conversion of the composite resin. Consistent with the findings for the degree of conversion, significant differences in the microhardness between the groups were not found. In conclusion, from a clinical point of view, the results of our study showed that the time of salivary contamination (before, during or after light curing of composite resin) has no significant effect on the polymerization (degree of conversion) and one of the important mechanical properties of dental composite resins (microhardness).


2011 ◽  
Vol 36 (3) ◽  
pp. 311-317 ◽  
Author(s):  
CA Pereira ◽  
E Eskelson ◽  
V Cavalli ◽  
PCS Liporoni ◽  
AOC Jorge ◽  
...  

SUMMARY This study evaluated Streptococcus mutans biofilm adhesion on the surface of three composite resins (nanofilled, Filtek Z350, 3M ESPE, Salt Lake City, UT, USA; nanohybrid, Vit-1-escence, Ultradent Products, South Jordan, UT, USA; and microhybrid, Esthet X, Dentsply, Milford, DE, USA) following different finishing and polishing techniques. Sixty standardized samples (6 × 3 mm) of each composite were produced and randomly divided into three finishing and polishing treatments (n=20): 1) control group: composite resin surface in contact with Mylar matrix strips with no finishing or polishing performed, 2) Sof-Lex aluminum oxide disc technique (3M ESPE, and 3) carbide bur finishing and Astrobrush polishing technique (Ultradent). Half the samples of each group were incubated in human saliva for 1 hour, and all the samples were subjected to S mutans (ATCC 35688) biofilm development. The mean log of CFU/mL present in the S mutans biofilm was calculated, and data were statistically analyzed by three-way analysis of variance and the Tukey test (p&lt;0.05). Human saliva incubation promoted a significant increase of bacterial adherence on all three of the composites' surfaces, regardless of the polishing treatment performed (p&lt;0.05). Of the three, the nanofilled composite (Filtek Z350) had the lowest bacterial adherence with each of the finishing and polishing techniques despite the presence or absence of human saliva (p&lt;0.05). Mylar matrix strips (control group) promoted the lowest bacterial adhesion on the surface of the microhybrid and nanofilled composites in the absence of human saliva.


2014 ◽  
Vol 25 (4) ◽  
pp. 321-326 ◽  
Author(s):  
Eliseu A. Münchow ◽  
Ana Cláudia A. Ferreira ◽  
Raissa M. M. Machado ◽  
Tatiana S. Ramos ◽  
Sinval A. Rodrigues-Junior ◽  
...  

Composite resins may undergo wear by the action of chemical substances (e.g., saliva, alcohol, bacterial acids) of the oral environment, which may affect the material's structure and surface properties. This study evaluated the effect of acidic substances on the surface properties of a micro-hybrid composite resin (Filtek Z-250). Eighty specimens were prepared, and baseline hardness and surface roughness (KMN0 and Ra0, respectively) were measured. The specimens were subjected to sorption (SO) and solubility (SL) tests according to ISO 4049:2009, but using different storage solutions: deionized water; 75/25 vol% ethanol/water solution; lactic acid; propionic acid; and acetic acid. The acids were used in two concentrations: PA and 0.02 N. pH was measured for all solutions and final hardness (KMN1) and surface roughness (Ra1) were measured. Data were analyzed with paired t-tests and one-way ANOVA and Tukey's test (a=5%). All solutions decreased hardness and increased the Ra values, except for the specimens stored in water and 0.02 N lactic acid, which maintained the hardness. All solutions produced similar SO and SL phenomena, except for the 0.02 N lactic acid, which caused lower solubility than the other solutions. Ethanol showed the highest pH (6.6) and the 0.02 N lactic acid the lowest one (2.5). The solutions affected negatively the surface properties of the composite resin; in addition, an acidic pH did not seem to be a significant factor that intensifies the surface degradation phenomena.


Biomaterials ◽  
2002 ◽  
Vol 23 (7) ◽  
pp. 1707-1719 ◽  
Author(s):  
F. Jaffer ◽  
Y. Finer ◽  
J.P. Santerre

2004 ◽  
Vol 83 (1) ◽  
pp. 22-26 ◽  
Author(s):  
Y. Finer ◽  
J.P. Santerre

Pseudocholinesterase (PCE) and cholesterol esterase (CE) can hydrolyze bisphenylglycidyl dimethacrylate (bisGMA) and triethylene glycol dimethacrylate (TEGDMA) monomers. This study will test the hypothesis that enzyme activities showing CE and PCE character are found in human saliva at levels sufficient to hydrolyze ester-containing composites important to restorative denstistry. The study also seeks to ask if the active sites of CE and PCE with respect to composite could be inhibited. Photo-polymerized model composite resin was incubated in PCE and CE solutions, in the presence and absence of a specific esterase inhibitor, phenylmethylsulfonyl fluoride (PMSF). Incubation solutions were analyzed for resin degradation products by high-performance liquid chromatography (HPLC), UV spectroscopy, and mass spectrometry. Saliva was found to contain both hydrolase activities at levels that could degrade composite resins. PMSF inhibited the composite degradation, indicating a material hydrolysis mechanism similar to the enzymes’ common function.


2002 ◽  
Vol 15 (1) ◽  
pp. 19-22 ◽  
Author(s):  
T. Katarzyna Różyło ◽  
Anna Żabińska ◽  
Ingrid Różyło-Kalinowska
Keyword(s):  

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