scholarly journals Color stability evaluation of micro hybrid composite resins submitted to accelerated artificial aging

Author(s):  
Gisseli Bertozzi Ávila ◽  
Sergio Candido Dias ◽  
Mariana Lima da Costa Valente ◽  
José Augusto Marcondes Agnelli ◽  
Andréa Candido dos Reis

Objective: The aesthetics of dental materials is extremely important for the success of oral rehabilitation. Thus, in the present study we evaluated the color stability and the surface degradation of three micro hybrid composite resins after accelerated artificial aging process (AAA). Methods: Were prepared 24 specimens (n=8) for each material: Solidex, Artglass and Cesead, dimensions of Ø 15 mm by 2 mm in thickness. The samples were subjected to color analysis, before and after AAA, in a spectrophotometer according to the CIE L*a*b* parameters, and a sample of each material, was selected for morphological evaluation under scanning electron microscopy (SEM). The data were submitted to one-way ANOVA and Tukey test (α=0.05). Results: Artglass showed higher stability regarding the presence of red and yellow (p<0.05) when subjected to the AAA and fewer of these pigments (p<0.05) when compared to the Cesead and Solidex, which showed the highest luminance stability (p<0.05). ΔE Cesead was the most unstable (p<0.05). All resins analyzed by SEM showed superficial degradation when submitted to the AAA, mainly in resin Cesead. Conclusion: All materials analyzed demonstrate color change and surface degradation, Cesead resin showed the worse results.

2013 ◽  
Vol 14 (4) ◽  
pp. 718-723 ◽  
Author(s):  
P Sarveshwar Reddy ◽  
KL Sunil Tejaswi ◽  
Suneeth Shetty ◽  
BM Annapoorna ◽  
Sudarshan C Pujari ◽  
...  

ABSTRACT Background Consumption of certain beverages may affect the esthetic and physical properties of the resin composite, thereby undermining the quality of restorations. Aim To analyze the effect of three beverages (cola, coffee, tea) on color stability and surface roughness of three different types of resin composites at various time intervals in vitro. Materials and methods Nano, microhybrid and hybrid resin composites were used. Each material was randomly divided into four equal subgroups of 10 samples each according to the beverages used (cola, coffee, tea, distilled water). The samples were immersed in each beverage for 1, 15 and 30 days. Surface roughness and color changes measurements were noted at the baseline—the first, fifteenth and thirteenth day. Results It was found that nanoresin composite followed by microhybrid and hybrid showed least surface roughness and color change. The Coke beverage subgroup showed more surface roughness and the subgroup coffee has shown more color changes with respect to other subgroups. Conclusion All specimens showed discoloration after completion of the test period which was visually perceptible and clinically unacceptable. At the end of 30th day, among the materials, nanofilled composite resin showed comparatively less surface roughness and color change than microhybrid and hybrid composite resins. How to cite this article Reddy PS, Tejaswi KLS, Shetty S, Annapoorna BM, Pujari SC, Thippeswamy HM. Effects of Commonly Consumed Beverages on Surface Roughness and Color Stability of the Nano, Microhybrid and Hybrid Composite Resins: An in vitro Study. J Contemp Dent Pract 2013;14(4): 718-723.


2021 ◽  
Vol 15 (1) ◽  
pp. 53-58
Author(s):  
Lais Sampaio Souza ◽  
Tais Rocha Donato ◽  
Gabriela Alves Cerqueira ◽  
Andrea Nobrega Cavalcanti ◽  
Paula Mathias

Background. Post-cured composite resins exhibit improvements in physical and mechanical properties due to additional polymerization conversion. However, the post-curing techniques might influence the color stability of composite resin materials. Thus, this study evaluated the color stability of a nanofilled composite resin (Filtek Z350 XT - 3M ESPE) subjected to different post-curing techniques. Methods. Sixty samples (color A2) were randomly allocated to six experimental groups (n=10): G1: photoactivation (P) (control); G2: P + microwave oven with distilled water; G3: P + microwave oven without distilled water; G4: P + conventional oven; G5: P + dry-heat sterilizer; G6: P + steam autoclave. All the groups were stored in distilled water for 60 days and immersed daily in 5 mL of a coffee solution for 3 minutes. The color readings (CIEL*a*b* system) were performed at two different time intervals, initially and after 60 days, in a reflectance spectrophotometer (UV-2600; Shimadzu). The colorimetric readings were performed using the Color Analysis software (CIEL*a*b* system). Results. Group G6 exhibited significantly low values of total color change (ΔE=13.16). The control (ΔE=15.32) and G5 (ΔE=15.49) groups exhibited intermediate values, with no difference between them. In turn, the groups in which the resin was heated in a microwave (G2 ΔE=18.55 and G3 ΔE=19.45) exhibited the most significant color changes (one-way ANOVA and Tukey test, P≤0.05). Conclusion. Steam autoclave post-polymerization increased the color stability of the nanofilled resin subjected to artificial aging and coffee immersion.


2020 ◽  
Vol 14 (01) ◽  
pp. 085-091
Author(s):  
Sedighe Sadat Hashemikamangar ◽  
Farnoosh Hoseinpour ◽  
Nazanin Kiomarsi ◽  
Mehrzad Gholampour Dehaki ◽  
Mohammad Javad Kharazifard

Abstract Objectives This study aimed to assess the effect of an optical whitening toothpaste on color stability of microhybrid, nanofilled, and microfilled composite resins and resin-modified glass ionomer (RMGI) cement in comparison of two other toothpastes. Materials and Methods In this experimental study, disc-shaped composite samples were fabricated. The samples were then polished using silicon carbide papers. Twenty-seven samples of each material were fabricated and subjected to colorimetry using a spectrophotometer. Each group of material was then divided into three subgroups for the application of conventional whitening and whitening containing blue covarine toothpastes. One operator brushed the samples with an electric soft toothbrush with circular motion twice a day, each time for 30 seconds. Colorimetry was performed at 0, 1, 7, 30, and 90 days. Statistical Analysis Two-way analysis of variance (ANOVA), one-way ANOVA, and Tukey’s honestly significant difference (HSD) test were used for statistical analysis. Results The interaction effect of type of restorative material and time on ∆E was not significant at baseline or 1 day (p > 0.05). The effect of type of toothpaste on ∆E was not significant at baseline or 1 day (p = 0.78) but the effect of type of material was significant (p < 0.05). The toothpastes had significantly different effects on ∆E of Z250 at all time points (p < 0.05) except for ∆E0–30 (p = 0.106). The toothpastes had significantly different effects on ∆E of Z350 and Gradia at all time points (p < 0.05). The same was true for RMGI except for ∆E0–7 (p = 0.43) and ∆E0–90 (p = 0.52). The majority of color changes caused by toothpastes were not clinically perceivable (∆E < 3.3), except for ∆E0–90 by the whitening toothpaste (∆E = 9), ∆E0–90 by the conventional toothpaste for Z350 (∆E = 3.9), and ∆E0–1 by the whitening toothpaste for RMGI (∆E = 3.7). Conclusion The color change of all composite samples was not clinically perceivable (<3.3) at all time points, which shows that the tested toothpastes do not cause a significant change in color of composite materials.


2021 ◽  
Vol 23 (2) ◽  
pp. 85-91
Author(s):  
Guilherme Ortiz Pinto Cruz ◽  
Larissa Martins Costa ◽  
Cesar Penazzo Lepri ◽  
Ruchele Dias Nogueira ◽  
Regina Guenka Palma-Dibb ◽  
...  

AbstractThe aim of this study was to evaluate the color stability and the surface roughness of different composites brushed with toothpastes presenting different levels of abrasivity. Thirty discs of each material were obtained using michohybrid composites (Brilliant NG and Charisma Diamond) and a nanocomposite (Filtek Z350XT). The initial color (CIELab) and surface roughness (confocal laser scanning microscopy) of resin discs were evaluated. Afterwards, 10 specimens per group were brushed with the following dentifrices: Maximum Cavity Protection, Sensodyne Repair & Protect and Colgate Sensitive Pro-Relief. Brushing was performed with an electric toothbrush equipped with soft bristle head, with standard power and weight, for 30 minutes. Every 30 seconds, 1.0 ml of the slurry was injected between the bristles of the brush and the specimen. After abrasive challenge, the samples had their color and roughness reevaluated. Data were submitted to the Kruskal-Wallis test (color change) or the t-test (surface roughness). The level of significance was 5%. Results: Brushing did not significantly change the color of the composites tested in the study herein . On the other hand, the surface roughness of the composites was significantly affected by the abrasive challenge, regardless of the toothpaste used. The surface roughness change was similar for all the composites. The abrasive challenge with the toothpastes Maximum Cavity protection, Sensodyne Repair & Protect and Colgate Sensitive Pro-Relief was not able to significantly change the color of the composite resins. Nevertheless, the abrasive challenges significantly altered the surface roughness of all the evaluated composites. However, the changes in surface roughness were statistically similar in the microhybrid and nanofilled composites. Keywords: Composites Resins. Dentifrices. Color. ResumoO objetivo deste estudo foi avaliar a estabilidade de cor e a rugosidade superficial de diferentes resinas compostas escovadas com dentifrícios de diferentes níveis de abrasividade. Trinta discos de cada material foram obtidos utilizando compósitos micro-híbridos (Brilliant NG e Charisma Diamond) e um nanocompósito (Filtek Z350XT). A cor inicial (CIELab) e a rugosidade superficial (microscopia confocal de varredura a laser) dos discos de resina foram avaliadas. Em seguida, 10 amostras por grupo foram escovadas com os dentifrícios Máxima Proteção Anticáries, Sensodyne Repair & Protect e Colgate Sensitive Pro-Alívio. A escovação foi realizada com uma escova elétrica com cabeça de cerdas macias, com potência e peso padronizados, durante 30 minutos. A cada 30 segundos, 1,0 ml da pasta era injetada entre as cerdas da escova e a amostra. Após o desafio abrasivo, as amostras tiveram sua cor e rugosidade reavaliadas. Os dados foram submetidos ao teste de Kruskal-Wallis (alteração de cor) ou ao teste t (rugosidade da superfície) (α=5%). A escovação não alterou significativamente a cor dos compósitos. Por outro lado, a rugosidade superficial dos compósitos foi significativamente afetada pelo desafio abrasivo, independentemente do dentifrício utilizado. A alteração da rugosidade superficial foi semelhante para todos os compósitos. O desafio abrasivo com a Máxima Proteção Anticáries, o Sensodyne Repair & Protect e o Colgate Sensitive Pro-Alívio não foi capaz de alterar significativamente a cor das resinas. Diferentemente, os desafios abrasivos alteraram significativamente a rugosidade superficial de todos os compósitos avaliados. No entanto, as mudanças na rugosidade foram estatisticamente semelhantes nos compósitos micro-híbridos e nanoparticulado. Palavras-chave: Resinas Compostas. Dentifrícios. Cor.


2018 ◽  
Vol 20 (3) ◽  
pp. 167
Author(s):  
Ruchele Dias Nogueira ◽  
Rosa Maria Pereira Moisés Barbosa Andrade ◽  
Ailla Carla Rocha Acosta Lancellotti ◽  
Regina Guenka Palma-Dibb ◽  
Vinícius Rangel Geraldo-Martins

ResumoA resina composta é o material restaurador mais utilizado atualmente. Apesar de seu sucesso clínico, o material está sujeito a alterações em suas propriedades físicas, quando exposto ao meio bucal. O objetivo foi avaliar a influência da degradação química na estabilidade de cor e na rugosidade superficial de resinas micro-híbrida e nanoparticulada. Foram confeccionados 40 discos (6,0mm x 2,0mm) da resina composta micro-híbrida (Z250XT) e 40 da resina nanoparticulada (Z350XT). Após a análise da cor inicial e da rugosidade inicial, 10 discos de cada resina foram imersos em saliva artificial (Controle, pH=6,4), suco de laranja (pH= 3,4), refrigerante de limão (pH=2,9) e vinho tinto (pH=3,1), por 4 horas por dia (37ºC) durante 30 dias. Após, foram realizadas as leituras finais de cor e rugosidade. Os dados obtidos para a estabilidade de cor foram analisados pelo Teste de Kruskal-Wallis, seguido pelo Teste de Dunn (α=5%). Para a análise da rugosidade foi utilizado o Teste t para amostras pareadas (α=5%). O manchamento provocado pela saliva artificial, suco de laranja e refrigerante foi similar, mas foi estatisticamente diferente do manchamento produzido pelo vinho, em ambas as resinas testadas. O vinho produziu o mesmo grau de manchamento nas resinas micro-híbrida e nanoparticulada. Foi observado que o suco de laranja, o refrigerante e o vinho promoveram aumento da rugosidade superficial dos discos de resina. Diante disso, concluiu-se que o vinho alterou a cor de resinas compostas micro-híbrida e nanoparticulada, e que a rugosidade superficial dos discos de resina foi alterada por todas as bebidas utilizadas.Palavras chave: Resinas Compostas. Corantes. Cor.Abstract Composite resin is the most used restorative material. Despite its clinical success, it is susceptible to changes in its physical properties when exposed to the oral environment. The aim was to evaluate the influence of acidic beverages on the color stability and on the surface roughness of the nanofilled and micro hybrid composite. Forty discs (6.0mm x 2.0mm) of the micro hybrid composite (Z250XT) and 40 of the nanofilled composite (Z350XT) were manufactured. After the measurement of the initial color and the initial roughness, 10 discs of each composite were individually immersed in artificial saliva (control, pH = 6.4), orange juice (pH=3.4), lime soda (pH = 2.9) and red wine (pH = 3.1) during 4 hours per day at 37°C for 30 days. At the end of the experiment, the final analysis of color and surface roughness were performed. The data obtained for the color stability were analyzed by Kruskal-Wallis and Dunn’s test (α= 5%). For the analysis of the surface roughness, the t test for related samples was used (α= 5%). The color changes promoted by artificial saliva, orange juice and soda were similar, but they were statistically different from staining produced by wine, in both tested composites. Wine produced the same degree of staining in both composites. Orange juice, soda and red wine increased the surface roughness of the composite discs. It was concluded that red wine significantly changes the color of micro hybrid and nanofilled composites. Furthermore, all beverages increased the surface roughness of the composites tested in the study herein.Keywords: Composite Resins. Coloring Agents. Color.


2007 ◽  
Vol 18 (2) ◽  
pp. 119-123 ◽  
Author(s):  
Fernanda de Carvalho Panzeri Pires-de-Souza ◽  
Lucas da Fonseca Roberti Garcia ◽  
Hisham Mohamad Hamida ◽  
Luciana Assirati Casemiro

The purpose of this study was to evaluate, in vitro, the color stability of three composite resins of two different shades (A3 and C3) cured with either a quartz tungsten halogen (QTH) or a light emitting diode (LED) source. Forty specimens (20 x 2 mm) were prepared for each composite (Tetric Ceram®, Heliomolar® and Esthet-X®), being 20 for each shade. In each group, 10 specimens were light-cured using the QTH unit and 10 with the LED source. The shade of the materials was evaluated before and after submitting the specimens to artificial accelerated aging (4 h UV-B/4 h condensing vapor), using a reflection spectrophotometer. deltaE means were calculated and analyzed statistically by 2-way ANOVA and Tukey's test at 5% significance level. Both A3 and C3 shades of Esthet-X composite resin showed the lowest color change when cured with the QTH light, while Tetric C3 cured with the QTH light showed the highest color change.


2016 ◽  
Vol 2016 ◽  
pp. 1-5 ◽  
Author(s):  
Sayna Shamszadeh ◽  
Seyedeh Mahsa Sheikh-Al-Eslamian ◽  
Elham Hasani ◽  
Ahmad Najafi Abrandabadi ◽  
Narges Panahandeh

We aimed to evaluate the color stability of bulk-fill and conventional composite resin with respect to thickness and storage media. Twenty specimens of a conventional composite resin (6 mm diameter and 2 mm thick) and 40 specimens of the bulk-fill Tetric EvoCeram composite resin at two different thicknesses (6 mm diameter and 2 mm thick or 4 mm thick,n=20) were prepared. The specimens were stored in distilled water during the study period (28 d). Half of the specimens were remained in distilled water and the other half were immersed in coffee solution 20 min/d and kept in distilled water between the cycles. Color changes (ΔE) were measured using the CIEL⁎a⁎b⁎color space and a digital imaging system at 1, 7, 14, and 28 days of storage. Data were analyzed using Two-way ANOVA and Tukey’s HSD post hoc test (P<0.05). Composite resins showed significant increase in color changes by time (bulk-fill > conventional;P<0.001). Coffee exhibited significantly more staining susceptibility than that of distilled water (P<0.001). There was greater color changes with increasing the increment thickness, which was significant at 14 (P<0.001) and 28 d (P<0.01). Color change of bulk-fill composite resin was greater than that of the conventional one after coffee staining and is also a function of increment thicknesses.


2020 ◽  
Vol 24 (1) ◽  
Author(s):  
Beatriz Maria Arruda ◽  
Julio Cesar Bassi ◽  
Rafael Pino Vitti ◽  
Renata Siqueira Scatolin

 Objective: The aim of this in vitro study was to evaluate the color stability of different bulk fill composite resins after extrinsic staining with coffee. Material and methods: Forty-eight disk-shaped specimens (6 mm diameter x 2 mm thick) of each composite resin were prepared for color change test. The composite resins were divided into 4 groups (n=12): one conventional composite resin (Filtek Z250) and three bulk-fill composite resins (Filtek Bulk Fill, Aura Bulk Fill, and Opus Bulk Fill). The samples were stained with 20 mL coffee solution for 7 days, with the solution being replaced every 24 h. The color change analysis was performed using a spectrophotometer, according to the CIE Lab formula. Data were analyzed using the Analysis of variance (ANOVA) and Tukey HSD tests (?=0.05). Results: The results revealed significant differences in color change among the composite resins tested (?<0.0001). The Aura Bulk Fill and Opus Bulk Fill showed the highest color change values. Conclusions: Thus, all the resins analyzed were susceptible to extrinsic staining with coffee, and the Filtek Bulk Fill showed the lowest color change value.


Author(s):  
Haleh Kazemi Yazdi ◽  
Negin Nasoohi ◽  
Mahla Benvidi

Objectives: Color stability of composite resins has a significant role in their durability and clinical service. Considering the increasing use of composite resins and their gradual discoloration, this study aimed to assess the efficacy of Listerine whitening mouthwash for color recovery of two discolored composite resins. Materials and Methods: This in-vitro experimental study was performed on 20 samples fabricated of Filtek Z350XT (3M ESPE, St. Paul, MN, USA) and IPS Empress Direct (Ivoclar Vivadent, Schaan, Liechtenstein) composite resins. Primary colorimetry was performed using a spectrophotometer. The samples were immersed in a coffee drink for 7 days. They were then immersed in Listerine mouthwash for 4 minutes daily for 56 days. After this period, the color change of composite resins was reevaluated. Data were analyzed using repeated-measures analysis of variance (ANOVA) and t-test. Results: The primary color change of Z350XT after immersion in coffee was 1.6 times greater than that of IPS composite (P<0.0001). The color recovery of IPS and Z350XT after immersion in the mouthwash was 1.06±0.58 (P<0.01) and 2.58±1.65 (P<0.001) units, respectively. The color change of Z350XT after exposure to the mouthwash was 25% (1.4 times) greater than that of IPS (P<0.01). Conclusion: Both composite resins experienced a clinically unacceptable discoloration after exposure to coffee (∆E>3.3). Filtek Z350XT showed greater color change than IPS. Use of Listerine whitening mouthwash caused significant color recovery in both composite resins.


2021 ◽  
Vol 22 (3) ◽  
pp. 191-194
Author(s):  
Ângela Dalla Nora ◽  
Camila da Silva Rodrigues ◽  
Rachel de Oliveira Rocha

AbstractDespite composite resins capacity to mimic dental tissues, they can discolor over time. However, there is no information on the effect of prebrushing mouthwashes on the composite resin staining. This study aimed to evaluate the effect of prebrushing mouthwashes on the color stability of three composite resins. Twenty specimens of each resin were prepared: Filtek Z250 (3M ESPE –S Paul, MN, USA), Charisma (Heraeus Kulzer GmbH - Hanau - Germany) e EvoluX (Dentsply- Petrópolis - Brazil). Groups were randomly divided accord to the treatment: immersion in prebrushing mouthwash (test group) or immersion in deionized water (control group). Test groups were immersed in 10 ml of prebrushing mouthwash Plax Magic (Colgate-Palmolive, São Bernardo do Campo, SP, Brazil) for 60 s three times a day during 35 days following the manufacturer’s instructions. Color measurements were performed after 24 h of specimen’s preparation and after 7, 14, 21, and 35 days of immersion time. Results showed that prebrushing mouthwash Plax Magic promoted a color change in all the tested materials and evaluation time. The color change was greater in composite resin Charisma, followed by Z250 and EvoluX. Therefore, prebrushing mouthwash promoted a color change in all the materials used. Composite resin Charisma demonstrated less color stability than Filtek Z250 resin and EvoluX resin, which was the most stable.Keywords: Composite Resins. Oral Hygiene. Color.ResumoApesar da capacidade das resinas compostas de mimetizar os tecidos dentais, esses materiais podem ter sua cor alterada com o tempo. No entanto, não há informação na literatura sobre o efeito de evidenciadores de placa na estabilidade de cor desses materiais. Este estudo teve por objetivo avaliar o efeito de um evidenciador de placa na estabilidade de cor e três resinas compostas. Para isso, 20 espécimes de cada resina foram preparados: Filtek Z250 (3M ESPE –S Paul, MN, EUA), Charisma (Heraeus Kulzer GmbH - Hanau - Alemanha) e EvoluX (Dentsply- Petrópolis - Brasil). Os grupos foram aleatoriamente divididos de acordo com o tratamento a ser submetido: imersão no evidenciador de placa (grupo teste) ou imersão em água deionizada (grupo controle). Os grupos teste foram imersos em 10 ml do evidenciador de placa Plax Magic (Colgate-Palmolive, São Bernardo do Campo, SP, Brasil) por 60 s três vezes por dia durante 35 dias, de acordo com a orientações de uso do fabricante. As leituras de cor foram feitas após 24 h da preparação dos espécimes e após 7, 14, 21 e 35 dias de imersão. Os resultados mostraram que o evidenciador de placa Plax Magic promoveu alteração de cor em todos os materiais usados e em todos os tempos de leitura. A alteração de cor foi maior na resina Charisma, seguida da Z250 e EvoluX. Portanto, o evidenciador de placa promove alteração de cor em todos os materiais testados. A resina composta Charisma demonstrou menor estabilidade de cor que as resinas Z250 e EvoluX, que, por sua vez, foi a mais estável. Palavras-chave: Resinas Compostas. Higiene Oral. Cor.


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