An oscillatory pressure sintering of zirconia powder: Rapid densification with limited grain growth

2017 ◽  
Vol 100 (7) ◽  
pp. 2774-2780 ◽  
Author(s):  
Yao Han ◽  
Shuang Li ◽  
Tianbin Zhu ◽  
Zhipeng Xie
Keyword(s):  
Grain Growth ◽  
Zirconia Powder ◽  
Oscillatory Pressure

Relation Between Coarsening and Densification in Solid-state Sintering of Ceramics: Experimental Test on Superfine Zirconia Powder Compacts

1999 ◽  
Vol 14 (4) ◽  
pp. 1389-1397 ◽  
Author(s):  
J. L. Shi
Keyword(s):  
Grain Size ◽  
Grain Growth ◽  
Linear Relation ◽  
Intermediate Stage ◽  
Size Distributions ◽  
Zirconia Powder ◽  
Pore Growth ◽  
Pore Size Distributions ◽  
Powder Compacts ◽  
Compaction Properties

Coarsening (including grain growth and pore growth) and densification behavior of superfine Y-TZP and YSZ powder compacts in the intermediate stage were investigated. It has been found that grain growth in the compacts is basically not affected by the compaction properties, and pore growth is driven by both grain growth and densification. Grain growth alone leads to size-proportional pore growth, and densification results in pore shrinkage. The relation between grain size and density is analyzed to be linear when grain growth and densification are believed to be driven by different stresses under an identical diffusion process. Both theoretical and experimental results show that compaction properties and the heating rate do not alter this linear relation between grain size and density but influence the slope of the linear relation. Larger dihedral angle, higher green density, and narrower particle and pore size distributions are found favorable for the achievement of the grain size-density trajectory with promoted densification and minimized grain growth.

Densification and grain growth in oscillatory pressure sintering of alumina toughened zirconia ceramic composites

2020 ◽  
Vol 845 ◽  
pp. 155644
Author(s):  
Jianye Fan ◽  
Yi Yuan ◽  
Junshan Li ◽  
Jinling Liu ◽  
Ke Zhao ◽  
...  
Keyword(s):  
Grain Growth ◽  
Ceramic Composites ◽  
Zirconia Ceramic ◽  
Oscillatory Pressure

An oscillatory pressure sintering of zirconia powder: Densification trajectories and mechanical properties

2018 ◽  
Vol 101 (5) ◽  
pp. 1824-1829 ◽  
Author(s):  
Yao Han ◽  
Shuang Li ◽  
Tianbin Zhu ◽  
Weiwei Wu ◽  
Di An ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Zirconia Powder ◽  
Powder Densification ◽  
Oscillatory Pressure

Grain Refinement in Titanium-Erbium Alloys

1974 ◽  
Vol 32 ◽  
pp. 522-523
Author(s):  
B. B. Rath ◽  
J. E. O'Neal ◽  
R. J. Lederich
Keyword(s):  
Electron Microscopy ◽  
Size Distribution ◽  
Grain Refinement ◽  
Grain Growth ◽  
Volume Fraction ◽  
Pure Titanium ◽  
Systematic Investigation ◽  
Second Phase ◽  
Titanium Matrix ◽  
Average Size

Addition of small amounts of erbium has a profound effect on recrystallization and grain growth in titanium. Erbium, because of its negligible solubility in titanium, precipitates in the titanium matrix as a finely dispersed second phase. The presence of this phase, depending on its average size, distribution, and volume fraction in titanium, strongly inhibits the migration of grain boundaries during recrystallization and grain growth, and thus produces ultimate grains of sub-micrometer dimensions. A systematic investigation has been conducted to study the isothermal grain growth in electrolytically pure titanium and titanium-erbium alloys (Er concentration ranging from 0-0.3 at.%) over the temperature range of 450 to 850°C by electron microscopy.

Microstructural characterization of a rapidly solidified Al-Fe-V-Si alloy for elevated temperature applications

1988 ◽  
Vol 46 ◽  
pp. 550-551
Author(s):  
R. E. Franck ◽  
J. A. Hawk ◽  
G. J. Shiflet
Keyword(s):  
High Temperature ◽  
Elevated Temperature ◽  
Grain Growth ◽  
Volume Fraction ◽  
Microstructural Characterization ◽  
Second Phase ◽  
Microstructural Stability ◽  
Elevated Temperature Strength ◽  
Temperature Applications

Rapid solidification processing (RSP) is one method of producing high strength aluminum alloys for elevated temperature applications. Allied-Signal, Inc. has produced an Al-12.4 Fe-1.2 V-2.3 Si (composition in wt pct) alloy which possesses good microstructural stability up to 425°C. This alloy contains a high volume fraction (37 v/o) of fine nearly spherical, α-Al12(Fe, V)3Si dispersoids. The improved elevated temperature strength and stability of this alloy is due to the slower dispersoid coarsening rate of the silicide particles. Additionally, the high v/o of second phase particles should inhibit recrystallization and grain growth, and thus reduce any loss in strength due to long term, high temperature annealing.The focus of this research is to investigate microstructural changes induced by long term, high temperature static annealing heat-treatments. Annealing treatments for up to 1000 hours were carried out on this alloy at 500°C, 550°C and 600°C. Particle coarsening and/or recrystallization and grain growth would be accelerated in these temperature regimes.

ZIRCAR ZIRCONIA POWDER TYPE ZYP-4.5

Alloy Digest ◽  
1989 ◽  
Vol 38 (3) ◽  
Keyword(s):  
Fracture Toughness ◽  
Physical Properties ◽  
Yttrium Oxide ◽  
Zirconium Oxide ◽  
Raw Material ◽  
Bend Strength ◽  
Powder Metal ◽  
Zirconia Powder ◽  
Tetragonal Crystal ◽  
Powder Type

Abstract ZIRCAR ZIRCONIA POWDER TYPEZYP-4.5 is a highly reactive form of zirconium oxide stabilized in the tetragonal crystal state with added yttrium oxide. It is an excellent raw material for producing dense structural and wear resistant parts. This datasheet provides information on composition, physical properties, microstructure, hardness, elasticity, and bend strength as well as fracture toughness. It also includes information on powder metal forms. Filing Code: Cer-1. Producer or source: Zircar Products Inc..

Microstructural Considerations on the Reliability of 3D Packaging

2012 ◽  
Author(s):  
Zhiheng Huang ◽  
Zhiyong Wu ◽  
Hua Xiong ◽  
Yucheng Ma
Keyword(s):  
Mechanical Behavior ◽  
Grain Growth ◽  
Spinodal Decomposition ◽  
Elastic Energy ◽  
Modeling Approach ◽  
3D Packaging ◽  
Ultrafine Interconnects

Abstract Microstructure and its effect on mechanical behavior of ultrafine interconnects have been studied in this paper using a modeling approach. The microstructure from the processes of solidification, spinodal decomposition, and grain growth in ultrafine interconnects has highlighted its importance. The size, geometry and composition of interconnects as well as the elastic energy can influence microstructure and thus the mechanical behavior. Quantification of microstructure in ultrafine interconnects is a necessary step to establish the linkage between microstructure and reliability.

PREDICTION OF GRAIN GROWTH IN HYBRID WELDING HAZ OF TCS STAINLESS STEEL

2013 ◽  
Vol 48 (2) ◽  
pp. 199-204 ◽  
Author(s):  
Zhuanzhuan ZHANG ◽  
Chuansong WU ◽  
Jinqiang Gao
Keyword(s):  
Stainless Steel ◽  
Grain Growth ◽  
Hybrid Welding
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