Surface and Bulk Residual Stress in Ti6Al4V Welded Aerospace Tanks

2004 ◽  
Vol 126 (3) ◽  
pp. 284-292 ◽  
Author(s):  
G. Bruno ◽  
B. D. Dunn
Keyword(s):  
Heat Treatment ◽  
Residual Stress ◽  
Neutron Diffraction ◽  
Separate Determination ◽  
X Rays ◽  
X Ray Diffraction ◽  
Β Phase ◽  
Propellant Tank ◽  
Neutron Diffraction Technique

The residual stress (RS) in two curved plates cut from a large welded propellant tank for spacecrafts was investigated nondestructively by neutron and laboratory x-ray diffraction. Each plate had two weld beads symmetric to a central monoblock reinforcement. One plate had received a post-weld heat-treatment. The two nondestructive test techniques successfully determined both the bulk (thickness averaged) and the surface stress state, due to the highly different penetration of these radiations in metals. In the as-welded tank, both neutrons and x-rays show a stress level (both in the axial and hoop directions) higher in the heat affected zone (HAZ) than in the weld pool (300 against 160 MPa). A considerable degree of relaxation annealing was observed by neutron diffraction after the application of the heat treatment. In this case, the hoop stress in the HAZ relaxes from about 300 to about 100 MPa. X-rays also permitted the separate determination of the α and β-phase stresses and the calculation of the macro-RS. The latter showed the bending deformation resulting from the cut of the plates from the original tank. The average stress measured by x-rays was found to be very similar to the RS obtained by neutron diffraction technique.

Determination of the Residual Stress Field around Scratches Using Synchrotron X-Rays and Nanoindentation

2010 ◽  
Vol 652 ◽  
pp. 25-30
Author(s):  
M.K. Khan ◽  
Michael E. Fitzpatrick ◽  
L.E. Edwards ◽  
S.V. Hainsworth
Keyword(s):  
Residual Stress ◽  
Stress Field ◽  
Residual Stresses ◽  
Small Scale ◽  
X Rays ◽  
X Ray Diffraction ◽  
Residual Stress Field ◽  
Fine Grained ◽  
Load Displacement

The residual strain field around the scratches of 125µm depth and 5µm root radius have been measured from the Synchrotron X-ray diffraction. Scratches were produced using different tools in fine-grained aluminium alloy AA 5091. Residual stresses up to +1700 micro-strains were measured at the scratch tip for one tool but remained up to only +1000 micro-strains for the other tool scratch. The load-displacement curves obtained from nanoindentation were used to determine the residual stresses around the scratches. It was found that the load-displacement curves are sensitive to any local residual stress field present and behave according to the type of residual stresses. This combination of nanoindentation and synchrotron X-rays has been proved highly effective for the study of small-scale residual stresses around the features such as scratches.

scholarly journals Electronic Excitations and Radiation Damage in Macromolecular Crystallography

Crystals ◽  
2018 ◽  
Vol 8 (7) ◽  
pp. 273 ◽  
Author(s):  
José Brandão-Neto ◽  
Leonardo Bernasconi
Keyword(s):  
Chemical Information ◽  
X Rays ◽  
Electronic Excitations ◽  
Macromolecular Crystallography ◽  
X Ray Diffraction ◽  
X Ray ◽  
Atomic Structures ◽  
Successful Approach ◽  
Structural Research

Macromolecular crystallography at cryogenic temperatures has so far provided the majority of the experimental evidence that underpins the determination of the atomic structures of proteins and other biomolecular assemblies by means of single crystal X-ray diffraction experiments. One of the core limitations of the current methods is that crystal samples degrade as they are subject to X-rays, and two broad groups of effects are observed: global and specific damage. While the currently successful approach is to operate outside the range where global damage is observed, specific damage is not well understood and may lead to poor interpretation of the chemistry and biology of the system under study. In this work, we present a phenomenological model in which specific damage is understood as the result of a single process, the steady excitation of crystal electrons caused by X-ray absorption, which acts as a trigger for the bulk effects that manifest themselves in the form of global damage and obscure the interpretation of chemical information from XFEL and synchrotron structural research.

scholarly journals Residual Stress Evolution during Decomposition of Ti(1-x)Al(x)N Coatings Using High-Energy X-Rays

2006 ◽  
Vol 524-525 ◽  
pp. 619-624 ◽  
Author(s):  
Mark R. Terner ◽  
Peter Hedström ◽  
Jonathan Almer ◽  
J. Ilavsky ◽  
Magnus Odén
Keyword(s):  
Residual Stress ◽  
Phase Separation ◽  
Elevated Temperatures ◽  
High Energy ◽  
Film Plane ◽  
X Rays ◽  
X Ray Diffraction ◽  
Synchrotron Source ◽  
Simultaneous Acquisition ◽  
Initial Stage

Residual stresses and microstructural changes during phase separation in Ti33Al67N coatings were examined using microfocused high energy x-rays from a synchrotron source. The transmission geometry allowed simultaneous acquisition of x-ray diffraction data over 360° and revealed that the decomposition at elevated temperatures occurred anisotropically, initiating preferentially along the film plane. The as-deposited compressive residual stress in the film plane first relaxed with annealing, before dramatically increasing concurrently with the initial stage of phase separation where metastable, nm-scale c-AlN platelets precipitated along the film direction. These findings were further supported from SAXS analyses.

scholarly journals Synchrotron Nano-Diffraction Study of Thermally Treated Asbestos Tremolite from Val d’Ala, Turin (Italy)

Minerals ◽  
2018 ◽  
Vol 8 (8) ◽  
pp. 311 ◽  
Author(s):  
Carlotta Giacobbe ◽  
Jonathan Wright ◽  
Dario Di Giuseppe ◽  
Alessandro Zoboli ◽  
Mauro Zapparoli ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Heat Treatment ◽  
Risk Management ◽  
Structure Analysis ◽  
X Rays ◽  
X Ray Diffraction ◽  
X Ray ◽  
Adverse Health Effects ◽  
Nano Crystalline ◽  
Original Fibre

Nowadays, due to the adverse health effects associated with exposure to asbestos, its removal and thermal inertization has become one of the most promising ways for reducing waste risk management. Despite all the advances in structure analysis of fibers and characterization, some problems still remain that are very hard to solve. One challenge is the structure analysis of natural micro- and nano-crystalline samples, which do not form crystals large enough for single-crystal X-ray diffraction (SC-XRD), and their analysis is often hampered by reflection overlap and the coexistence of multiple fibres linked together. In this paper, we have used nano-focused synchrotron X-rays to refine the crystal structure of a micrometric tremolite fibres from Val d’Ala, Turin (Italy) after various heat treatment. The structure of the original fibre and after heating to 800 °C show minor differences, while the fibre that was heated at 1000 °C is recrystallized into pyroxene phases and cristobalite.

Design Optimisation of a Ferritic Ring Weld Specimen Using FE Modelling

2009 ◽  
Author(s):  
Christopher M. Gill ◽  
Paul Hurrell ◽  
John Francis ◽  
Mark Turski
Keyword(s):  
Heat Treatment ◽  
Residual Stress ◽  
Finite Element ◽  
Neutron Diffraction ◽  
Stress Field ◽  
Finite Element Modelling ◽  
Post Weld Heat Treatment ◽  
Stress Fields ◽  
Element Modelling ◽  
Weld Heat

This paper describes the design optimisation of an SA508 ferritic steel ring weld specimen using FE modelling techniques. The aim was to experimentally and analytically study the effect of post weld heat treatment upon a triaxial residual stress field. Welding highly constrained geometries, such as those found in some pressure vessel joints, can lead to the formation of highly triaxial stress fields. It is thought that application of post weld heat treatments will not fully relax hydrostatic stress fields. Therefore a ferritic multi-pass ring weld specimen was designed and optimised, using 2D finite element modelling, to generate a high magnitude triaxial stress field. The specimen thickness and weld-prep geometry was optimised to produce a large hydrostatic stress field and still allow efficient use of neutron diffraction to measure the residual stress. This paper reports the development of the test specimen geometry and compares the results of welding FE analysis and neutron diffraction measurements. Welding residual stresses were experimentally determined using neutron diffraction; both before post weld heat treatment. Three dimensional moving heat source weld finite element modelling has been used to predict the residual stresses generated by the welding process used. Finite element modelling examined the effect of phase transformation upon the residual stress field produced by welding. The relaxation of welding stresses by creep during post weld heat treatment has also been modelled. Comparisons between the modelled and measured as-welded residual stress profiles are presented. This work allows discussion of the effect of post weld heat treatment of triaxial stress fields and determines if finite element modelling is capable of correctly predicting the stress relaxation.

scholarly journals Electronic Excitations and Radiation Damage in Macromolecular Crystallography

2018 ◽  
Author(s):  
José Brandão-Neto ◽  
Leonardo Bernasconi
Keyword(s):  
Chemical Information ◽  
X Rays ◽  
Electronic Excitations ◽  
Macromolecular Crystallography ◽  
X Ray Diffraction ◽  
X Ray ◽  
Atomic Structures ◽  
Successful Approach ◽  
Structural Research

Macromolecular crystallography at cryogenic temperatures has so far provided the majority of the experimental evidence that underpins the determination of the atomic structures of proteins and other biomolecular assemblies by means of single crystal X-ray diffraction experiments. One of the core limitations of the current methods is that crystal samples degrade as they are subject to X-rays, and two broad groups of effects are observed: global and specific damage. While the currently successful approach is to operate outside the range where global damage is observed, specific damage is not well understood and may lead to poor interpretation of the chemistry and biology of the system under study. In this work, we present a phenomenological model in which specific damage is understood as the result of a single process, the steady excitation of crystal electrons caused by X-ray absorption, which acts as a trigger for the bulk effects that manifest themselves in the form of global damage and obscure the interpretation of chemical information from XFEL and synchrotron structural research.

X-Ray Diffraction Determination of Metallurgical Damage in Turbo Blower Rotor Shafts

1988 ◽  
Vol 142 ◽  
Author(s):  
John F. Porter ◽  
Dan O. Morehouse ◽  
Mike Brauss ◽  
Robert R. Hosbons ◽  
John H. Root ◽  
...  
Keyword(s):  
Residual Stress ◽  
Hole Drilling ◽  
X Ray Diffraction ◽  
X Ray ◽  
Turbo Blower ◽  
Diffraction Determination ◽  
Defence Research ◽  
Stress Profiles ◽  
Non Destructive

AbstractStudies have been ongoing at Defence Research Establishment Atlantic on the evaluation of non-destructive techniques for residual stress determination in structures. These techniques have included neutron diffraction, x-ray diffraction and blind-hole drilling. In conjunction with these studies, the applicability of these procedures to aid in metallurgical and failure analysis investigations has been explored. The x-ray diffraction technique was applied to investigate the failure mechanism in several bent turbo blower rotor shafts. All examinations had to be non-destructive in nature as the shafts were considered repairable. It was determined that residual stress profiles existed in the distorted shafts which strongly indicated the presence of martensitic microstuctures. These microstructures are considered unacceptable for these shafts due to the potential for cracking or in-service residual stress relaxation which could lead to future shaft distortion.

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