Correlation Between Steel Microstructural Characteristics and the Initiation and Arrest Toughness Determined From Small-Scale Mechanical Testing

Author(s):  
Jessica Taylor ◽  
Philippa Moore ◽  
Ali Mehmanparast ◽  
Rob Kulka

Abstract Modern high Charpy toughness steels can nonetheless show low crack arrest toughness[1]. In this paper, the relationship between initiation and arrest toughness is investigated in five different carbon steels, including S355 structural steels, X65 pipeline steel, and high strength reactor pressure vessel, RPV, steels. The results from small-scale mechanical tests, including instrumented Charpy, drop weight Pellini, fracture toughness, and tensile testing (including STRA in the through-thickness direction) were used to determine the behaviour of the different steels in terms of initiation fracture toughness and crack arrest toughness parameters. There was no correlation between the upper shelf initiation toughness and the arrest toughness when the results from the five steels were collated. The mechanical test results were then correlated to the steels’ microstructural characteristics, including parent metal microstructure, average grain size and grain aspect ratio to identify the relative roles of microstructure and texture in the fracture initiation and arrest performance of carbon steels.

Author(s):  
Marjorie EricksonKirk ◽  
Mark EricksonKirk ◽  
Tim Williams

Models to predict the fracture and arrest behavior of ferritic steels, particularly those in use in the nuclear industry, have long been under development. The current, most widely accepted model of fracture toughness behavior is the ASTM E1921-02 “Master Curve” that is used to predict the variation of the mean cleavage fracture toughness with temperature in the transition temperature region as well as predicting the scatter of data about the mean at any given temperature. Recently, models describing the variation of arrest fracture toughness and of ductile initiation toughness with temperature have also been proposed. A study has been conducted with the goal of assessing how the scatter in cleavage initiation toughness may vary with temperature and level of irradiation embrittlement, which utilizes the crack arrest and ductile crack initiation models to redefine limits of applicability of the Master Curve-assumed Weibull distribution by developing empirically-derived interrelationships between the three models. These relationships are expected as all three parameters, KIc, KIa, and JIc, are controlled by the flow behavior of the material. There is a physical basis for viewing the crack arrest toughness as an absolute lower bound to the distribution of crack initiation toughness values for a fixed material condition and temperature. This physically based relationship, borne of the fact that both cleavage crack initiation toughness and cleavage crack arrest toughness are controlled by dislocation mobility, has brought about the suggestion that crack arrest toughness could be used to modify the lower tails of the crack initiation fracture toughness distribution. Using both empirical evidence and a hardening model proposed by Natishan and Wagenhofer, we investigate the relationship between initiation and arrest toughness and the implications on use of toughness models.


2017 ◽  
Vol 27 (2) ◽  
pp. 210-215 ◽  
Author(s):  
Teppei Okawa ◽  
Hiroyuki Shirahata ◽  
Kiyotaka Nakashima ◽  
Kazuhisa Yanagita ◽  
Takehiro Inoue

1996 ◽  
Vol 118 (4) ◽  
pp. 292-299 ◽  
Author(s):  
L. Malik ◽  
L. N. Pussegoda ◽  
B. A. Graville ◽  
W. R. Tyson

The awareness of the presence of local brittle zones (LBZs) in the heat-affected zone (HAZ) of welds has led to the requirements for minimum initiation (CTOD) toughness for the HAZ for critical applications (API RP 2Z, CSA S473). Such an approach, however, is expensive to implement and limits the number of potential steel suppliers. A fracture control philosophy that is proposed to be an attractive alternative for heat-affected zones containing LBZs is the prevention of crack propagation rather than of crack initiation. Such an approach would be viable if it could be demonstrated that cracks initiated in the LBZs will be arrested without causing catastrophic failure, notwithstanding the low initiation (CTOD) toughness resulting from the presence of LBZs. Unstable propagation of a crack initiating from an LBZ requires the rupture of tougher microstructural regions surrounding the LBZ in HAZ, and therefore the CTOD value reflecting the presence of LBZ is unlikely to provide a true indication of the potential for fast fracture along the heat-affected zone. Base metal specifications (CSA S473) usually ensure that small unstable cracks propagating from the weld zone into the base metal would be arrested. Past work has also shown that unstable crack initiation resulting from interaction of surface semi-elliptical cracks parallel to the fusion boundary with the local brittle zones can get arrested once the crack has popped through the depth of the LBZ. However, the potential for arrest when a through-thickness HAZ crack runs parallel to the fusion boundary, and thus parallel to the LBZs, has not been examined previously. To investigate the likelihood of fast fracture within the HAZ, a test program has been carried out that involved performing compact plane strain (ASTM E1221) and plane stress crack arrest tests on a heataffected zone that contained LBZs, and thus exhibited unacceptable low CTOD toughness for resistance to brittle fracture initiation. The results indicated that in contrast to the initiation toughness (CTOD toughness), the crack arrest toughness was little influenced by the presence of local brittle zones. Instead, the superior toughness of the larger proportion of finer-grain HAZ surrounding the LBZ present along the crack path has a greater influence on the crack arrest toughness. It further seems that there may be potential to estimate the HAZ crack arrest toughness from more conventional smaller-scale laboratory tests, such as conventional or precracked instrumented Charpy impact tests.


Author(s):  
A. Wasylyk ◽  
A. H. Sherry ◽  
J. K. Sharples

Structural integrity assessments of structures containing defects require valid fracture toughness properties as defined in national and international test standards. However, for some materials and component geometries, the development of valid toughness values — particularly for ductile fracture — is difficult since sufficiently large specimens cannot be machined. As a consequence, the validity of fracture toughness properties is limited by the development of plasticity ahead of the crack tip and the deviation of crack tip conditions at failure from small scale yielding. This paper described the use of local approach models, calibrated against invalid test data, to define initiation toughness in 304 stainless steel pipe material. Three fracture toughness geometries were tested, shallow cracked single edge cracked specimens tested under three point bending, deep cracked single edge cracked specimens tested under three point bending, and deep cracked single edge cracked specimen tested under tension. Initiation toughness and J-Resistance curves were defined for each specimen using the multi-specimen technique. All initiation toughness values measured were above the specimen validity limits. The fracture conditions at initiation were analysed using three local approach models: the Generalised Rice & Tracey, High Constraint Rice & Tracey and the Work of Fracture. The adequacy of local approaches to define the fracture conditions under large strains in 304 stainless steels was demonstrated. A modified boundary layer analysis combined with the local approach models was used to predict the “valid” initiation toughness under small scale yielding condition in this material by defining a J-Q fracture locus. The analytically derived fracture locus was compared to the J-Q values obtained experimentally and shown to be consistent.


Author(s):  
Muhammad S. Ali

It is well established that sour operating environments can give rise to significantly reduced fracture toughness of pipelines made of carbon manganese steel. Fracture resistance of a material is usually defined in terms of a fracture resistance curve, commonly known as an R-curve which is determined by testing pre-cracked specimens under a rising load. Fracture resistance data can be derived by the single specimen method, where crack extension is determined using unloading compliance or the multiple specimen method, where crack extension is measured from the fracture face of each specimen and each specimen is taken to a different load level. The fracture resistance behaviour of API 5L X65 grade pipeline steel determined by testing single edge notched bend specimens in a specific sour environment using both single and multiple specimen test methods is reported. The fracture resistance of the steel was found to be highly sensitive to the loading rates (described by the initial rate of increase of stress intensity factor in the elastic range) applied during the fracture resistance tests. It was possible to identify a loading rate slow enough to provide fracture initiation toughness reasonably close to the expected lower bound toughness. It is possible to produce similar R-curves from single and multiple specimen testing methods (if conditions are otherwise the same). Under comparable loading rates and environmental conditions, side grooved specimens resulted in lower fracture toughness as compared to the toughness determined from the plane sided specimens. It was also noticed that there was a weaker correlation between side grooving and toughness at slower loading rates.


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