Use of the absolute method in neutron activation analysis: application to National Bureau of Standards coal and spinach

1982 ◽  
Vol 60 (17) ◽  
pp. 2278-2280 ◽  
Author(s):  
J. St-Pierre ◽  
L. Zikovsky

Absolute neutron activation analysis, which consists of gamma-ray counting and direct calculation of weights from nuclear constants, was applied to two National Bureau of Standards materials: coal (SRM 1632a) and spinach (SRM 1570). Al, As, Br, Cl, Co, Cr, Cs, Eu, Fe, Ga, K, La, Mg, Na, Sb, Sc, Sr, Ti, V, W, and Zn were instrumentally determined in these samples with accuracy ranging from −18 to +21% among elements for which reference values were available.




2011 ◽  
Vol 1 (1) ◽  
pp. 305-312
Author(s):  
R. B. Firestone ◽  
Zs. Révay

Abstract Independent databases of nuclear constants for Neutron Activation Analysis (NAA) have been independently maintained by the physics and chemistry communities for many year. They contain thermal neturon cross sections σ 0, standardization values k 0, and transition probabilities P γ . Chemistry databases tend to rely upon direct measurements of the nuclear constants k 0 and P γ which are often published in chemistry journals while the physics databases typically include evaluated σ 0 and P γ data from a variety of experiments published mainly in physics journals. The IAEA/LBNL Evaluated Gamma-ray Activation File (EGAF) also contains prompt and delayed γ-ray cross sections σ γ from Prompt Gamma-ray Activation Analysis (PGAA) measurements that can also be used to determine k 0 and σ 0 values. As a result several independent databases of fundamental constants for NAA have evolved containing slightly different and sometimes discrepant results. An IAEA CRP for a Reference Database for Neutron Activation Analysis was established to compare these databases and investigate the possibilitiy of producing a self-consistent set of σ 0, k 0, σ γ , and P γ values for NAA and other applications. Preliminary results of this IAEA CRP comparison are given in this paper.



2016 ◽  
Vol 5 (03) ◽  
pp. 4892 ◽  
Author(s):  
Ratna Raju M.* ◽  
Madhusudhana Rao P. V. ◽  
Seshi Reddy T. ◽  
Raju M. K. ◽  
Brahmaji Rao J. S. ◽  
...  

A study was undertaken to evaluate the inorganic elements for humans in two Indian medicinal plants leaves, namely Sphaeranthus indicus, and Cassia fistula by Instrumental Neutron Activation Analysis (INAA). INAA experiment was performed by using 20 kW KAMINI Reactor at Indira Gandhi Centre for Atomic Research (IGCAR), Kalpakkam. The emitted gamma rays were measured using gamma ray spectrometer. The concentrations of Al, Br, Ca, Fe, K, La, Mg, Mn, Na, Sc, V and Zn were determined in the selected medicinal plants. The medicinal leaves are using in treatment of various important ailments. The elemental content in selected medicinal leaves is various proportions depending on the soil composition, location of plant specimen and the climate in which the plant grows.



2012 ◽  
Vol 84 (2) ◽  
pp. 237-244 ◽  
Author(s):  
Diego R.G. Tudela ◽  
Sonia H. Tatumi ◽  
Márcio Yee ◽  
Silvio L.M. Brito ◽  
José L. Morais ◽  
...  

This paper presents the results of TL and OSL dating of soil and fragments of bricks from a grave, which was occupied by two mummified nuns, found at "Luz" Monastery, located in the state of São Paulo, Brazil. The TL and OSL ages were compared to C-14 dating ones obtained from bone collagens of the mummies. The majority of the ages is related to the eighteenth century. The gamma-ray spectroscopy was used to evaluate natural radioisotope concentrations in the samples, and by using these concentrations the annual dose rates, from 3.0 to 5.3 Gy/kyr, were obtained. Neutron activation analysis was performed and the radioisotope contents results are in agreement with those obtained by gamma-ray spectroscopy. The contents of U, Th and Ce elements were higher than those found in usual sediments.



1984 ◽  
Vol 30 (10) ◽  
pp. 1700-1703 ◽  
Author(s):  
M Simonoff ◽  
Y Llabador ◽  
A M Peers ◽  
G N Simonoff

Abstract Vanadium concentrations have been measured in the serum of 23 healthy subjects by neutron activation analysis, with post-irradiation chemical separation. The values obtained fall in a fairly narrow range (260-1300 ng/L, mean 670 ng/L), which suggests a physiological role for this element. We checked the method by analysis of standard (U.S. National Bureau of Standards) water samples and serum samples supplemented with 48V, and we found excellent agreement with expected results in both cases. We consider the reported results for human serum to be more reliable than those obtained by atomic absorption spectroscopy.



Sign in / Sign up

Export Citation Format

Share Document