PREPARATION OF TIN OXIDE NANOPARTICLES BY LASER ABLATION IN SOLUTION

2006 ◽  
Vol 05 (02n03) ◽  
pp. 259-264 ◽  
Author(s):  
MEI LI ◽  
QINGHUA LU ◽  
ZONGGUANG WANG

Tin oxide nanoparticles with a narrow size distribution were prepared by pulsed laser ablation of a pure tin target both in aqueous solutions and in pure water. Laser beam of 266 nm, 355 nm and 532 nm from an Nd :YAG laser were applied and the wavelength effects on preparation of tin oxide particles were examined. The particle size and phase structure were characterized by using transmission electron microscope (TEM). The observation revealed that the particle size of the nanoparticles was about 2–5 nm. Chemical components of obtained nanoparticles were analyzed by using an energy dispersive X-ray analysis (EDX) and the results demonstrated that the nanoparticles mainly consisted of Sn and O elements. Furthermore, aqueous solutions of sodium dodecyl sulfate (SDS) were used to study the influence of surfactant concentration on the formation of tin oxide nanoparticles. When the surfactant reached critical micelle concentration, relatively stable colloidal suspensions consisting of well-dispersed tin oxide nanoparticles were obtained. UV-vis spectrometer was used to measure the absorption of suspensions of tin oxide nanoparticles.

2018 ◽  
Vol 4 (5) ◽  
pp. 564-566
Author(s):  
I. Merlin ◽  
C. Vedhi ◽  
K. Muthu ◽  
A. Syed Mohamed

A systematic study on the preparation of tin oxide nanoparticles using the precipitation method has been conducted. The preparation of nanomaterials was by varying reaction parameters such as pH and temperature. The tin oxide nanoparticles were characterized by using AFM, SEM, XRD and UV-Vis. Particle size was obtained using XRD studies the value is 28.8 nm, 35.2 nm, 30.8 nm and 33.8 nm. It was found that the alteration of pH and temperature changes the particle size.


Silicon ◽  
2020 ◽  
Author(s):  
Raid A. Ismail ◽  
Sule Erten-Ela ◽  
Abdulrahman K. Ali ◽  
Cagdas Yavuz ◽  
Khaleel I. Hassoon

2021 ◽  
Vol 68 ◽  
pp. 114-122
Author(s):  
Ana Qona’ah ◽  
Iis Nurhasanah ◽  
Ali Khumaeni

Tin oxide nanoparticles (SnNPs) are very useful to be employed as an antibacterial agent for both gram-positive and gram-negative bacteria. In this present work, the synthesis of SnNPs was successfully carried out using the neodymium yttrium aluminum garnet (Nd:YAG) laser with a wavelength of 1064 nm, pulse duration of 7 ns, and a laser frequency of 10 Hz. Experimentally, a pulse Nd:YAG laser was directed and focused on a high-purity tin (Sn) metal, immersed in various liquid media including pure water and ethylene glycol. A brownish colloidal colour was produced both in pure water and ethylene glycol liquid media. Characterizations of tin oxide nanoparticles were made using UV-Vis, EDX, FTIR, and TEM. UV-Vis characterization produced absorbance values in pure water and ethylene glycol media of 1.314 a.u. and 1.119 a.u., respectively. TEM images show that the shape of tin oxide nanoparticles produced is spherical. Measurement of nanoparticle size distribution was made using image-J software and the average diameter of nano-size in the ethylene glycol medium is 12.55 nm, which is smaller than the size in the pure water of 19.98 nm. The EDX spectrum analysis results show that there are only Sn and O atoms in colloidal tin oxide nanoparticles (SnNPs). FTIR results show the formation of tin oxide (SnO2) spectrum at the wavenumber of 629.03 cm-1. The produced colloidal SnNPs were then applied as an antibacterial agent of E. coli using the disk diffusion method. Results certified that various concentrations of SnNPs of 10 ppm, 20 ppm, and 30 ppm gain the diameter of inhibition zone (DIZ) in sequence 6.50 mm, 6.75 mm, and 9.50 mm. Based on these experimental results, it shows that the higher the concentration of SnNPs given, the greater the ability to degrade and inhibit bacteria.


RSC Advances ◽  
2015 ◽  
Vol 5 (102) ◽  
pp. 84321-84327 ◽  
Author(s):  
Andrzej P. Nowak ◽  
A. Lisowska-Oleksiak ◽  
K. Siuzdak ◽  
M. Sawczak ◽  
M. Gazda ◽  
...  

This report concerns carbonaceous electrodes doped with tin(ii) oxide nanoparticles.


Author(s):  
Ivan Merino-Garcia ◽  
Lionel Tinat ◽  
Jonathan Albo ◽  
Manuel Alvarez-Guerra ◽  
Angel Irabien ◽  
...  

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