scholarly journals EDXRF study of Tupi-Guarani archaeological ceramics.

2003 ◽  
pp. 199 ◽  
Author(s):  
Fernando R. Espinoza Quiñones ◽  
Carlos R. Appoloni ◽  
Adenilson O. dos Santos ◽  
Luzeli M. da Silva ◽  
Paulo F. Barbieri ◽  
...  
Keyword(s):  
Compositional Data ◽  
Physical Characteristics ◽  
Intensity Data ◽  
Archaeological Ceramics ◽  
X Ray ◽  
Xrf Analysis ◽  
The North ◽  
Ceramic Paste ◽  
Representation Method ◽  
Non Destructive

A set of indian Brazilian pottery fragments belonging to Tupi-Guarani tradition has been studied by an archaeometric non-destructive technique. The pottery fragments were accidentally discovered in the Santa Dalmacia farm, sited near Cambé city at the north of Paraná Brazilian state. Each one of these fragments came from different ceramic recipients and their physical characteristics are very similar. The EDXRF measurements were performed employing both an X-ray tube and three radioisotope sources (Fe, Cd and Pu). The compositional data of the ceramics paste and pigments is investigated. For detection of the elements within the ceramic paste, the fragments were irradiated at the center of the lateral section, while several superficial areas with remaining plastic decoration were also chosen and irradiated at the convex and concave sides of each fragment. A paste-subtracted compositional data of the remaining pigments was statically extracted from the XRF analysis of each area. A program based on the graphic polygonal representation method was developed and used to correlate the representative intensity data of each fragment.

scholarly journals The metal artefacts from the prehistoric walled enclosure of Castelo Velho de Freixo de Numão within the early metallurgy of north-west of Iberian Peninsula

2019 ◽  
pp. 305-328
Author(s):  
Carlo Bottaini ◽  
Ignacio Montero-Ruiz ◽  
Susana Lopes ◽  
Lídia Baptista ◽  
Sérgio Gomes ◽  
...  
Keyword(s):  
Iberian Peninsula ◽  
Analytical Study ◽  
Pure Copper ◽  
X Ray ◽  
North West ◽  
The North ◽  
Metal Artefacts ◽  
Non Destructive ◽  
Arsenical Copper ◽  
North Western

This paper deals with the preliminary results of the typological and analytical study of a collection of copper-based objects found at the site of Castelo Velho (Freixo de Numão). This collection is associated to different contexts from the 3rd millennium BC (Chalcolithic). The analyses, performed by non-destructive X-ray fluorescence (XRF), show that the metals were produced with almost pure copper and arsenical copper (> 2% As). Impurities, such as As (<2%), Fe, Bi, Ag, Sn, Sb and Ni, were also identified, likely due to their presence in the ores used for the production of the objects. The data suggest that the metals from Castelo Velho may be framed within the metallurgical production already known for the Chalcolithic of the North-Western Iberian Peninsula.

Sensitivity, Precision, and Accuracy: Their Roles in Ceramic Compositional Data Bases

1990 ◽  
Vol 55 (3) ◽  
pp. 537-546 ◽  
Author(s):  
Ronald L. Bishop ◽  
Veletta Canouts ◽  
Patricia L. Crown ◽  
Suzanne P. de Atley
Keyword(s):  
Neutron Activation Analysis ◽  
Compositional Data ◽  
Analytical Sensitivity ◽  
Geological Environment ◽  
Data Bases ◽  
Archaeological Ceramics ◽  
X Ray ◽  
Commercial Laboratory ◽  
Characterization Studies ◽  
Precision And Accuracy

Differences in analytical sensitivity, precision, and accuracy exist among techniques and laboratories involved in the chemical analysis of archaeological ceramics. Large differences in these analytical parameters become significant in the formulation of data bases where comparability of the data is being sought. Small differences become significant when comparing pottery produced from clay resources located within a discrete geological environment. To better assess and report on the analytical results being obtained from laboratories, neutron-activation analysis and X-ray fluorescence are discussed relative to the level of precision required for ceramic characterization studies, the use of standards, and the preparation and submission of samples for commercial laboratory analysis.

XRD AND XRF ANALYSIS OF THE ANCIENT BRICKS FROM CANDI KAMPUNG BARU, KEDAH

2018 ◽  
Vol 16 ◽  
Author(s):  
Zuliskandar Ramli ◽  
Muhammad Nu'man Mohd Nasir ◽  
Abdul Latif Samian ◽  
Nor Zalina Harun ◽  
Mohd Shamsul Bahari Abdul Hadi ◽  
...  
Keyword(s):  
Raw Materials ◽  
Construction Material ◽  
Xrd Analysis ◽  
Major And Trace Elements ◽  
X Ray Diffraction ◽  
X Ray ◽  
Xrf Analysis ◽  
The North ◽  
The Many ◽  
The Temple

XRD and XRF analysis on the ancient bricks were conducted to identify whether the raw materials to produce the bricks originate from the site. Candi Kampung Baru is recorded as one of the temple that used bricks as the main construction material. This site is suggested to be built between the 8th to 10th centuries AD based on the size of the bricks and imported ceramics associated with the structure. The position of this candi that is facing to the north is a major indication that the candi in Kampung Baru Site is one of the many Buddhist candis that have been found in Bujang Valley. This study used X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) analysis techniques to identify the composition of the major and trace elements and minerals found in the bricks. The results of the analysis on the ancient brick of Candi Kampung Baru revealed that the mineral content contained in the brick samples consists of quartz, muscovite, microcline and sanidine. Minerals found suggest that open burning technique was used during the brick making process with the local raw clay sources were used to produce the bricks. The results therefore implied that the participation of the local communities in Old Kedah Kingdom contributed to the prosperity of this region.

scholarly journals XRD AND XRF ANALYSIS OF THE ANCIENT BRICKS FROM CANDI KAMPUNG BARU, KEDAH

2018 ◽  
Vol 16 (5) ◽  
Author(s):  
Zuliskandar Ramli ◽  
Muhammad Nu'man Mohd Nasir ◽  
Abdul Latif Samian ◽  
Nor Zalina Harun ◽  
Mohd Shamsul Bahari Abdul Hadi ◽  
...  
Keyword(s):  
Raw Materials ◽  
Construction Material ◽  
Xrd Analysis ◽  
Major And Trace Elements ◽  
X Ray Diffraction ◽  
X Ray ◽  
Xrf Analysis ◽  
The North ◽  
The Many ◽  
The Temple

XRD and XRF analysis on the ancient bricks were conducted to identify whether the raw materials to produce the bricks originate from the site. Candi Kampung Baru is recorded as one of the temple that used bricks as the main construction material. This site is suggested to be built between the 8th to 10th centuries AD based on the size of the bricks and imported ceramics associated with the structure. The position of this candi that is facing to the north is a major indication that the candi in Kampung Baru Site is one of the many Buddhist candis that have been found in Bujang Valley. This study used X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) analysis techniques to identify the composition of the major and trace elements and minerals found in the bricks. The results of the analysis on the ancient brick of Candi Kampung Baru revealed that the mineral content contained in the brick samples consists of quartz, muscovite, microcline and sanidine. Minerals found suggest that open burning technique was used during the brick making process with the local raw clay sources were used to produce the bricks. The results therefore implied that the participation of the local communities in Old Kedah Kingdom contributed to the prosperity of this region.

Handheld XRF and Raman equipment for the in situ investigation of Roman finds in the Villa dei Quintili (Rome, Italy)

2017 ◽  
Vol 32 (1) ◽  
pp. 117-129 ◽  
Author(s):  
R. Alberti ◽  
V. Crupi ◽  
R. Frontoni ◽  
G. Galli ◽  
M. F. La Russa ◽  
...  
Keyword(s):  
Cultural Heritage ◽  
X Ray ◽  
Xrf Analysis ◽  
In Situ Investigation ◽  
Non Destructive ◽  
Handheld Xrf

A variety of fragments of frescoes coming from the Villa dei Quintili in Rome and dating back to the II century A.D. were subjected to, first of all, an X-ray fluorescence (XRF) analysis by optimizing a portable spectrometer for non-destructive investigation in the field of cultural heritage.

scholarly journals Investigation of the Internal Structure and Gold-thin Layer of the Gilt-bronze Seated Avalokitesvara Bodhisattva at Anseong Cheonryong Temple through the Non-destructive Analysis

2021 ◽  
Vol 37 (6) ◽  
pp. 670-678
Author(s):  
Jung Eun Choi ◽  
Hak Choi
Keyword(s):  
Thin Layer ◽  
Gold Foil ◽  
Visual Observation ◽  
X Ray ◽  
Xrf Analysis ◽  
Peak Intensity ◽  
Korean Buddhism ◽  
Destructive Analysis ◽  
Γ Ray ◽  
Non Destructive

Anseong Cheonryongsa, a temple located in Anseong Seoun Mountain, is a part of the second Jogye Order of Korean Buddhism, under the Yongju Temple, and enshrines a gilt-bronze seated Avalokitesvara Bodhisattva. In this study, X-ray fluorescence (XRF) analysis revealed that this statue is composed of Cu-27.2 wt%, Sn-12.6 wt% and Pb-48 wt%. A gamma (γ) ray (Ir-192) image confirmed damage on the backside of the statue, which was later repaired with wood. The XRF analysis and visual observation determined the boundary between the metal and wood in the statue. In addition, results of standard X-ray peak intensity of gold foil and correlation with thickness helped to derive an equation for calculating the thickness of the Avalokitesvara Bodhisattva’s gold foil. It was determined that the gilded chest (21 µm) and face (20.7 µm) of the statue were the thickest sections, the wooden substratum (11.9 µm) was the next-most thick, and the bronze (7.4 µm) was the thinnest layer.

scholarly journals Dolomitic marble from Thasos at the Louvre

2013 ◽  
Vol 1 (1) ◽  
pp. 14 ◽  
Author(s):  
Thomas Calligaro ◽  
Yvan Coquinot ◽  
Maria Filomena Guerra ◽  
John J. Herrmann ◽  
Ludovic Laugier ◽  
...  
Keyword(s):  
Coarse Grained ◽  
Dolomitic Marble ◽  
X Ray ◽  
Aegean Island ◽  
The North ◽  
New Information ◽  
North Aegean ◽  
Non Destructive

Many Greek and Roman sculptures in the Louvre appear to be made of coarse-grained, very white dolomitic marble from the north Aegean island of Thasos, and permission was given to test twelve of them in a non-destructive way using a mobile X-ray fluorescence (XRF) spectrometer. Coarse-grained, white dolomitic marble sources were rare in antiquity, and if these Thasian-looking sculptures proved to be dolomitic rather than calcitic, it is highly likely that they were in fact made of Thasian marble. Ten of the twelve sculptures did prove to be dolomitic marble and therefore very probably Thasian in origin. This new information makes it possible to expand and enrich our knowledge of the exportation of marble from Thasos in both geographic and chronological terms. The tests furthermore confirm that dolomitic marble from Thasos was preferred for colossal replicas of Athena of the Velletri type and also reveal that a group of imperial portraits in Algeria were carved from marble blocks from Thasos. One test offered confirmation that a fragment in the Louvre was part of a relief in Izmir.

Highlights in the history of X-ray topography1

1995 ◽  
Vol 210 (6) ◽  
Author(s):  
A. R. Lang
Keyword(s):  
Magnetic Domain ◽  
Diffraction Theory ◽  
Dislocation Loops ◽  
X Ray Diffraction ◽  
X Ray ◽  
Domain Structures ◽  
Structure Factors ◽  
History Of ◽  
Dislocation Sources ◽  
Non Destructive

AbstractX-ray topography provides a non-destructive method of mapping point-by-point variations in orientation and reflecting power within crystals. The discovery, made by several workers independently, that in nearly perfect crystals it was possible to detect individual dislocations by X-ray diffraction contrast started an epoch of rapid exploitation of X-ray topography as a new, general method for assessing crystal perfection. Another discovery, that of X-ray Pendellösung, led to important theoretical developments in X-ray diffraction theory and to a new and precise method for measuring structure factors on an absolute scale. Other highlights picked out for mention are studies of Frank-Read dislocation sources, the discovery of long dislocation helices and lines of coaxial dislocation loops in aluminium, of internal magnetic domain structures in Fe-3 wt.% Si, and of stacking faults in silicon and natural diamonds.

Stoichiometric Determination of Graphite Intercalation Compounds Using Rutherford Backscatiering Spectrometry

1983 ◽  
Vol 27 ◽  
Author(s):  
L. Salamanca-Riba ◽  
B.S. Elman ◽  
M.S. Dresselhaus ◽  
T. Venkatesan
Keyword(s):  
Experimental Error ◽  
Rutherford Backscattering Spectrometry ◽  
Rutherford Backscattering ◽  
Intercalation Compounds ◽  
Graphite Intercalation Compounds ◽  
X Ray ◽  
Donor And Acceptor ◽  
Graphite Intercalation ◽  
Non Destructive

ABSTRACTRutherford backscattering spectrometry (RBS) is used to characterize the stoichiometry of graphite intercalation compounds (GIC). Specific application is made to several stages of different donor and acceptor compounds and to commensurate and incommensurate intercalants. A deviation from the theoretical stoichiometry is measured for most of the compounds using this non-destructive method. Within experimental error, the RBS results agree with those obtained from analysis of the (00ℓ) x-ray diffractograms and weight uptake measurements on the same samples.

X-Ray Tomography for Electronic Packages

2000 ◽  
Author(s):  
Deepak Goyal
Keyword(s):  
3D Imaging ◽  
Development Time ◽  
Analytical Techniques ◽  
Electronic Packages ◽  
X Ray ◽  
Imaging Capability ◽  
Imaging Results ◽  
Key Drivers ◽  
Analytical Tools ◽  
Non Destructive

Abstract Next generation assembly/package development challenges are primarily increased interconnect complexity and density with ever shorter development time. The results of this trend present some distinct challenges for the analytical tools/techniques to support this technical roadmap. The key challenge in the analytical tools/techniques is the development of non-destructive imaging for improved time to information. This paper will present the key drivers for the non-destructive imaging, results of literature search and evaluation of key analytical techniques currently available. Based on these studies requirements of a 3D imaging capability will be discussed. Critical breakthroughs required for development of such a capability are also summarized.

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