Fracture Resistance Testing of Monolithic and Composite Brittle Materials

2014 ◽  
Vol 2 (1) ◽  
pp. 13
Author(s):  
Francisco Carlos Bontorim ◽  
Milton Carlos Kuga ◽  
Sabrina Spinelli Cioffi ◽  
Marcus Vinicius Reis Só ◽  
Gisele Faria ◽  
...  

PURPOSE: This study evaluated the effect of 10% sodium ascorbate (10SA), in gel (10SAg) or aqueous solution (10SAs) formulations, on fracture resistance of endodontically treated tooth submitted to dental bleaching procedures with 15% hydrogen peroxide associated with titanium dioxide (15HP-TiO2) nanoparticles and photoactivated by LED-laser. MATERIAL AND METHODS: Forty maxillary premolars were endodontically-treated and embedded in acrylic resin up to the cement-enamel junction. The specimens were divided into four groups (n=10): G1 (negative control): no bleaching, coronal access restored with composite resin; G2 (positive control): three dental bleaching  sessions using 15HP-TiO2 and LED-laser photoactivation and restored with composite resin (positive control); G3 (10SAg): similar procedures to G2, but applied  10SA, in gel formulation, for 24 hours before restoration; G4 (10SAs): similar procedures to G3, but applied  10SA, in aqueous solution formulation.  The 15HP-TiO2 was applied on buccal and lingual surfaces of the crown tooth and inside the pulp chamber and photoactivated by LED-laser. Between each bleaching session, the teeth were maintained in artificial saliva, at 37oC, for 7 days. In sequence, the teeth were submitted to fracture resistance testing using an eletromechanical machine test. The data was analyzed using Kruskal Wallis test (p = 0.05) RESULTS: There are no differences significant among the groups in relation to fracture resistance of endodontically treated teeth (p>0.05). CONCLUSIONS: The use of 10% sodium ascorbate, in gel or aqueous solution formulations, did not interfered on the fracture resistance teeth after dental bleaching using 15HP-TiO2 and LED-laser photoactivation.


2020 ◽  
Vol 121 (13) ◽  
pp. 2929-2945 ◽  
Author(s):  
Chi Wu ◽  
Jianguang Fang ◽  
Shiwei Zhou ◽  
Zhongpu Zhang ◽  
Guangyong Sun ◽  
...  

2021 ◽  
Vol 24 (3) ◽  
Author(s):  
Amr El-Etreby ◽  
Mahmoud Metwally ◽  
Gihan EL-Nagar

Objective: The recycling of heat pressed lithium disilicate glass-ceramic leftover material has been reported to be done by dental laboratories. The effect of this procedure on the fracture resistance of single crowns is unknown, especially when it is functioning inside the oral cavity with subsequent exposure to temperature changes and cycles of mastication. Material and Methods: A total of 28 lithium disilicate glass-ceramic crowns (IPS emax Press) were constructed and randomly assigned into two groups (n = 14); Group (P): Included crowns fabricated from new e.max ingots. Group (R): Included crowns fabricated from repressed e.max buttons. Specimens of each group were divided into two equal subgroups (n = 7) according to whether the aging of specimens will be performed or not before fracture resistance testing. Subgroup (N), samples were subjected to fracture resistance without thermo-mechanical aging, while subgroup (A), samples were subjected to thermo-cycling and cyclic loading before being subjected to fracture strength testing. Different methods; SEM, XRD, EDAX were used to characterize the properties of lithium disilicate glass-ceramics before and after repressing. Results: The highest statistically significant fracture resistance value was recorded for the subgroup (RN) repressed/non-aged, followed by the subgroup repressed/aged (RA), while the lowest statistically significant mean value was recorded for the subgroup pressed/aged (PA). There was no significant difference between pressed/non-aged (PN) and repressed/aged (RA) subgroups. Conclusion: Repressing of leftover buttons may increase the fracture resistance of IPS emax Press crowns. Thermo-mechanical aging may negatively affect the fracture resistance of IPS emax Press crowns, yet Repressing may decrease this effect. Clinical implications: This is a novel approach that targets a point of research that has not been investigated before. It elaborates how repressing may decrease the effect of aging and increase the fracture resistance of lithium disilicate crowns. Thus, recycling of lithium disilicate glass ceramics might decrease its failure and prolong their serviceability.   Keywords Fracture resistance; Heat pressed; Lithium disilicate; Recycling; Repressing; Thermo-mechanical aging.


2018 ◽  
Vol 115 (50) ◽  
pp. 12698-12703 ◽  
Author(s):  
Madeleine Grossman ◽  
Florian Bouville ◽  
Kunal Masania ◽  
André R. Studart

The nacreous layer of mollusk shells holds design concepts that can effectively enhance the fracture resistance of lightweight brittle materials. Mineral bridges are known to increase the fracture resistance of nacre-inspired materials, but their role is difficult to quantify due to the lack of experimental systems where only this parameter is controllably varied. In this study, we fabricate tunable nacre-like composites that are used as a model to experimentally quantify the influence of the density of mineral bridges alone on the fracture properties of nacre-like architectures. The composites exhibit a brick-and-mortar architecture comprising highly aligned alumina platelets that are interconnected by titania mineral bridges and infiltrated by an epoxy organic phase. By combining experimental mechanical data with image analysis of such composite microstructures, an analytical model is put forward based on a simple balance of forces acting on an individual bridged platelet. Based on this model, we predict the flexural strength of the nacre-like composite to scale linearly with the density of mineral bridges, as long as the mineral interconnectivity is low enough to keep fracture in a platelet pullout mode. Increasing the mineral interconnectivity beyond this limit leads to platelet fracture and catastrophic failure of the composite. This structure-property correlation provides powerful quantitative guidelines for the design of lightweight brittle materials with enhanced fracture resistance. We illustrate this potential by fabricating nacre-like bulk composites with unparalleled flexural strength combined with noncatastrophic failure.


2014 ◽  
Vol 633 ◽  
pp. 286-289
Author(s):  
Li Xian Zhang ◽  
Yu Xiao Liu ◽  
Ya Li Liu ◽  
Qiong Rong

Objective: To evaluate the fracture resistance of endodontically treated teeth reinforced with cast titanium posts and prefabricated glass-fiber posts with different diameters. Materials and Methods: 50 recently extracted human maxillary central incisors were endodontically treated and randomly divided into 5 groups of 10 specimens each: Group A: 1.35mm diameter of cast titanium post; Group B: 1.5mm diameter of cast titanium post; Group C: 1.375mm diameter of prefabricated fiber post; Group D: 1.5mm diameter of prefabricated fiber post; Group E: resin restoration. All specimens were subjected to fracture resistance testing in a universal testing machine, statistical analysis was performed and the fracture modes were analyzed. Results: The mean fracture resistance of five groups as follows: 404.22±73.92N for group A, 488.17±78.68N for group B, 280.32±45.23N for group C, 317.53±50.87N for group D, 222.76±38.67N for group E. The fracture resistance of restored teeth between group C and group D had no significant difference (P>0.05). The fracture resistance of the rest pairwise group comparisons had significant difference (P<0.05). Most of cast post samples fractured at the root middle or apical portion, while most of the fiber post samples fractured at the root cervical or post fracture, which could be retreated. Conclusion: Human maxillary central incisors restored with cast posts could bear higher fracture load and fiber post could protect the root from fracture preferably.


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