Impression creep behavior of SiC particle-MoSi2 composites

1996 ◽  
Vol 11 (6) ◽  
pp. 1528-1536 ◽  
Author(s):  
Darryl P. Butt ◽  
David A. Korzekwa ◽  
Stuart A. Maloy ◽  
H. Kung ◽  
John J. Petrovic

Using a cylindrical indenter (or punch), the impression creep behavior of MoSi2-SiC composites containing 0–40% SiC by volume, was characterized at 1000–1200 °C, 258–362 MPa punch pressure. Through finite element modeling, an equation that depends on the material stress exponent was derived that converts the stress distribution beneath the punch to an effective compressive stress. Using this relationship, direct comparisons were made between impression and compressive creep studies. Under certain conditions, compressive creep and impression creep measurements yield comparable results after correcting for effective stresses and strain rates beneath the punch. However, rate-controlling mechanisms may be quite different under the two stressing conditions, in which case impression creep data should not be used to predict compressive creep behavior. The addition of SiC affects the impression creep behavior of MoSi2 in a complex manner by pinning grain boundaries during pressing, thus leading to smaller MoSi2 grains and by obstructing or altering both dislocation motion and grain boundary sliding.

1993 ◽  
Vol 322 ◽  
Author(s):  
Darryl P. Butt ◽  
Stuart A. Maloy ◽  
H. Kung ◽  
David A. Korzekwa ◽  
John J. Petrovic

AbstractUsing a cylindrical indenter, the indentation creep behavior of hot pressed and HIPed MoSi2-SiC composites containing 0-40% SiC by volume, was characterized at 1000-1200°C, 258-362 MPa. The addition of SiC affects the creep behavior of MoSi2 in a complex manner by pinning grain boundaries during pressing, thus leading to smaller MoSi2 grains; by obstructing or altering both dislocation motion and grain boundary sliding; and by increasing the overall yield stress of the material. Comparisons are made between indentation and compressive creep studies. It is shown that under certain conditions, compressive creep and indentation creep measurements yield comparable results after correcting for effective stresses and strain rates beneath the indenter.


Author(s):  
K.J. Hollis ◽  
D.P. Butt ◽  
R.G. Castro

Abstract The use of MoSi2 as a high temperature oxidation resistant structural material is hindered by its poor elevated temperature creep resistance. The addition of second phase Si3N4 holds promise for improving the creep properties of MoSi2 without decreasing oxidation resistance. The high temperature impression creep behavior of atmospheric plasma sprayed (APS) and hot pressed (HP) MoSi2/Si3N4 composites was investigated. Values for steady state creep rates, creep activation energies, and creep stress exponents were measured. Grain boundary sliding and splat sliding were found to be the dominant creep mechanisms for the APS samples while grain boundary sliding and plastic deformation were found to be the dominant creep mechanisms for the HP samples.


2014 ◽  
Vol 97 (9) ◽  
pp. 2957-2964 ◽  
Author(s):  
Manab Mallik ◽  
Kalyan Kumar Ray ◽  
Rahul Mitra

2012 ◽  
Vol 190-191 ◽  
pp. 431-434
Author(s):  
Dao Fen Xu ◽  
Chun Ping Du ◽  
Dong Ye

The compressive creep behavior of Mg-4Al-1RE-1Ca-0.2Sr (AECJ411002) alloy was investigated at temperatures in the range of 125~175°C and different compressive stress in the range of 88~112MPa with special apparatus. The results show that the creep deformation increases with the increasing of temperature and compressive stress. There is linear logarithmic relationship between the steady creep rate and all the temperature and stress used. The steady creep rate obeys an empirical equation. The stress exponents are similar at different temperatures and the appearance activation energies are not greatly different under different stresses. Their average value is respectively 6.19 and 39.05kJ/mol. Material constant A is 4.18×10-14. The steady creep rate is controlled by a dislocation climb led by grain boundary sliding. The creep resistance enhances because of the heat-resistant phases Al2Ca and Al4Sr distributing at grain boundary.


2015 ◽  
Vol 752-753 ◽  
pp. 189-193 ◽  
Author(s):  
Serkan Abali

In the present work, compressive creep characteristics of directionally solidified MAS-YAG (MgAl2O4/Y3Al5O12) were investigated at high temperature. The compressive creep strength of a crystal grown at a rate of 5 mm/min and a flow rate of 1.2 mm/min at 1500 °C under a strain rate of 1.0 × 10-4 was only 400 MPa, which is slightly higher than that of crystals grown under different conditions. The compressive creep strength of an oxide eutectic fabricated by the directional solidification method is higher than that of a polycrystalline sintered eutectic with the same composition. The creep behavior at high temperature was studied and the mechanisms of deformation by dislocation motion were revealed by Transmission Electron Microscopy (TEM) observations.


2004 ◽  
Vol 39 ◽  
pp. 397-401 ◽  
Author(s):  
Min Song ◽  
David M. Cole ◽  
Ian Baker

AbstractExperimental observations of the influence of particles at grain boundaries on the anelasticity and creep behavior of granular fresh-water ice are presented. Ice with particle contents of 0–4 wt.% was investigated under both reversed direct-stress and creep loading conditions at –12˚C. The results show that the particles decreased the grain-boundary relaxation by suppressing grain-boundary sliding at higher frequencies (10–1 to 101 Hz). In addition, the modulus increased by up to 30%, and the internal friction decreased by up to 30% at a frequency of 1 Hz. Staged creep tests showed that the particles affected the creep rate substantially. The minimum creep rate of ice containing 1 wt.% particles is 40% higher than that of particle-free ice, indicating that mechanisms besides dislocation glide aid the creep deformation.


2014 ◽  
Vol 703 ◽  
pp. 363-369
Author(s):  
Jian Qiang Zhang ◽  
Yan Jun Zheng ◽  
Li Wang ◽  
Shao Wei Li ◽  
Jing Xu ◽  
...  

The effect of precipitated phases on the creep in 300s type austenitic stainless steel used in auto-tailpipe was studied. Flat tensile samples with marker scratches on the surface were strained at slow rate at 400°C. It show that the sensitized material decreased creep rate and needed more stress to generate deformation of grain boundary, suggesting Cr carbides decreased the grain boundary sliding. Thus, the resistance to SCC crack propagation could be improved. Characterizations of the tensile samples were carried out using a SEM in order to understand whether second phases can affect the creep behavior and grain boundary moving.


2014 ◽  
Vol 606 ◽  
pp. 69-72
Author(s):  
Petr Král ◽  
Jiří Dvořák ◽  
Marie Kvapilová ◽  
Jaroslav Lukeš ◽  
Vaclav Sklenička

Experiments were conducted to evaluate creep behavior of conventional and ultrafine-grained metallic materials using nanoindentation technique. The polished surface of samples was loaded up to 5 mN. The load was held constant to examine the creep behavior. Nanoindentation tests were performed at room temperature. Strain rate was evaluated from load and displacement data. The stress exponents of strain rates n were determined from loading stress dependences of creep rate. The values of stress exponents of the indentation strain rate indicate that creep behavior of investigated materials is influenced in particular by slip of intragranular dislocations. By contrast, deformation mechanisms like grain boundary sliding and diffusion processes seem to be improbable.


2001 ◽  
Vol 695 ◽  
Author(s):  
P. A. El-Deiry ◽  
R. P. Vinci

ABSTRACTIn order to shed light on the role that grain boundaries and dislocations play in anelastic relaxation of thin films and small-scale structures, we measured the effective elastic moduli of 99.99% pure Al and Cu 10 m m diameter micro-wires in the as-received (drawn and slight tempered) and annealed states. Moduli were determined using microtensile tests at various strain rates (6.7x10-6s-1, 1.3x10-5s-1, 2.6x10-5s-1, 4.5x10-5s-1, 2.5x10-4s-1, 4.5x10-4s-1). Focused-ion beam scanning electron microscopy was used for imaging grain sizes. Results from the as-received wires are compared with the annealed wires to illustrate the effects of grain size and dislocation density on effective moduli, which closely relates to grain boundary sliding and dislocation motion, respectively. We conclude that microstructure is more significant than scale in inducing anelasticity in small-scale wires and, by extension, thin films.


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