Self-affine Fracture Surface Parameters and Their Relationship with Microstructure in a Cast Aluminum Alloy

2002 ◽  
Vol 17 (6) ◽  
pp. 1276-1282 ◽  
Author(s):  
M. Hinojosa ◽  
J. Aldaco

The possible role of microstructural features in determining the self-affinity of the fracture surface of a cast aluminum alloy is explored in this work. Fracture surfaces generated both in tension and impact tests were topometrically analyzed by atomic force microscopy, scanning electron microscopy, and stylus profilometry. The roughness exponent exhibited the “universal” value ζ ≈ 0.78, and the correlation length ζ was of the order of the grain size. The brittle intermetallic compounds known to be important in crack initiation did not show any correlation with the self-affine parameters of the resulting fracture surfaces in this particular case.

2007 ◽  
Vol 560 ◽  
pp. 41-46 ◽  
Author(s):  
Claus Guerra-Amaro ◽  
M. Hinojosa ◽  
E. Reyes-Melo ◽  
V. González

In the present work we discuss the self-affine properties of the fracture surfaces of sodalime glass obtained under quasi-static conditions. The fracture surfaces are generated using a threepoint bending system in normal room conditions and under high humidity conditions. The surfaces were recorded both by Scanning Electron Microscopy and Atomic Force Microscopy, and their selfaffine properties are characterized using the Variable Bandwidth method. For both conditions it is observed that the major part of the fracture surface is occupied by the mirror zone. On the other hand, the self-affine analysis reveals that for both conditions the roughness exponent has values centred at around 0.58 with moderate dispersion, in agreement with previous results. Our findings support the hypothesis of the existence of a characteristic roughness exponent for quasi-static fracture with a value that is significantly lower than the value of 0.8 reported for rapid fracture conditions.


2006 ◽  
Vol 509 ◽  
pp. 43-48 ◽  
Author(s):  
J. Niño ◽  
M. Hinojosa ◽  
V. González

The fracture surfaces of SAE-1018 steel tension and impact test specimens with different grain sizes are analyzed in order to explore the possible relations between the microstructure and the self-affine fracture surface parameters such as the roughness exponent, ζ, and the correlation length, ξ. The topography of the fracture surfaces was observed and quantified by means of scanning electron microscopy, atomic force microscopy, optical microscopy and optical digitizer. It is confirmed that the fracture surfaces exhibit a self-affine behavior extending over six decades of length scale, from nanometers up to a few millimeters. The roughness exponent exhibits a value of ζ∼0.82 for all the cases regardless of the microstructural condition.


COSMOS ◽  
2008 ◽  
Vol 04 (02) ◽  
pp. 173-183
Author(s):  
BOON TEE ONG ◽  
PARAYIL KUMARAN AJIKUMAR ◽  
SURESH VALIYAVEETTIL

The present article reviews the self-assembly of oligopeptides to form nanostructures, both in solution and in solid state. The solution structures of the peptides were examined using circular dichroism and dynamic light scattering. The solid state assembly was examined by adsorbing the peptides onto a mica surface and analyzing it using atomic force microscopy. The role of pH and salt concentration on the peptide self-assembly was also examined. Nanostructures within a size range of 3–10 nm were obtained under different conditions.


2001 ◽  
Vol 696 ◽  
Author(s):  
F. Arciprete ◽  
F. Patella ◽  
M. Fanfoni ◽  
S. Nufris ◽  
E. Placidi ◽  
...  

AbstractWe have followed by Atomic Force Microscopy (AFM) the epitaxial growth of InAs on GaAs(001) starting from the initial formation of a strained two-dimensional wetting layer up to the self-assembled nucleation and growth of 3D nanoparticles. In this work we underline many aspects of the morphology of this system, which substantiate the role either of kinetics on thermodynamics in the process of growth as well as the role of surface instabilities in controlling lateral ordering of the nanoaggregates.


2001 ◽  
Vol 707 ◽  
Author(s):  
F. Arciprete ◽  
F. Patella ◽  
M. Fanfoni ◽  
S. Nufris ◽  
E. Placidi ◽  
...  

ABSTRACTWe have followed by Atomic Force Microscopy (AFM) the epitaxial growth of InAs on GaAs(001) starting from the initial formation of a strained two-dimensional wetting layer up to the self-assembled nucleation and growth of 3D nanoparticles. In this work we underline many aspects of the morphology of this system, which substantiate the role either of kinetics on thermodynamics in the process of growth as well as the role of surface instabilities in controlling lateral ordering of the nanoaggregates.


CORROSION ◽  
1998 ◽  
Vol 54 (2) ◽  
pp. 129-134 ◽  
Author(s):  
O. P. Modi ◽  
M. Saxena ◽  
B. K. Prasad ◽  
A. K. Jha ◽  
S. Das ◽  
...  

2019 ◽  
Author(s):  
Kevin N. Baumann ◽  
Luca Piantanida ◽  
Javier García-Nafría ◽  
Diana Sobota ◽  
Kislon Voïtchovsky ◽  
...  

The self-assembly of the protein clathrin on biological membranes facilitates essential processes of endocytosis in biological systems and has provided a source of inspiration for materials design by the highly ordered structural appearance. By mimicking the architecture of clathrin self-assemblies to coat liposomes with biomaterials, new classes of hybrid carriers can be derived. Here we present a method for fabricating DNA-coated liposomes by hydrophobically anchoring and subsequently growing a DNA network on the liposome surface which structurally mimics clathrin assemblies. Dynamic light scattering (DLS), ζ-potential and cryo-electron microscopy (cryo-EM) measurements independently demonstrate successful DNA coating. Nanomechanical measurements conducted with atomic force microscopy (AFM) show that the DNA coating enhances the mechanical stability of the liposomes relative to uncoated ones. Furthermore, we provide the possibility to reverse the coating process by triggering the disassembly of the DNA coating through a toehold-mediated displacement reaction. Our results describe a straightforward, versatile, and reversible approach for coating and stabilizing lipid vesicles by an interlaced DNA network. This method has potential for further development towards the ordered arrangement of tailored functionalities on the surfaces of liposomes and for applications as hybrid nanocarrier.


2019 ◽  
Vol 20 (2) ◽  
pp. 268-276
Author(s):  
G. G. Krushenko ◽  
◽  
V. P. Nazarov ◽  
S. N. Reshetnikova ◽  
G. V. Dvirnyi ◽  
...  

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