Fabrication of Highly-ordered and Densely-spaced Silicon Nano-needle Arrays for Bio-sensing Applications

2005 ◽  
Vol 900 ◽  
Author(s):  
Aijun Yin ◽  
Jimmy Xu

ABSTRACTIn this work, we report a success in fabricating highly-ordered and densely-packed array of silicon nano-needles that are vertically aligned, straight and long, meeting many of the requirements for biomolecular sensing and integration with silicon electronics. Yet, we show that they can be fabricated with a relatively simple and non-lithographic method.In this approach the array of nano-needles of high uniformity in length and diameter are made out of silicon by reactive ion etching (RIE) through either an anodic aluminum oxide (AAO) membrane or an array of metallic nano-dot caps that are evaporated on a silicon wafer using an AAO membrane as mask. The AAO membrane itself is formed non-lithographically via anodization of pure aluminum foil and contains an array of highly-ordered and highly-uniform nano-pores. By using the AAO membrane either directly as an etching mask or as an evaporation mask to deposit metallic nanodots which in turn serve as an etching mask, deep and high aspect-ratio etching is possible to allow the formation of the nanoneedles in a Si substrate.

2010 ◽  
Vol 663-665 ◽  
pp. 272-275
Author(s):  
Wen Bin Yang ◽  
Xiao Hong Tang

Anodic aluminum oxide (AAO) film with nanopore arrays was prepared by one-step anodization of highly pure aluminum foil. Morphology, structure and photoluminescence property of AAO were characterized. Results showed that AAO owned honeycomb structure which was characterized by close-packed arrays of columnar hexagonal cells, each containing a central pore normal to the substrate. There were three peaks at around 370, 385 and 470 nm in the PL spectrum of AAO, which should be mainly attributed to the oxygen vacancies.


2005 ◽  
Vol 17 (24) ◽  
pp. 6181-6185 ◽  
Author(s):  
Pyung-Soo Lee ◽  
Ok-Joo Lee ◽  
Sun-Kyu Hwang ◽  
Seung-Ho Jung ◽  
Sang Eun Jee ◽  
...  

2008 ◽  
Vol 8 (9) ◽  
pp. 4803-4807 ◽  
Author(s):  
Youn-Su Kim ◽  
Hyo-Jin Ahn ◽  
Sang Hoon Nam ◽  
Sang Ho Lee ◽  
Hee-Sang Shim ◽  
...  

Patterned arrays of Fe oxide nanoparticles were transferred via contact printing method on a substrate surface using carbon nanotubes embedded in anodic aluminum oxide (CNTs/AAO) as a stamp, in which vertically aligned CNTs in hexagonally patterned array was first fabricated by chemical vapor deposition into the AAO, followed by a partial chemical etching to expose the CNTs from the AAO. Fe precursor inked CNTs stamp was contact-printed on a Pt-coated Si substrate, and after heat treatment at 200 °C, patterned array of Fe oxide nanoparticles with ca. 80 nm of diameter and ca. 120 nm of inter-distance between the nanoparticles was consequently obtained.


2013 ◽  
Vol 13 (11) ◽  
pp. 7401-7405 ◽  
Author(s):  
Jae-Hyun Lee ◽  
Yamujin Jang ◽  
Keun Heo ◽  
Jeong-Mi Lee ◽  
Soon Hyung Choi ◽  
...  

AIP Advances ◽  
2016 ◽  
Vol 6 (12) ◽  
pp. 125002 ◽  
Author(s):  
Chien-Yu Li ◽  
Ciao-Yu Li ◽  
You-Lin Wu ◽  
Chung-Ping Hsu ◽  
Ming-Ching Lee ◽  
...  

2013 ◽  
Vol 705 ◽  
pp. 332-336 ◽  
Author(s):  
Alimorad Rashidi ◽  
M. Omidi ◽  
M. Choolaei ◽  
M. Nazarzadeh ◽  
A. Yadegari ◽  
...  

In this paper a simple method is used for fabrication of vertically aligned carbon nanotube (VACNT) within the cylindrical pores anodic aluminum oxide (AAO) substrate. Electronic and mechanical properties of VACNT have been obtained after removing AAO substrate. Vertically aligned carbon nanotube shows very interesting electromechanical properties which can be used in CNT-based sensors to detect chemical analytical or physical properties such as temperature orpressure.


2013 ◽  
Vol 724-725 ◽  
pp. 63-66
Author(s):  
Guo Feng Ma ◽  
Hong Ling Zhang ◽  
Hong Bo Fu ◽  
Li Na Sun ◽  
Chun Lin He

The anodic aluminum oxide (AAO) templates on polycrystalline silicon substrate are studied for growth of ordered nano-dot arrays in order to fabricate the porous silicon layers. The AAO templates on polycrystalline silicon substrate with pores of average diameter 50nm were successfully prepared by one-step anodization of high pure aluminum layer deposited on polycrystalline silicon in oxalic acid solution. Scanning electron microscopy (SEM) showed that alumina nano-pore arrays were nicely constructed with smooth wall morphologies and well-defined diameters.


Author(s):  
Kashif Azher ◽  
Maaz Akhtar ◽  
Shao-Fu Chang ◽  
Shih-Hsun Chen

In this study, we have developed a swift and well-ordered growth of the Anodic Aluminum Oxide (AAO) nanoporous structure by two-step high temperature anodization of pure Aluminum substrate. The pre-anodization surface treatment of the aluminum substrate assists in the formation of well-organized nanoporous structures. The two-step anodization process was performed in 0.3 M of oxalic acid at 20 °C for 40 V and 45 V to obtain tunable pore diameters. The high temperature of the electrolyte solution helps in the rapid growth of the AAO nanoporous structure. The top surface image of AAO shows a well-ordered nanoporous structure with an average pore diameter of 70 nm at 40 V and 100 nm at 45 V. The SEM cross sectional view also illustrates the well-ordered nano channel and the elemental mapping elaborates the presence of aluminum and oxygen. The thickness of the AAO nanoporous structure was determined by using SEM for three anodization time spans (20, 24 and 28 hours), in which an increasing trend was observed. The fabricated AAO has a higher thickness and a well-ordered nanoporous structure that shows it can be used as a template for fabricating nanostructured materials.


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