Experimental Investigation of Interface Properties in SiC Fiberreinforced Reaction-Bonded Silicon Nitride Matrix Composites

1994 ◽  
Vol 365 ◽  
Author(s):  
J.I. Eldridge ◽  
R.T. Bhatt

ABSTRACTInterfacial properties of 1-D SiC/RBSN composites were measured by the matrix crack spacing method and by the fiber push-out method, and the results were compared. The composites consisted of 8 to 33 vol% of aligned SCS-6 SiC fibers (142 μm diameter) in a relatively porous (20 to 40 vol%) Si3N4 matrix. The effects of fiber volume fraction and test temperature on the interfacial properties have been investigated. The advantages and limitations of both methods in evaluating the interface properties of fiber-reinforced ceramic matrix composites and the factors influencing the interfacial measurements are discussed.

2007 ◽  
Vol 546-549 ◽  
pp. 1555-1558
Author(s):  
Chun Jun Liu ◽  
Yue Zhang ◽  
Da Hai Zhang ◽  
Zhong Ping Li

In this paper the composite fracture process has been simulated via the finite element method. A micromechanics model was developed to predict the stress-strain response of a SiO2f/ SiO2 composite explicitly accounting for the local damage mechanisms such as fiber fracture and interfacial debonding. The effects of interfacial strength and fiber volume fraction on the toughness of fiber-reinforced ceramic matrix composites were investigated. The results showed that the composite failure behaviors correlated with the interface strength, which could achieve an optimum value for the elevation of the composite toughness. The increase of fiber volume fraction can make more toughening contributions.


2021 ◽  
pp. 002199832110112
Author(s):  
Qing Yang Steve Wu ◽  
Nan Zhang ◽  
Weng Heng Liew ◽  
Vincent Lim ◽  
Xiping Ni ◽  
...  

Propagation of ultrasonic wave in Carbon Fiber Reinforced Polymer (CFRP) is greatly influenced by the material’s matrix, resins and fiber volume ratio. Laser ultrasonic broadband spectral technique has been demonstrated for porosity and fiber volume ratio extraction on unidirection aligned CFRP laminates. Porosity in the matrix materials can be calculated by longitudinal wave attenuation and accurate fiber volume ratio can be derived by combined velocity through the high strength carbon fiber and the matrix material with further consideration of porosity effects. The results have been benchmarked by pulse-echo ultrasonic tests, gas pycnometer and thermal gravimetric analysis (TGA). The potentials and advantages of the laser ultrasonic technique as a non-destructive evaluation method for CFRP carbon fiber volume fraction evaluation were demonstrated.


1994 ◽  
Vol 77 (7) ◽  
pp. 1897-1900 ◽  
Author(s):  
Hockin H. K. Xu ◽  
Claudia P. Ostertag ◽  
Linda M. Braun ◽  
Isabel K. Lloyd

Author(s):  
Rajesh S. Kumar

Abstract Initial mechanical behavior of Ceramic Matrix Composites (CMCs) is linear until the proportional limit. This initial behavior is characterized by linear elastic properties, which are anisotropic due to the orientation and arrangement of fibers in the matrix. The linear elastic properties are needed during various phases of analysis and design of CMC components. CMCs are typically made with ceramic unidirectional or woven fiber preforms embedded in a ceramic matrix formed via various processing routes. The matrix processing of interest in this work is that formed via Polymer Impregnation and Pyrolysis (PIP). As this process involves pyrolysis process to convert a pre-ceramic polymer into ceramic, considerable volume shrinkage occurs in the material. This volume shrinkage leads to significant defects in the final material in the forms of porosity of various size, shape, and volume fraction. These defect structures can have a significant impact on the elastic and damage response of the material. In this paper, we develop a new micromechanics modeling framework to study the effects of processing-induced defects on linear elastic response of a PIP-derived CMC. A combination of analytical and computational micromechanics approaches is used to derive the overall elastic tensor of the CMC as a function of the underlying constituents and/or defect structures. It is shown that the volume fraction and aspect ratio of porosity at various length-scales plays an important role in accurate prediction of the elastic tensor. Specifically, it is shown that the through-thickness elastic tensor components cannot be predicted accurately using the micromechanics models unless the effects of defects are considered.


1995 ◽  
Vol 62 (3) ◽  
pp. 590-594
Author(s):  
N. Chandra ◽  
Zhiyum Xie

A pair of two new tensors called GPS tensors S and D is proposed for the concentric cylindrical inclusion problem. GPS tensor S relates the strain in the inclusion constrained by the matrix of finite radius to the uniform transformation strain (eigenstrain), whereas tensor D relates the strain in the matrix to the same eigenstrain. When the cylindrical matrix is of infinite radius, tensor S reduces to the appropriate Eshelby’s tensor. Explicit expressions to evaluate thermal residual stresses σr, σθ and σz in the matrix and the fiber using tensor D and tensor S, respectively, are developed. Since the geometry of the present problem is of finite radius, the effect of fiber volume fraction on the stress distribution can be easily studied. Results for the thermal residual stress distributions are compared with Eshelby’s infinite domain solution and finite element results for a specified fiber volume fraction.


Author(s):  
Rajesh Kumar

Abstract Initial mechanical behavior of Ceramic Matrix Composites (CMCs) is linear until the proportional limit. This initial behavior is characterized by linear elastic properties, which are anisotropic due to the orientation and arrangement of fibers in the matrix. The linear elastic properties are needed during analysis and design of CMC components. CMCs are made with ceramic unidirectional or woven fiber preforms embedded in a ceramic matrix formed via various processing routes. The matrix processing of interest in this work is the Polymer Impregnation and Pyrolysis (PIP) process. As this process involves pyrolysis to convert a pre-ceramic polymer into ceramic, considerable volume shrinkage occurs in the material. This leads to significant defects in the form of porosity of various size, shape, and volume fraction. These defect structures can have a significant impact on the elastic and damage response of the material. In this paper, we develop a new micromechanics modeling framework to study the effects of processing-induced defects on linear elastic response of a PIP-derived CMC. A combination of analytical and computational micromechanics approaches is used to derive the overall elastic tensor of the CMC as a function of the underlying constituents and/or defect structures. It is shown that the volume fraction and aspect ratio of porosity at various length-scales plays an important role in accurate prediction of the elastic tensor. Specifically, it is shown that the through-thickness elastic tensor components cannot be predicted accurately using the micromechanics models unless the effects of defects are considered.


2019 ◽  
Vol 90 (7-8) ◽  
pp. 909-924 ◽  
Author(s):  
Longbiao Li

In this paper, the stress-dependent matrix multiple fracture in silicon carbide fiber-reinforced ceramic-matrix composites with different fiber preforms is investigated. The critical matrix strain energy criterion is used to determine the matrix multiple fracture considering the interface debonding. The effects of the fiber radius, fiber elastic modulus, matrix elastic modulus, fiber volume, interface shear stress, and interface debonded energy on the matrix multiple fracture and the interface debonding are analyzed. The experimental matrix multiple cracking and interface debonding of minicomposite, unidirectional, and two-dimensional woven SiC/SiC composites with different fiber volumes and interphases are predicted. The matrix cracking density increases with the increasing of the fiber volume, fiber elastic modulus, interface shear stress, and interface debonded energy, and the decreasing of the fiber radius and matrix elastic modulus.


1981 ◽  
Vol 12 ◽  
Author(s):  
M. R. Jackson ◽  
J. L. Walter

ABSTRACTFor the Ni-base TaC eutectics, it has been shown previously that carbide volume fraction is a strong function of Ta/C ratio. Now in a number of Ni,Cr-TaC and Ni,Cr,Al-TaC alloys, Cr has been observed to have only a small influence on volume fraction of carbide, while Al has a major influence acting to decrease the volume fraction. The Al present in the matrix causes the phase equilibrium to approach that of a much greater Ta/C ratio. This analysis has been extended to more complex NiTaC alloys as well. For the simple Ni-Cr-Ta-C alloys, creep behavior has been studied as a function of volume fraction of carbide.Other carbide systems have been evaluated as well, including TiC and NbC. A general understanding of volume fraction differences between these systems and TaC can be reached by consideration of ideal solution behavior and the appropriate phase diagrams.


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