Interconnect Failure Mechanism Maps for Different Metallization Materials and Processes

1999 ◽  
Vol 563 ◽  
Author(s):  
V. K. Andleigh ◽  
Y. J. Park ◽  
C. V. Thompson

AbstractA tool for simulation of electromigration and electromigration-induced damage, MIT/EmSim, has been used to investigate interconnect reliability, focusing on transitions in failure mechanisms associated with void nucleation, growth, and growth saturation. Conventional scaling of electromigration test results assume that the median time to electromigration-induced failure scales with the current density j to the power −n. The effects of transitions in failure mechanisms have been studied by characterizing the apparent current density exponent. When failure is limited by void nucleation, n=2 scaling is observed, and when failure requires substantial void growth, n=1 scaling is observed. When lines end at diffusion barriers such as W or liner-filled vias, void growth saturates in short lines at low current densities, and, depending on the failure criterion, lines under these conditions can be ‘immortal’. As growth saturates, apparent current density exponents increase above 2. Failure mechanism maps can be constructed to illustrate the failure mechanisms and scaling behavior as a function of line length and current density. Failure maps can be used in accurately scaling test results to service conditions, to suggest layout strategies for optimized circuit reliability, and to assess the reliability of new interconnect materials and structures.

1995 ◽  
Vol 391 ◽  
Author(s):  
J. J. Clement ◽  
J. R. Lloyd ◽  
C. V. Thompson

AbstractFailure of the tungsten-filled via interconnect structure is modelled. Two mechanisms contributing to void growth are considered: relief of stress due to differential thermal expansion, and electromigration. A self-limiting void volume is predicted, resulting in a self-limiting resistance increase which is a function of structure geometry and the void morphology. The relative contributions of the two mechanisms change significantly as the temperature and current density are reduced from accelerated test conditions, affecting the extrapolation of test results to service conditions. Modified procedures for extrapolating lifetimes are discussed, as well as suggested process changes to improve reliability.


2006 ◽  
Vol 15-17 ◽  
pp. 816-821 ◽  
Author(s):  
Geert Mertens ◽  
Lode Duprez ◽  
Bruno C. De Cooman ◽  
Marc Verhaege

The presence of hydrogen in steel decreases its toughness and formability leading to hydrogen embrittlement. To understand the failure mechanisms of steel due to the presence of hydrogen, a profound insight in the hydrogen household of the steel is needed. This includes a study of the solubility, the diffusion and the trapping of hydrogen. Next, the absorption and desorption behavior during and after electrolytic charging must be well determined. This was investigated in this research for steels with various types of traps, e.g. dislocations, microcracks, grain boundaries and precipitates such as TiC and Ti4C2S2. The samples were cathodically charged at three different current densities: 0.8mA/cm2; 8.3mA/cm2 and 62.5mA/cm2. It was noticed that the cathodic current density used for hydrogen loading had a great influence on the results. Observation of the samples by scanning electron microscopy (SEM) showed that at the highest current density major damage of the surface had occurred. Hence it was decided to study more systematically the influence of charging current density on the resulting surface aspect and on hydrogen absorption and desorption. The hydrogen charging kinetics, maximum hydrogen solubility and hydrogen desorption behavior have also been evaluated for the different current densities during charging.


1993 ◽  
Vol 308 ◽  
Author(s):  
O. Kraft ◽  
S. Bader ◽  
J.E. Sanchez ◽  
E. Arzt

ABSTRACTAccelerated electromigation tests on unpassivated, pure aluminum interconnects were performed. The failure mechanisms were observed by interrupting the tests and examining the conductor lines using an SEM. Because the metal thin film was subjected to a so-called laser reflow process before patterning, grain boundaries were visible in the SEM as thermal grooves. Voids were observed to move along the line and to grow in a transgranular manner, and a characteristic asymmetric void shape was identified which seems to be related to the failure mechanism. It is argued that substantial progress in modelling and understanding of electromigration failure can be made by consideration of such void shape effects.


1993 ◽  
Vol 309 ◽  
Author(s):  
O. Kraft ◽  
S. Bader ◽  
J.E. Sanchez ◽  
E. Arzt

AbstractAccelerated electromigation tests on unpassivated, pure aluminum interconnects were performed. The failure mechanisms were observed by interrupting the tests and exanming the conductor lines using an SEM. Because the metal thin film was subjected to a so-called laser reflow process before patterning, grain boundaries were visible in the SEM as thermal grooves. Voids were observed to move along the line and to grow in a transgranular manner, and a characteristic asymmetric void shape was identified which seems to be related to the failure mechanism. It is argued that substantial progress in modelling and understanding of electromigration failure can be made by consideration of such void shape effects.


2003 ◽  
Vol 766 ◽  
Author(s):  
C. L. Gan ◽  
C.V. Thompson ◽  
K. L. Pey ◽  
W. K. Choi ◽  
C. W. Chang ◽  
...  

AbstractThe reliability of Cu dual-damascene interconnect trees with 3-terminal (dotted-I), 4-terminal (‘T’) and 5-terminal (‘+’) configurations has been investigated. The lifetime of multiterminal interconnect trees with the same current density through the common middle via was determined to be independent of the number of segments connected at the common junction. Furthermore, our experimental results on dotted-I test structures showed an increase in the reliability of the interconnect tree when the distribution of a same current was not equal in the two connected segments, especially for the cases where one of the segments was acting as a passive reservoir or active source of Cu atoms for the adjoining segment. Due to the low barrier for void nucleation at the Cu/Si3N4 interface, the presence of any small atomic source in neighboring segments will enhance the reliability of a connected segment in which Cu atoms are being drained away. As a consequence, failure can occur in a tree segment which is stressed at significantly lower current densities than more highly stressed adjoining segments.


1994 ◽  
Vol 338 ◽  
Author(s):  
U.E. Möckl ◽  
M. Bauer ◽  
O. Kraft ◽  
J.E. Sanchez ◽  
E. Arzt

ABSTRACTBecause of the continuing miniaturization, electromigration (EM) phenomena are still a key issue in reliability of VLSI metallizations. The present study of EM induced voiding and hillocking was performed on unpassivated conductor lines with various widths and current densities. Stressed and unstressed interconnects were carefully examined with SEM and TEM techniques, especially with regard to void densities, void sizes and characteristic lengths between void and hillock. The fatal void shape was related to current density and line width indicating that the failure mechanism changes with decreasing line width and decreasing current density.


Author(s):  
Jin Young Kim ◽  
R. E. Hummel ◽  
R. T. DeHoff

Gold thin film metallizations in microelectronic circuits have a distinct advantage over those consisting of aluminum because they are less susceptible to electromigration. When electromigration is no longer the principal failure mechanism, other failure mechanisms caused by d.c. stressing might become important. In gold thin-film metallizations, grain boundary grooving is the principal failure mechanism.Previous studies have shown that grain boundary grooving in gold films can be prevented by an indium underlay between the substrate and gold. The beneficial effect of the In/Au composite film is mainly due to roughening of the surface of the gold films, redistribution of indium on the gold films and formation of In2O3 on the free surface and along the grain boundaries of the gold films during air annealing.


Author(s):  
I-Fei Tsu ◽  
D.L. Kaiser ◽  
S.E. Babcock

A current theme in the study of the critical current density behavior of YBa2Cu3O7-δ (YBCO) grain boundaries is that their electromagnetic properties are heterogeneous on various length scales ranging from 10s of microns to ˜ 1 Å. Recently, combined electromagnetic and TEM studies on four flux-grown bicrystals have demonstrated a direct correlation between the length scale of the boundaries’ saw-tooth facet configurations and the apparent length scale of the electrical heterogeneity. In that work, enhanced critical current densities are observed at applied fields where the facet period is commensurate with the spacing of the Abrikosov flux vortices which must be pinned if higher critical current density values are recorded. To understand the microstructural origin of the flux pinning, the grain boundary topography and grain boundary dislocation (GBD) network structure of [001] tilt YBCO bicrystals were studied by TEM and HRTEM.


Author(s):  
M. R. McCartney ◽  
J. K. Weiss ◽  
David J. Smith

It is well-known that electron-beam irradiation within the electron microscope can induce a variety of surface reactions. In the particular case of maximally-valent transition-metal oxides (TMO), which are susceptible to electron-stimulated desorption (ESD) of oxygen, it is apparent that the final reduced product depends, amongst other things, upon the ionicity of the original oxide, the energy and current density of the incident electrons, and the residual microscope vacuum. For example, when TMO are irradiated in a high-resolution electron microscope (HREM) at current densities of 5-50 A/cm2, epitaxial layers of the monoxide phase are found. In contrast, when these oxides are exposed to the extreme current density probe of an EM equipped with a field emission gun (FEG), the irradiated area has been reported to develop either holes or regions almost completely depleted of oxygen. ’ In this paper, we describe the responses of three TMO (WO3, V2O5 and TiO2) when irradiated by the focussed probe of a Philips 400ST FEG TEM, also equipped with a Gatan 666 Parallel Electron Energy Loss Spectrometer (P-EELS). The multi-channel analyzer of the spectrometer was modified to take advantage of the extremely rapid acquisition capabilities of the P-EELS to obtain time-resolved spectra of the oxides during the irradiation period. After irradiation, the specimens were immediately removed to a JEM-4000EX HREM for imaging of the damaged regions.


Coatings ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 56
Author(s):  
Ashutosh Sharma ◽  
Byungmin Ahn

Metallic and alloyed coatings are used widely in several decorative and technology-based applications. In this work, we selected Sn coatings plated on Cu substrates for joining applications. We employed two different plating baths for the fabrication of Sn and Ni coatings: acidic stannous sulfate for Sn and Watts bath for Ni layer. The plating current densities were varied from 100–500 mA/cm2. Further, the wear and friction behavior of the coatings were studied using a ball-on-disc apparatus under dry sliding conditions. The impact of current density was studied on the morphology, wear, and coefficient of friction (COF) of the resultant coatings. The wear experiments were done at various loads from 2–10 N. The sliding distance was fixed to 7 m. The wear loss was quantified in terms of the volume of the track geometry (width and depth of the tracks). The results indicate that current density has an important role in tailoring the composition and morphology of coatings, which affects the wear properties. At higher loads (8–10 N), Sn coatings on Ni/Cu had higher volume loss with a stable COF due to a mixed adhesive and oxidative type of wear mechanism.


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