Wear behavior of hydroxyapatite reinforced polymer composite for biomedical applications

In medical fields, hydroxyapatite (HA) is used for restoring the human bones and teeth. Nowadays, newer bio composites are being developed to replace the broken or removed teeth in human using hydroxyapatite. The original teeth may be removed from human, due to various reasons such as tooth decay, periodontal disease and gum diseases. Due to the bioactivity property of HA, it helps the tooth to grow. In this work, tribological properties of HA powder reinforced composite are investigated. Three most important factors that affect the properties of the composites were chosen and varied during wear testing of the composites. The HA powder weight %, applied load (P) and sliding distance (SD) were varied on the basis of Taguchi’s experimental design. Analysis of variance (ANOVA) and (Signal to Noise) SN ratio analysis was used to study the influence of each factor on the specific wear rate (SWR). It was concluded that the HA wt. % highly influences the SWR of the composite during pin on disc testing.

Effect of Reinforcements on the Sliding Wear Behavior of Self-Lubricating AZ91D-SiC-Gr Hybrid Composites

This article statistically investigates the effect of various parameters such as material factors: silicon carbide (SiC) reinforcement, graphite (Gr) reinforcement and mechanical factors: normal load, sliding distance and speed on the sliding wear rate of vacuum stir cast self-lubricating AZ91D-SiC-Gr hybrid magnesium composites. The sliding wear tests have been performed on pin-on-disc tribometer at 10-50N loads, 1-3m/s sliding speed and 1000-2000m sliding distance. It has been examined that hybrid composites yielded improved wear resistance with reinforcement of SiC and solid lubricant graphite. ANOVA and signal-to-noise ratio investigation indicated that applied load was the most critical factor influencing the wear rate, followed by sliding distance. Further, the AZ91D/5SiC/5Gr hybrid composite has exhibited the best wear properties. From the SEM and EDS analysis of worn surfaces, delamination was confirmed as the dominant wear mechanism for AZ91D-SiC-Gr hybrid composites.

Comparison of the Wear Behavior and Hardness of Vinylester Resin Reinforced by Glass Fiber and Nano ZrO2 and Fe3O4

The current trend in scientific researches is to improve the performance of mechanical and physical properties of polymeric compounds, one of these methods is to add nanoparticles to polymeric composites. In this work, the wear behaviour (pin to disc) of nanocomposites composed of vinyl ester reinforced glass fibers and nanoparticles was evaluated under three different factors, such as specimen content, load applied, and distance sliding using a sliding time constant, as well as studying the hardness shore for these nanocomposites. The (hand-lay) method was used for the purpose of preparing the nanocomposites from vinyl ester filled with 10% vf. glass fiber and (0.5%, 1%, 1.5%, and 2% vf. of nano-Fe3O4 and ZrO2). The results are tabulated and analysed using Taguchi experiments (L9) (Minitab 18) for the purpose of determining which of the factors under consideration had the greatest influence on the wear behaviour. From the results, it was found that the specimens (vinyl ester-10% vf. glass fibers-2% ZrO2) and (vinyl ester-10% vf. glass fibers-2% Fe3O4) give the best wear resistance 0.003×10-5, 0.012×10-5 mm3/Nm respectively under the factors (load 20 N, sliding distance 45 cm). It was found that the specimen content is the most important factor influencing the wear behaviour, followed by the factors of the applied load and then the sliding distance. The addition of nanoparticles (0.5-2% vf. ZrO2, Fe3O4) to the vinyl ester resin improved the hardness values. Furthermore, the findings show that the addition of nanoparticles (ZrO2, Fe3O4) had a positive effect on the (wear and hardness) tests, implying that the nanoparticles improved the bonding between the base material and reinforcing material.

Optimization and analysis of dry sliding wear process parameters on cellulose reinforced ABS polymer composite material

Purpose This study aims to the optimization using three factors and three-level parameters (sliding speed [rpm], sliding distance [m/s] and load [N]) of design matrix were adapted to Box–Behnken design using design expert v8.0 software. Based on the parameters, to develop the linear regression equation and to find the significant considerable wear process parameters based on output responses like wear loss (WL) and coefficient of friction (COF) value of polymer matrix composites (PMC) specimen of Acrylonitrile-butadiene-styrene (ABS)/cellulose composite (80 wt% of ABS and 20 wt% of cellulose). Design/methodology/approach The fabrication of the ABS/cellulose composite sample was carried out by the simple hands-on stir process method. As per the American Society for Testing and Materials G99 standard, the sample was made by the molding process. The wear analysis was made by multi tribotester TR25 machine and validated the developed model by using statistical software design expert v.8.0 and numerical tools like analysis of variance. The surface morphology [field emission scanning electron microscopy (FESEM) analysis] of the sample was also observed using the Quanta FEG-250 FESEM instrument. Findings The parameters like sliding speed, sliding distance and load are independently affected the COF value and WL of the 80% of ABS matrix and 20% cellulose reinforced composite material. The regression equations were generated by the coefficient of friction value and WL, which predicted the minimum WL of 80% of ABS matrix and 20% of cellulose reinforced composite material. The worn surface analysis result exposes the worn path and equal distribution of reinforcement and matrix on the surface of composite material. Originality/value The literature survey revealed a small number of studies available regarding wear analysis of ABS matrix and cellulose reinforced composite materials. In the present work, to fabricate and evaluate the wear performance of PMC (80% of ABS and 20% of cellulose) depends on the WL and COF value. The maximum and minimum COF value (µ) of 80% of ABS and 20% of cellulose composite material is 4.71 and 0.28 with the optimized wear process parameter by 1,000 mm of sliding distance, 0.25 (m/s) of sliding speed and 9 N of load.

An investigation on dry sliding wear behavior of Al6061/ Titanium carbide/ Basalt hybrid metal matrix composites

Dry sliding wear plays an important role in selecting material for automotive and aerospace applications. Researchers have been exploring novel aluminum matrix composites (AMC), which offer minimum wear rate for various tribological applications. The present work involves multi-objective optimization for dry sliding wear behavior of Al6061 reinforced with 6 % of Titanium carbide and 4% of basalt hybrid metal matrix composites using principal component analysis (PCA)-based grey relational analysis (GRA). In this article, the effects of input variables of wear parameters such as applied load, sliding speed and sliding distance were investigated on different output responses, namely the wear rate, friction force and specific wear rate. Taguchi’s L9 orthogonal array with three-level settings was chosen for conducting experiments. Three output responses in each experiment were normalized into a weighted grey relational grade using grey relational analysis coupled with the principal component analysis. The analysis of variance indicated that sliding distance is the most influential parameter followed by load and sliding velocity that contributes to the quality characteristics. Optimal results have been verified through additional experiments.

Wear characteristics of additively manufactured AlSi10Mg against EN-31 and silicon carbide abrasive sheet counter bodies using box Behnken design approach

High strength-to-weight ratio materials are used in the automotive and aerospace industries, and AlSi10Mg is suitable for those applications. The research aims to compare and investigate the wear characteristics of selective laser melted AlSi10Mg pin against two counter bodies, EN-31 hardened steel, and silicon carbide abrasive sheet. The wear rate of additively manufactured AlSi10Mg pin at 0° building orientation was investigated using the box Behnken design approach to identify the suitable wear parameters with the pin on the disc testing facility. Based on analysis of variance, the interaction of load with sliding distance significantly influenced the wear rate of AlSi10Mg in both counter body cases. The adhesion and abrasion wear mechanism were observed in AlSi10Mg with EN-31 and silicon carbide abrasive sheet, respectively. The findings reveal the effect of two counter bodies on the SLMed AlSi10Mg wear phenomenon. Finally, severe wear was observed in the AlSi10Mg pin against the silicon carbide counter body.

Wear analysis of natural-inorganic fiber reinforced automotive brake composites

Brake friction composite materials comprising varying proportions of natural (banana) and inorganic (lapinus) fibers were designed, fabricated by compression molding, and characterized for sliding wear performance. The sliding wear properties of the manufactured friction composites have been studied by the Taguchi method. An orthogonal array (L 16) was used to investigate the influence of sliding wear parameters. A series of tests were conducted on a pin-on-disc machine by considering four control parameters: composition, normal load, sliding velocity, and sliding distance, each having four levels. The results showed that the wear in terms of weight loss decreases with increasing banana fiber and increases with increasing lapinus fiber, normal load, sliding velocity, and sliding distance. The results indicate that the normal load emerges as the most significant control parameter affecting wear performance, followed by sliding distance and sliding velocity.

Tensile and wear properties of repetitive corrugation and straightened Al 2024 alloy: an experimental and RSM approach

Repetitive Corrugation and Straightening (RCS) on sheet geometries causes Cyclic Plastic Deformation, resulting in potential improvements of mechanical characteristics in metals and alloys. In this study, sample sheets of Al 2024 are subjected to severe plastic deformation with specially designed corrugated rollers to generate heterogeneous repeated plastic deformation at room temperature. The material shows enhanced properties under severe plastic deformation, with 5.07% increase in tensile strength, compared to unprocessed material. Maximum tensile strength was observed at annealed temperature of 150 °C is of about 3.49% increase in tensile strength over other temperature conditions. A wear study was carried out by considering the processed sheet that yields high tensile strength (annealed at 150 °C) by varying process parameters like sliding distance, load and sliding velocity as per design of experiments. In comparison to all other combinations, the wear resistance was shown to be better with a sliding distance of 6000 m, a load of 9.81 N, and a sliding velocity of 1.45 m s−1. The Response Surface Methodology (RSM) approach was adopted for comparing purpose, the experimental findings are found to be more similar to the RSM approach’s outcomes.

The investigation of the effect of nano particles on dry sliding wear and corrosion behavior of Al-Mg/Al2O3 composites

Aluminum matrix composites were extensively used as structural material as it possesses good surface properties such as wear and corrosion resistance. The practical importance of nano particles in composite materials has triggered widespread attention towards the enhancement of its properties. In this study, Al-Mg/Al2O3 (0–8 wt%) metal matrix nano composites fabricated by two step stir casting route was investigated to comprehend its wear and corrosion behaviour. The Pin-on-Disc dry sliding wear test was performed on Al-Mg/Al2O3 (0–8 wt%) by adopting Design of Experiments under the action of different contact loads and sliding distance following the ASTM G99 Standard. The experimental results conveyed that specific wear rate decreases with increase in sliding distance. Statistical analysis was performed by Taguchi’s Technique and Analysis of Variance (ANOVA) to determine the most dominating factor that influences specific wear rate for the optimum weight percentage of reinforcement. Analysis revealed adequacy with the constructed model in predicting the wear behavior of composite and unreinforced Al-Mg alloy. The corrosion behaviour of the base alloy and composites was analysed by static immersion and electrochemical assessments, by immersing prepared specimens in aqueous sodium chloride (3.5%) solution. The dependance of corrosion rate of the composites with the weight percentage of Al2O3, exposure duration and temperature of the corrosive medium was studied in detail. Corrosion test results exhibit that corrosion rate decreases with increase in weight percentage of Al2O3 particles and exposure duration, whereas it follows reverse trend with increase in corrosion medium temperature.

Liquid Crystal Display (LCD) and Organic Light Emitting Diode (OLED) Applications on Natural Fibre Reinforced Polymer Matrix Composites

Natural materials are the alternative source for the manufacture of products due to environmental requirements. Hot injection moulding techniques make the composite product with fibreglass, granite waste filler, and polylactic acid (PLA). Five samples of each set and sampled with better hardness varied the volumetric percentage of glass fibre and the waste nanogranite particles. This effort is mainly concerned with evaluating the wear of dry sliding and friction of composites. Varying 15, 25, 35, and 45 N load, 750 and 1500 m sliding distance tested the composite materials, respectively. Parametric condition experiments were carried out at the stated process to record answers. Nanogranite composite materials are better than higher concentrations of glass fibre in PLA matrices composites, which are more resistant to wear and friction coefficients. The nanogranite powder is added with the filler element in the PLA matrix to provide a better coefficient of wear and rubbing. A high load of 45 N and a sliding distance of 1500 m were measured at low wear and low friction coefficients.