Proton Conducting Organic/Inorganic Nanocomposite Polymer Electrolytic Membrane Synthesized by Sol-Gel Process

ABSTRACTIn this paper, new synthetic routes have been investigated for the preparation of Organic/inorganic nanocomposite polymer membranes consisting of SiO2 /PTMO(polytetramethylene oxide) hybrids and novel proton conducting materials. These materials have been synthesized through sol-gel processes in flexible, ductile, free-standing thin membrane form. The hybrid membrane has been found to be thermally stable up to 160 C and possesses proton conductivities of approximately 10−4 S/cm from a room temperature to 160 C.

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Preparation of the PVA/TiO2 nanocomposite polymer membranes by a sol-gel process for alkaline DMFC

ECS Transactions ◽

10.1149/1.2927185 ◽

2019 ◽

Vol 6 (26) ◽

pp. 17-44 ◽

Cited By ~ 8

Author(s):

Chun-Chen Yang ◽

Che-Tseng Lin

Keyword(s):

Sol Gel ◽

Polymer Membranes ◽

Nanocomposite Polymer ◽

Sol Gel Process

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Effect of Annealing temperature on the Structural and Magnetic Properties of TbxY3-xFe5O12(x = 0.0, 1.0, 2.0) Thin Films Prepared by Sol-Gel Process

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.501.236 ◽

2012 ◽

Vol 501 ◽

pp. 236-241 ◽

Cited By ~ 1

Author(s):

Ftema W. Aldbea ◽

Noor Bahyah Ibrahim ◽

Mustafa Hj. Abdullah ◽

Ramadan E. Shaiboub

Keyword(s):

Thin Films ◽

Magnetic Properties ◽

Room Temperature ◽

Annealing Temperature ◽

Sol Gel ◽

Vibrating Sample Magnetometer ◽

X Ray ◽

Garnet Phase ◽

Sol Gel Process ◽

Amorphous Structures

Thin films nanoparticles TbxY3-xFe5O12 (x=0.0, 1.0, 2.0) were prepared by the sol-gel process followed by annealing process at various annealing temperatures of 700° C, 800° C and 900° C in air for 2 h. The results obtained from X-ray diffractometer (XRD) show that the films annealed below 900°C exhibit peaks of garnet mixed with small amounts of YFeO3 and Fe2O3. Pure garnet phase has been detected in the films annealed at 900°C. Before annealing the films show amorphous structures. The particles sizes measurement using the field emission scanning electron microscope (FE-SEM) showed that the particles sizes increased as the annealing temperature increased. The magnetic properties were measured at room temperature using the vibrating sample magnetometer (VSM). The saturation magnetization (Ms) of the films also increased with the annealing temperature. However, different behavior of coercivity (Hc) has been observed as the annealing temperature was increased.

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Indium oxide octahedrons based on sol–gel process enhance room temperature gas sensing performance

Journal of Alloys and Compounds ◽

10.1016/j.jallcom.2015.03.002 ◽

2015 ◽

Vol 637 ◽

pp. 55-61 ◽

Cited By ~ 14

Author(s):

Xiaohui Mu ◽

Changlong Chen ◽

Liuyuan Han ◽

Baiqi Shao ◽

Yuling Wei ◽

...

Keyword(s):

Indium Oxide ◽

Room Temperature ◽

Gas Sensing ◽

Sol Gel ◽

Sol Gel Process ◽

Sensing Performance

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Fabrication of sulfonated poly(ether ether ketone)-based hybrid proton-conducting membranes containing carboxyl or amino acid-functionalized titania by in situ sol–gel process

Journal of Power Sources ◽

10.1016/j.jpowsour.2014.11.132 ◽

2015 ◽

Vol 276 ◽

pp. 271-278 ◽

Cited By ~ 50

Author(s):

Yongheng Yin ◽

Tao Xu ◽

Guangwei He ◽

Zhongyi Jiang ◽

Hong Wu

Keyword(s):

Amino Acid ◽

Sol Gel ◽

Proton Conducting ◽

Ether Ether Ketone ◽

Poly Ether Ether Ketone ◽

Sol Gel Process ◽

Ether Ketone ◽

Conducting Membranes ◽

Sulfonated Poly

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Preparation of PVDF/Al2O3hybrid membrane via the sol–gel process and characterization of the hybrid membrane

Desalination and Water Treatment ◽

10.1080/19443994.2013.781986 ◽

2013 ◽

Vol 51 (19-21) ◽

pp. 3685-3690 ◽

Cited By ~ 14

Author(s):

Hao Dong ◽

Kai-jun Xiao ◽

Xiang-li Li ◽

Yuan Ren ◽

Si-yuan Guo

Keyword(s):

Sol Gel ◽

Hybrid Membrane ◽

Sol Gel Process

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Structural, Optical, and pH-Stimulus Response Properties of Cresol Red Immobilized Nanocomposite Silica Films Derived by a Sol–Gel Process Employing Different Synthetic Routes

Industrial & Engineering Chemistry Research ◽

10.1021/ie500846z ◽

2014 ◽

Vol 53 (49) ◽

pp. 18863-18872 ◽

Cited By ~ 5

Author(s):

Shobhit Singh Chauhan ◽

R. V. Jasra ◽

A. L. Sharma

Keyword(s):

Sol Gel ◽

Silica Films ◽

Response Properties ◽

Stimulus Response ◽

Sol Gel Process ◽

Synthetic Routes ◽

Cresol Red

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Evaluations of Hydrogen Permeation on γ-Al2O3 Synthesized by Sol-Gel Process

Materials Science Forum ◽

10.4028/www.scientific.net/msf.620-622.25 ◽

2009 ◽

Vol 620-622 ◽

pp. 25-28

Author(s):

Ji Hee Park ◽

Mie Won Jung ◽

Tae Whan Hong

Keyword(s):

Room Temperature ◽

Ceramic Membrane ◽

Hydrogen Permeation ◽

Thermal Evolution ◽

Sol Gel ◽

Alumina Ceramic ◽

Distilled Water ◽

Ceramic Support ◽

Sol Gel Process ◽

Metal Ceramic

The purpose of this work was hydrogen permeation of ceramic or metal/ceramic membrane using γ-Al2O3 by synthesizing. The γ-Al2O3 was synthesized by using the sol-gel process with aluminum isopropoxide and primary distilled water as the precursor and solvent. The γ-Al2O3-based membranes were prepared using HPS. The phase transformation, thermal evolution, surface are and morphology of γ-Al2O3 and γ-Al2O3-based membranes were characterized by XRD, TG-DTA, BET and FE-SEM. The hydrogen permeation of γ-Al2O3-based membranes was examined at room temperature comparing with other paper using nickel composited membrane on alumina ceramic support.

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