Shock-induced amorphization in ultra-fine grained pure copper

Author(s):  
Tao Wang ◽  
Tian Ye ◽  
Yong Feng ◽  
Kai-Xuan Wang ◽  
Yu-Xuan Du ◽  
...  
Keyword(s):  
2006 ◽  
Vol 18 (22) ◽  
pp. 2949-2953 ◽  
Author(s):  
Y.-H. Zhao ◽  
J. F. Bingert ◽  
X.-Z. Liao ◽  
B.-Z. Cui ◽  
K. Han ◽  
...  
Keyword(s):  

Science ◽  
2020 ◽  
Vol 370 (6518) ◽  
pp. 831-836
Author(s):  
X. Y. Li ◽  
Z. H. Jin ◽  
X. Zhou ◽  
K. Lu

Metals usually exist in the form of polycrystalline solids, which are thermodynamically unstable because of the presence of disordered grain boundaries. Grain boundaries tend to be eliminated through coarsening when heated or by transforming into metastable amorphous states when the grains are small enough. Through experiments and molecular dynamics simulations, we discovered a different type of metastable state for extremely fine-grained polycrystalline pure copper. After we reduced grain sizes to a few nanometers with straining, the grain boundaries in the polycrystals evolved into three-dimensional minimal-interface structures constrained by twin boundary networks. This polycrystalline structure that underlies what we call a Schwarz crystal is stable against grain coarsening, even when close to the equilibrium melting point. The polycrystalline samples also exhibit a strength in the vicinity of the theoretical value.


2015 ◽  
Vol 641 ◽  
pp. 278-285
Author(s):  
Jacek Skiba ◽  
Adam Dominiak ◽  
Tomasz S. Wiśniewski ◽  
Wacek Pachla ◽  
Mariusz Kulczyk ◽  
...  

The study is aimed at comparing the changes which occur in the microstructure and thermo-physical properties of pure copper (99.9%) and when copper alloyed with chromium and zirconium subjected to severe plastic deformation (SPD). The plastic deformation techniques employed were hydrostatic extrusion (HE), equal channel angular pressing (ECAP), and a combination of these two processes. The materials thus obtained had an ultra-fine-grained structure with the thermo-physical properties differing from those of the untreated materials. It appeared that there is a correlation between the deformation method employed and the thermo-physical properties of the materials, such as diffusivity and specific heat.


2010 ◽  
Vol 64 (4) ◽  
pp. 524-527 ◽  
Author(s):  
X.X. Xu ◽  
F.L. Nie ◽  
J.X. Zhang ◽  
W. Zheng ◽  
Y.F. Zheng ◽  
...  

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3995 ◽  
Author(s):  
Radosław Łyszkowski ◽  
Magdalena Łazińska ◽  
Dariusz Zasada

A new cross-channel extrusion (CCE) method with the application of a back pressure (BP) is proposed and experimentally tested. The introduction of pressure blocks the free flow of material by using an additional set of pistons, which prevents the loss of consistency. The paper presents results of experimental trials of CCE process. Between one and eight passes of CCE with and without a BP were applied to pure copper billets to refine their initial coarse-grained microstructure at room temperature. It was found that processing by CCE results in the formation of a lamellar structure along the extruded axis and the fine-grained structure in the remaining volume. The material exhibited dynamic recrystallization, which results in the formation of 0.5- to 2-μm grains after one pass and 2- to 8-μm grains after four CCE passes. The fine-grained material had YS of 390-415 MPa. An increase in the microhardness from 70 to 130 HV02 after one pass and then a decrease after four passes were observed. This might indicate that secondary recrystallization and selective grain growth occur, because an exothermic peak (158.5 °C, 53 ± 2.1 J/mol) was observed during DSC (differential scanning calorimetry) testing. The resistivity of the once deformed copper significantly decreases, while its further processing causes the resistivity to increase.


2008 ◽  
Vol 22 (09n11) ◽  
pp. 1103-1110
Author(s):  
M. GONG ◽  
V. P. W. SHIM ◽  
L. M. YANG ◽  
F. CHEN

An experimental investigation is undertaken to examine the possibility of producing ultra-fine grained bulk material through high-speed impact compression followed by annealing. A gas gun was employed to impose high-rate deformation on oxygen-free high-conductivity copper specimens to 90% strain. Samples were also quasi-statically compressed to identical final strains and similar heat treatment. Results show that after impact compression, grain boundaries widen and become less sharply defined, and many narrow twins are formed. For dynamic loading, grain boundary slip appears to accompany dislocation movement. Two dislocation characteristics were identified and the dislocation density was lower than that in samples compressed quasi-statically. Small dislocation loops were also observed. Portions of grains in specimens subjected to impact were mechanically broken into sizes less than 1 μm before annealing. The microhardness of impacted and statically compressed samples increased respectively by HV50 and HV60. After annealing at 190°C for 1 hour, ultra-fine grains with grain sizes ranging from 40∼200 nanometers were observed in impacted samples. This study highlights the potential of utilizing impact compression to produce bulk material with ultra-fine grains.


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