scholarly journals Influence of Harvest Term on the Content of Carvacrol, p-Cymene, γ-Terpinene and β-Caryophyllene in the Essential Oil of Satureja montana

2014 ◽  
Vol 42 (2) ◽  
pp. 392-397 ◽  
Author(s):  
Aneta WESOŁOWSKA ◽  
Monika GRZESZCZUK ◽  
Dorota JADCZAK

The aim of the studies was to determine the optimal term of harvest for Satureja montana L. (winter savory) in order to obtain the essential oil rich in antioxidative compounds such as carvacrol, p-cymene, γ-terpinene and β-caryophyllene. Essential oils of S. montanaaerial parts were obtained by hydrodistillation in Deryng-type apparatus and analyzed by gas chromatography/mass spectrometry (GC/MS). In total, 30 compounds were identified in the savory volatile oil under different harvesting terms (before flowering, during flowering and after the flowering), that represented 94.61 to 97.55% of the oils. The major components were carvacrol (65.43 to 69.99%), its precursors: p-cymene (3.69 to 9.69%) and γ-terpinene (1.51 to 5.92%) as well as β-caryophyllene (2.74 to 4.71%). Moreover, the term of harvest had a significant effect on the content of main essential oil constituents. The highest concentrations of carvacrol, γ-terpinene and β-caryophyllene were observed in the herb collected before flowering, while the highest amounts of p-cymene were noted after the flowering.

2014 ◽  
Vol 2014 ◽  
pp. 1-9 ◽  
Author(s):  
Deribachew Bekana ◽  
Tesfahun Kebede ◽  
Mulugeta Assefa ◽  
Habtemariam Kassa

Oleogum resins of B. papyrifera, B. neglecta, and B. rivae were collected from northwestern, southern, and southeastern Ethiopia, and their respective methanol extracts and essential oils were extracted and analyzed by gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS). The investigation on essential oils led to the identification of 6, 7, and 8 constituents for B. papyrifera, B. neglecta, and B. rivae, respectively. The essential oil of B. papyrifera is mainly characterized by the presence of octyl acetate (57.1–65.7%) and n-octanol (3.4–8.8%). B. neglecta is rich in α-pinene (32.6–50.7%) followed by terpinen-4-ol (17.5–29.9%) and α-thujene (12.7–16.5%), whereas B. rivae was predominated by α-pinene (32.5–66.2%) followed by p-cymene (5.7–21.1%) and limonene (1.1–19.6%). Methanol extracts of the three Boswellia species were found to consist of diterpines (incensole, incensyl acetate and verticilla-4(20),7,11-triene), triterpenes (β-amyrin, α-amyrin, β-amyrenone, and α-amyrenone), nortriterpenes (24-noroleana-3,12-diene and 24-norursa-3,12-diene), and α-boswellic acid. The investigation on the methanol extract showed that only B. papyrifera contains diterpenes and nortriterpenes, whereas B. rivae and B. neglecta consist of only triterpenes. The results indicate that the three Boswellia species were characterized by some terpenes and these terpenoic constituents could be recognized as chemotaxonomical markers for each species.


2007 ◽  
Vol 2 (11) ◽  
pp. 1934578X0700201 ◽  
Author(s):  
Mostepha Dahia ◽  
Hocine Laouer ◽  
Adel N. Chaker ◽  
Soizic Prado ◽  
Uwe J. Meierhenrich ◽  
...  

The chemical composition of the essential oil of Pituranthos chloranthus ssp. cossonianus Maire (Apiaceae) was investigated by gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS) to reveal 54 compounds. The main constituents were myristicine (27.4%), limonene (15.8%), α-pinene (11.4%), and α-phellandrene (8.3%). The antibacterial activity of the oil was evaluated against several strains and was shown to be significant against Pseudomonas aeruginosa.


2004 ◽  
Vol 1 (3) ◽  
pp. 301-303 ◽  
Author(s):  
Betül Demirci ◽  
Dietrich H. Paper ◽  
Fatih Demirci ◽  
K. Hüsnü Can Başer ◽  
Gerhard Franz

The essential oil ofBetula pendulaRoth. buds was obtained using both hydrodistillation and microdistillation techniques and their chemical compositions were analyzed using both gas chromatography (GC) and gas chromatography–mass spectrometry (GC-MS). Overall, more than 50 compounds were identified representing 80% and 92% for hydrodistillation and microdistillation, respectively. The main components (by hydrodistillation and microdistillation, respectively) found were α-copaene (12% and 10%), germacrene D (11% and 18%) and δ-cadinene (11% and 15%) in the analyzed essential oils. The microdistillation technique proved to be a useful tool and compliant alternative when compared to hydrodistillation.


2014 ◽  
Vol 997 ◽  
pp. 136-139
Author(s):  
Dong Hai Huang ◽  
Fa Song Wang ◽  
Yun He Li ◽  
Jia Gui Xiang

The essential oil from the twig of Litsea mollis was isolated using hydrodistillation in a Clevenger-type apparatus, and characterized by gas chromatography–mass spectrometry (GC-MS). A total of 39 compounds were identified, representing 89.27% of the oil. Among the twig oil compounds, oxygenated monoterpenes (39.06%) and sesquiterpene hydrocarbons (36.62%) were predominant (75.68% in total). Among the oxygenated monoterpenes, eucalyptol (9.9%), (R)-citronellol (7.23%), (R)-citronellal (7.0%), and (Z)-citral (5.03%) were the major compounds. Of the sesquiterpene hydrocarbons, β-caryophyllene (7.96%), (-)-α-panasinsene (6.31) and à-Caryophyllene (6.28%) were the main components.


2005 ◽  
Vol 60 (1-2) ◽  
pp. 25-29 ◽  
Author(s):  
Ana P. Murray ◽  
María A. Frontera ◽  
María A. Tomas ◽  
María C. Mulet

The essential oil composition from the aerial parts of three Anacardiaceae growing in Bahía Blanca, Argentina was studied by gas chromatography and gas chromatography-mass spectrometry. The essential oils of S. longifolia and S. fasciculata have been studied for the first time. The major constituents were α-pinene (46.5%), β-pinene (15.1%) and α-phellandrene (10.1%) for S. longifolia and limonene (10.9%), β-phellandrene (6.16%) and α-phellandrene (5.6%) for S. fasciculata. The major components of the essential oil of S. areira were limonene (28.6%), α-phellandrene (10.1%), sabinene (9.2%) and camphene (9.2%) differing from the literature data. The essential oils from S. areira and S. longifolia exhibited a high biotoxicity in a brine shrimp assay with Artemia persimilis.


2016 ◽  
Vol 70 (12) ◽  
Author(s):  
Paulius Kaškonas ◽  
Žydrūnas Stanius ◽  
Vilma Kaškonienė ◽  
Kȩestutis Obelevičius ◽  
Ona Ragažinskienė ◽  
...  

AbstractThis study describes the analysis of total hops essential oils from 18 cultivated varieties of hops, five of which were bred in Lithuania, and 7 wild hop forms using gas chromatography-mass spectrometry. The study sought to organise the samples of hops into clusters, according to 72 semi-volatile compounds, by applying a well-known method,


2012 ◽  
Vol 7 (1) ◽  
pp. 1934578X1200700
Author(s):  
Xiaoying Zhou ◽  
Qian Yu ◽  
Haiyan Gong ◽  
Shuge Tian

The essential oils of Ziziphora clinopodioide Lam. from four different production areas (Banfang ditch; Altay mountains; Tuoli; Terks) were investigated. The oils were extracted by hydro-distillation and analyzed by gas chromatography-mass spectrometry (GC-MS). Seventeen constituents were identified in the essential oil from Banfang ditch, 20 in that from the Altay mountains, 12 in the Tuoli essential oil, and 9 in the Terks sample. The major components of the oils were pulegone (67.6%, 32.5%, 86.4%, and 82.1%) and p-menthanone (14.8%, 43.7%, 3.2%, and 8.2% from the Banfang ditch, Tuoli, Altay mountains, and Terks samples, respectively).


2014 ◽  
Vol 997 ◽  
pp. 132-135
Author(s):  
Fa Song Wang ◽  
Yun He Li ◽  
Dong Hai Huang ◽  
Jia Gui Xiang

The essential oil from the Root Bark of Litsea mollis was isolated using hydrodistillation in a Clevenger-type apparatus, and characterized by gas chromatography–mass spectrometry (GC-MS). A total of 31 compounds were identified, representing 95.22% of the oil. The main components identified were (R)-citronellal (39.9%), (R)-citronellol (13.63%), (Z)-citral (11.5%) and β-caryophyllene (5.78%).


2013 ◽  
Vol 8 (4) ◽  
pp. 1934578X1300800 ◽  
Author(s):  
Nor Akmalazura Jani ◽  
Hasnah Mohd. Sirat ◽  
NorAzah Mohamad Ali ◽  
Azrina Aziz

The chemical compositions of the essential oil of the rhizome, leaf and stem of Hornstedtia leonurus Retz., collected from Negeri Sembilan, Malaysia, are reported for the first time. The essential oils were extracted using hydrodistillation and analyzed by gas chromatography (GC-FID) and gas chromatography/mass spectrometry (GC/MS). Seventeen (96.4%), thirteen (89.2%) and nine components (98.8%) were successfully identified from the rhizome, stem and leaf oils, respectively. Phenylpropanoids were found to be the major fraction, with methyleugenol being the most abundant compound in all oils with percentage compositions of 76.4% (rhizome), 80.3% (stem) and 74.5% (leaf).


2011 ◽  
Vol 6 (5) ◽  
pp. 1934578X1100600 ◽  
Author(s):  
Farukh S. Sharopov ◽  
William N. Setzer

The chemical composition of the essential oils of Ziziphora clinopodioides Lam. from the aerial flowering parts, collected during two different years, were obtained by hydrodistillation and analyzed by gas chromatography – mass spectrometry. Forty-five components representing 100% and 94.7% of the total oil were identified. The main constituents of the essential oils were pulegone (72.8 and 35.0%), neomenthol (6.5 and 23.1%), menthone (6.2 and 13.3%), p-menth-3-en-8-ol (1.7 and 3.5%), piperitenone (2.6 and 1.1%) and piperitone (0.7 and 1.2%). A cluster analysis was carried out on the essential oil compositions of Z. clinopodioides.


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