scholarly journals Determination of CaCO3 and SiO2 content in the binders of historic lime mortars

2011 ◽  
Vol 45 (6) ◽  
pp. 841-849 ◽  
Author(s):  
Elif Uğurlu Sağın ◽  
Hasan Böke ◽  
Nadir Aras ◽  
Şerife Yalçın
Keyword(s):  
2022 ◽  
Vol 55 (1) ◽  
Author(s):  
Markssuel T. Marvila ◽  
Afonso R. G. de Azevedo ◽  
Ruan L. S. Ferreira ◽  
Carlos Maurício F. Vieira ◽  
Jorge de Brito ◽  
...  
Keyword(s):  

2014 ◽  
Vol 897 ◽  
pp. 135-138 ◽  
Author(s):  
Eva Navrátilová ◽  
Pavla Rovnaníková

The article deals with the assessment of three brick powders. Their properties are evaluated on the basis of their pozzolanic activity, specific surface area and amorphous area. The brick powders were used in amounts of 20 and 40% as a substitute for binder in lime mortars. The influence of the powders on the properties of the modified plasters in a hardened state was evaluated via the determination of strength characteristics. It was found that not all brick powders are suitable for use in modified lime mortars.


2013 ◽  
Vol 40 (1) ◽  
pp. 33-41 ◽  
Author(s):  
Danuta Michalska ◽  
Anna Pazdur ◽  
Justyna Czernik ◽  
Małgorzata Szczepaniak ◽  
Marta Żurakowska

AbstractLime mortars may contain carbon from different origins. If the mortars are made of totally burnt lime, radiocarbon dating yields the true age of building construction. The presence of carbonaceous aggregates gives the so-called dead carbon effect, which may generate older ages. Another source of carbon is charcoal present in mortars. An attempt has been made to apply the radiocarbon method to mortars of archaeologically estimated age from the Dead Sea region. Petrographical analyses of these samples show the carbonaceous character of the binder and large amounts of limestone aggregate. Determination of the mineral composition of the mortars and comparison with the geology of the surrounding, allows the provenance of the raw materials to be identified. They probably represent the Cretaceous rocks of the Judea Group.Separate radiocarbon dates were made on bulk mortar samples, binder, charcoal fragments and separated fractions from mortars. In the case of binder-aggregate mixture the reservoir effect correction has been applied.


2018 ◽  
Vol 20 (suppl 2) ◽  
pp. 819-825
Author(s):  
Gustavo Henrique Nalon ◽  
Roseli Oliveira Guedes Martins ◽  
Rita de Cássia Silva Sant'Ana Alvarenga ◽  
Gustavo Emilio Soares de Lima ◽  
Leonardo Gonçalves Pedroti ◽  
...  

2015 ◽  
Vol 1100 ◽  
pp. 17-20
Author(s):  
Radek Ševčík ◽  
Petr Šašek ◽  
Marta Pérez-Estébanez ◽  
Alberto Viani

The characterization of historic lime mortars is crucial for many cultural heritage conservation issues. In this work, the characterization of a historical lime mortar is described. Samples for chemical analysis were obtained after different milling times and using the RILEM acid digestion method on several replicates. Qualitative and quantitative determination of phases in the mortar and in the residues after acid attack and the potential presence of CaCO3 polymorphs, were accomplished with X-ray powder diffraction. Results suggest that representativeness of the sample and the homogenisation, although not always achievable in conservation practice, are strongly affecting results.


2010 ◽  
Vol 177 ◽  
pp. 478-480
Author(s):  
Jian Ping Xu

The co-volatilization of boron and silicon has been studied for determination of SiO2 content in boron-containing silica refractories. The co-volatilization of boron may cause positive interference for determining of SiO2 content. The interference can be eliminated by the volatilization of boron with 5mL and 2mL of ethanol by separately volatizing, before volatilization of SiO2 with hydrofluoric acid. The method for determination of SiO2 content in boron-containing silica refractories has been established. The scope and precision of this method are equaled to that of the conventional method by hydrofluoric acid gravimetry.


2019 ◽  
Vol 800 ◽  
pp. 235-239
Author(s):  
Inta Kirilovica ◽  
Margarita Karpe ◽  
Inta Vitina ◽  
Viktorija Sucevana

This study deals with the restoration of columns of the VEF Culture Palace. A complete restoration of the building was performed in 2016–2017 [1]. The methodology of physico-chemical investigation of the stone materials of two facade columns includes visual observation, granulometric analyses, classic wet chemical analyses, XRD and determination of soluble salts’ content. The data obtained indicate, that for rendering of columns dolomitic and calcitic lime mortars were used. An efflorescence of sulphates on the bricks’ surface is observed.


2006 ◽  
Vol 444 (2) ◽  
pp. 179-189 ◽  
Author(s):  
R.M.H. Lawrence ◽  
T.J. Mays ◽  
P. Walker ◽  
D. D’Ayala

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