Determination of carbonation profiles in non-hydraulic lime mortars using thermogravimetric analysis

2006 ◽  
Vol 444 (2) ◽  
pp. 179-189 ◽  
Author(s):  
R.M.H. Lawrence ◽  
T.J. Mays ◽  
P. Walker ◽  
D. D’Ayala
Keyword(s):  
Thermogravimetric Analysis ◽  
Hydraulic Lime ◽  
Lime Mortars

Characterization of Different Types of Biomass Wastes Using Thermogravimetric and ICP-MS Analyses

2020 ◽  
Vol 70 (12) ◽  
pp. 4594-4600
Keyword(s):  
Thermogravimetric Analysis ◽  
Food Industry ◽  
Wood Waste ◽  
Biomass Ash ◽  
Minor Elements ◽  
Ms Analysis ◽  
Icp Ms ◽  
Different Types

The purpose of this study was to characterize some types of biomass wastes resulted from different activities such as: agriculture, forestry and food industry using thermogravimetric and ICP-MS analyses. Also, it was optimized an ICP-MS method for the determination of As, Cd and Pb from biomass ash samples. The ICP-MS analysis revealed that the highest concentration of metals (As, Cd, Pb) was recorded in the wood waste ash sample, also the thermogravimetric analysis indicated that the highest amount of ash was obtained for the same sample (26.82%). The biomass wastes mentioned in this study are alternative recyclable materials, reusable as pellets and briquettes. Keywords: ash, biomass, ICP-MS, minor elements, TG

Influence of Sample Thickness and Capping on Characterization of Bedding Mortars from Historic Masonries by Double Punch Test (DPT)

2014 ◽  
Vol 624 ◽  
pp. 322-329 ◽  
Author(s):  
Enrico Sassoni ◽  
Elisa Franzoni ◽  
Claudio Mazzotti
Keyword(s):  
Compressive Strength ◽  
Poor Quality ◽  
Sample Thickness ◽  
Mortar Sample ◽  
Hydraulic Lime ◽  
Punch Test ◽  
Natural Hydraulic Lime ◽  
Wide Range ◽  
Surface Capping

For determination of compressive strength of bedding mortar used in historic masonries, a promising moderately-destructive technique is double punch test (DPT). DPT consists of loading prismatic samples of mortar (about 4×4×1 cm3) by means of two circular steel platens (typically 2 cm diameter) and then calculating mortar compressive strength as the ratio of the failure load to the cross section of the circular platens. In this study, the influence of mortar sample thickness and mortar sample capping on the reliability of results obtained by DPT was systematically investigated. The influence of sample thickness was assessed by comparing DPT results obtained for samples with 5, 10, 15 and 20 mm thickness with compressive strength determined by testing reference 4 cm-side cubes. Different mortars were considered (cement, lime-cement, natural hydraulic lime), in order to investigate a wide range of mortar mechanical characteristics. The influence of surface capping was evaluated on a lime-cement mortar by comparing compressive strength determined on reference cubes with strength obtained by DPT on proper samples, without capping and after capping with rubber, gypsum and cement. The results of the study indicate that sample thickness substantially influences mortar compressive strength determined by DPT, which may vary by up to three times depending on sample thickness. A good estimation of the actual mortar compressive strength was obtained when samples with thickness similar to the loading platens diameter were tested, which suggests that choosing the size of the loading platens for DPT based on the thickness of mortar joints under investigation may be an effective way for obtaining reliable estimations. As for the influence of surface capping, in those cases where no mortar sample regularization is possible, because of the poor quality of the mortar, the results of the study indicate that sample capping actually seems necessary in order to avoid significant underestimations of mortar compressive strength. Considering the higher practicality offered by gypsum with respect to rapid-setting cement for surface capping, the use of gypsum seems preferable.

scholarly journals Prediction of regional agro-industrial wastes characteristics by thermogravimetric analysis to obtain bioenergy using thermal process

2018 ◽  
Vol 37 (1) ◽  
pp. 544-557 ◽  
Author(s):  
Alejandra Saffe ◽  
Anabel Fernandez ◽  
Germán Mazza ◽  
Rosa Rodriguez
Keyword(s):  
Thermogravimetric Analysis ◽  
Analysis Data ◽  
Proximate Analysis ◽  
Industrial Wastes ◽  
Heating Value ◽  
Application Range ◽  
High Heating Value ◽  
One Step ◽  
Standard Techniques

The use of energy from biomass is becoming more common worldwide. This energy source has several benefits that promote its acceptance; it is bio-renewable, non-toxic and biodegradable. To predict its behavior as a fuel during thermal treatment, its characterization is necessary. The experimental determination of ultimate analysis data requires special instrumentation, while proximate analysis data can be obtained easily by using common equipment but, the required time is high. In this work, a methodology is applied based on thermogravimetric analysis, curves deconvolution and empirical correlations for characterizing different regional agro-industrial wastes to determine the high heating value, the contents of moisture, volatiles matter, fixed carbon, ash, carbon, hydrogen, oxygen, lignin, cellulose and hemicellulose. The obtained results are similar to those using standard techniques, showing the accuracy of proposed method and its wide application range. This methodology allows to determine the main parameters required for industrial operation in only in one step, saving time.

scholarly journals Influence of the addition of carbon fibers on the properties of hydraulic lime mortars: comparison with glass and basalt fibers

2020 ◽  
Vol 70 (340) ◽  
pp. 229
Author(s):  
A. Bustos ◽  
E. Moreno ◽  
F. González ◽  
A. Cobo
Keyword(s):  
Carbon Fibers ◽  
Negative Impact ◽  
Void Content ◽  
Historic Buildings ◽  
Basalt Fibers ◽  
Architectural Heritage ◽  
Hydraulic Lime ◽  
Lime Mortars ◽  
Air Void ◽  
Mechanical Strengths

In recent years, the use of hydraulic lime in conservation and restoration of historic buildings has increased due to the pathological processes involved in the use of Portland cement. This investigation deter­mines the properties of hydraulic lime mortars with added carbon fibers for their possible use in restoration of architectural heritage. The results obtained are compared with mortars to which glass and basalt fibers have been added. The results show that the fibers affect significantly the behaviour of the mortar. Although the fibers have a negative impact in the workability and increase the air void content, they improve significantly the mechanical strengths. Although no relevant differences have been found in the pre-cracking behaviour, it has been proven that the fibers avoid a fragile behaviour of the mortar, showing a better post-cracking behaviour. Mortars with carbon fibers are the ones that show the best performance, increasing the toughness up to 12080% over the reference mortars.

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