scholarly journals The Petrographic Analysis of Sherds from the Musgano Site (41RK19), Rusk County, Texas

Author(s):  
Steve A. Tomka ◽  
Lori B. Love ◽  
Timothy K. Perttula

Characterizing the mineralogical composition of ceramic vessels and sherds from Caddo sites in East Texas by means of petrographic analysis provides a unique opportunity to gather and investigate empirical evidence from ceramic vessels on: (1) technological and manufacturing practices, and (2) their trade and exchange at varying scales conducted by ancestral Caddo people with their neighbors, both near and far (i.e., other ancestral Caddo groups as well as non-Caddo communities). This evidence in turn can be used to explore changes in the nature of social and economic relationships between particular Caddo groups and other prehistoric populations. Identified compositional and paste differences that have been recognized between the different wares made by Caddo groups (i.e., plain wares, utility wares, and fine wares) can also be employed to explore functional and technological differences in vessel function and form. It is important to build on existing petrographic studies of Caddo vessels and vessel sherds by examining unstudied assemblages to (1) better clarify the compositional nature of these ceramic wares across the Caddo temporal and geographic landscape; (2) to help pinpoint other ceramic manufacturing locales and mineralogical compositional groups, but also to assess their apparent technological complexity; and (3) lead to better evaluations of the regional character of prehistoric and historic Caddo trade and interaction networks that existed, and more definitively establish whether there were changes through time in the direction and intensity of local and long distance trade and interaction. The disparate pieces of information contained within the sherds and vessel fragments of Caddo ceramics found on many prehistoric and early historic sites throughout the region have the potential to address these questions and research issues, and can contribute unique information concerning those relationships that existed in the distant (and not-so-distant) past between Caddo farmers. Twenty decorated sherds from the Musgano ceramic assemblage curated at the Texas Archeological Research Laboratory at The University of Texas at Austin (TARL) were selected for petrographic analysis. The sherds were split and one of the remaining fragments of each pair was used for the production of thin sections. Originally, the other half of each sherd was to be submitted for instrumental neutron activation analysis, but such analyses were not done; the remaining sherd fragment was returned for continued curation at TARL. Upon the receipt of the thin sections, they underwent petrographic analysis as reported on herein. The 20 sherds include sherds from engraved fine wares (n=8, 40 percent)—bottles and carinated bowls— as well as sherds from utility wares (n=12, 60 percent). The utility wares have brushed-appliqued, incised, incised-punctated (from Maydelle Incised, Weches Fingernail Impressed, and Washington Square Paneled vessels), and punctated decorative elements. Ten percent of the sherds are from bone-tempered vessels, based on macroscopic examination, while the others are from grog-tempered vessels.

Author(s):  
Timothy K. Perttula ◽  
Robert Z. Selden

Characterizing the chemical and mineralogical composition of ceramic vessels and sherds from Woodland and Caddo sites by means of instrumental neutron activation analysis (INAA) and petrographic analysis provides a unique opportunity to gather and investigate empirical evidence from ceramic vessels (and perhaps their contents?) on their trade and exchange at varying scales conducted by ancestral Caddo people with their neighbors, both near and far (i.e., other ancestral Caddo groups as well as non-Caddo communities). This evidence in turn can be used to explore changes in the nature of social and economic relationships between particular Caddo groups and other prehistoric populations. Identified compositional and paste differences that have been identified between the different wares made by Caddo groups (i.e., plain wares, utility wares, and fine wares) have also been employed to explore functional and technological differences in vessel function and form.


Author(s):  
Timothy Perttula ◽  
Julian Sitters

Late Caddo period sites belonging to the Frankston phase (ca. A.D. 1400-1680) and the Historic Caddo Allen phase (ca. A.D. 1680-1800) are common in the upper Neches River basin in East Texas, including habitation sites as well as associated and unassociated cemeteries. As is well known, ancestral Caddo cemeteries have burial features with associated funerary offerings, most commonly ceramic vessels. In this article, we document 34 ancestral Caddo ceramic vessels in the collections of the Texas Archeological Research Laboratory at The University of Texas at Austin (TARL) from six different sites in the upper Neches River basin, including the Ballard Estates (41AN53, n=4 vessels), O. L. Ellis (41AN54, n=15), Lee Ellis (41AN56, n=1), Dabbs Estate (41AN57, n=3), A. H. Reagor (41CE15, n=3), and John Bragg (41CE23, n=8 vessels) sites. Our first purpose is to put on record these ceramic vessels from six poorly known ancestral Caddo sites in order to better understand the history of Caddo settlement in the upper Neches River basin, including the history of burial interments at these sites. The second purpose is much broader, and is part of an effort to establish an East Texas Caddo ceramic vessel database that can be employed for a variety of research purposes. The synthesis of the stylistically diverse Caddo ceramic wares in different recognized ancestral communities across the Caddo area, including the upper Neches River basin occupied by a Hasinai Caddo group, would seem to be tailor-made for studies of ancestral Caddo social networks and social identities that rely on large regional ceramic datasets. The formal and statistical assessment of the regional variation in Caddo ceramic assemblages is currently being assembled in a Geographic Information System by Robert Z. Selden, Jr. (Stephen F. Austin State University), and the assemblages include the vessels from the six sites discussed herein. This is based on the delineation of temporal and spatial divisions in the character of Caddo ceramics (i.e., principally data on decorative methods, vessel forms, defined types and varieties, and the use of different tempers) across East Texas sites and other parts of the Caddo area, and then constructing networks of similarities between ceramic assemblages from these sites that can be used to assess the strength of cultural and social relationships among Caddo communities in the region through time and across space. The identification of such postulated relationships can then be explored to determine the underlying reasons for the existence of such relationships, including factors such as the frequency of interaction and direct contact between communities, the trade and exchange of ceramic vessels, population movement, and similarities in the organization of ceramic vessel production. In conjunction with a database on 2D/3D-scanned Caddo ceramic vessels from East Texas sites, the East Texas Caddo ceramic vessel database is made part of a digital database where comprehensive mathematical and quantitative analyses of morphological attributes and decorative elements on vessels can be conducted. Queries to such a combined database of vessels and sherds should lead to better understandings of regional Caddo ceramic stylistic and technological attributes and their spatial and temporal underpinnings. The results of past and current instrumental neutron activation analysis (INAA) and petrographic analysis of Caddo Area ceramics, including East Texas (where there is a robust INAA database) can also be explored as a means to corroborate production locales, and establish the chemical and paste characteristics of local fine ware and utility ware ceramics in assemblages of different ages. These in turn allow the evaluation of the possible movement of ceramic vessels between different Caddo communities in East Texas and the broader Caddo world.


LITOSFERA ◽  
2019 ◽  
pp. 228-241
Author(s):  
A. K. Vishnyakov ◽  
M. S. Vafina ◽  
V. I. Poklonov

Research subject. In this research, we set out to investigate polyhalite-containing rocks of the Southern Urals. The purpose of this study was to characterize the patterns of formation and transformation of polyhalite-containing rocks, as well as to identify conditions leading to their destruction. Materials and methods. We studied available literature and archive materials on the southern Urals, as well as core samples. Samples for thin sections were taken from the core of polyhalite-containing rocks. The sections were manufactured (where possible) in 2 mutually perpendicular cuts relative to the axis of the monolithic core sample. Considering a high solubility of salt minerals (halite) and the possibility of converting other minerals in aqueous media (e.g., polyhalite into gypsum due to the leaching of K and Mg cations herefrom), thin sections were manufactured in anhydrous liquids (kerosene, transformer oil). In order to determine the mineralogical composition, as well as the structural and textural features of the polyhalite-containing rocks under study, a petrographic analysis of the thin sections was carried out optically using a Polam-213 microscope. Geological sections were built using Corel Draw 13. To this end, geophysical data (gamma-ray logging) and lithological composition were studied.Results. It is found that pelitomorphic sulphate clusters transform into polyhalites followed by their further recrystallization into crystalline accretions. The diagenetic nature of this process is presumed. The location of polyhalite mineralization in the rocks under study confirms the effect of the basin bottom paleorelief on the intensity of polyhalite material accumulation. Conditions determining further destruction of these rocks were formed in local areas under the influence of various geological processes. Conclusion. The results of our research can be used for predicting zones rich in polyhalites in the southern Cis-Urals.


1987 ◽  
Vol 52 (3) ◽  
pp. 595-607 ◽  
Author(s):  
Owen K. Mason ◽  
Jean S. Aigner

By comparing thin sections of basalt artifacts from three early and middle Holocene Aleutian sites with geological samples, we can infer the location of the artifactual rock source or sources. Contrary to the sources, the comparison shows that the basalt artifacts came from a single flow or closely related flows 15-30 km from all three sites. This finding suggests we should reassess the role of cultural continuity, trade, and exchange in the early and middle Holocene of the Aleutians.


2020 ◽  
Vol 322 ◽  
pp. 01025
Author(s):  
Aneta Antolik ◽  
Daria Jóźwiak-Niedźwiedzka ◽  
Kinga Dziedzic ◽  
Karolina Bogusz ◽  
Michał A. Glinicki

Alkali silica reaction (ASR) is a harmful phenomenon occurring as a result of chemical interactions between sodium and potassium hydroxides in the pore solution and reactive minerals contained in the aggregate. Reactive minerals like microcrystalline, cryptocrystalline or strained quartz dissolve in the alkaline solution and form an expansive gel product. Proper selection of concrete constituents is necessary to ensure the durability of concrete structures. The proper recognition of the aggregate mineralogical composition is a very important element in the process of selection of concrete components due to the risk of ASR occurrence. This paper presents the results of detailed microscopic analysis of alkali-silica reactivity of domestic fine aggregates of various origins. Six siliceous sands from different locations in Poland and one limestone sand were tested. Detailed petrographic analysis was performed on thin sections. In all siliceous sands micro- and cryptocrystalline quartz was recognized as a reactive mineral. Digital image analysis was performed for quantitative assessment of the potential of reactivity of sands. It revealed, that siliceous river sands were the most susceptible to an alkali-silica reaction, which was confirmed by mortar bar expansion test performed according to the standard test method.


Geosciences ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 36
Author(s):  
Vayia Xanthopoulou ◽  
Ioannis Iliopoulos ◽  
Ioannis Liritzis

The present study deals with the characterization of a ceramic assemblage from the Late Mycenaean (Late Helladic III) settlement of Kastrouli, at Desfina near Delphi, Central Greece using various analytical techniques. Kastrouli is located in a strategic position supervising the Mesokampos plateau and the entire peninsula and is related to other nearby coeval settlements. In total 40 ceramic sherds and 8 clay raw materials were analyzed through mineralogical, petrographic and microstructural techniques. Experimental briquettes (DS) made from clayey raw materials collected in the vicinity of Kastrouli, were fired under temperatures (900 and 1050 °C) in oxidizing conditions for comparison with the ancient ceramics. The petrographic analysis performed on thin sections prepared from the sherds has permitted the identification of six main fabric groups and a couple of loners. The aplastic inclusions recognized in all fabric groups but one confirmed the local provenance since they are related to the local geology. Fresh fractures of representative sherds were further examined under a scanning electron microscope (SEM/EDS) helping us to classify them into calcareous (CaO > 6%) and non-calcareous (CaO < 6%) samples (low and high calcium was noted in earlier pXRF data). Here, the ceramic sherds with broad calcium separation are explored on a one-to-one comparison on the basis of detailed mineralogical microstructure. Moreover, their microstructure was studied, aiming to estimate their vitrification stage. The mineralogy of all studied samples was determined by means of X-ray powder diffraction (XRPD), permitting us to test the validity of the firing temperatures revealed by the SEM analysis. The results obtained through the various analytical techniques employed are jointly assessed in order to reveal potters’ technological choices.


2021 ◽  
Author(s):  
Irfan Sh. Asaad ◽  

Lithostratigraphy and microfacies analysis of the Avanah Formation (Middle Eocene) were studied in the Gomaspan section in the Bina Bawi anticline, northeast of Erbil city, Kurdistan Region, Iraq. The field observations refer that the formation attains 56 m of medium to thick bedded yellow limestone, grey dolomitic limestone and blue marly dolomitic limestone interbedded with thin beds of blue marl and dark grey shale with an interval of sandy limestone in the middle part and thin to medium bedded limestone interbedded with red mudstone. The petrographic study of 29 thin sections of Avanah carbonates revealed that the majority of the matrix is carbonate mud (micrite) with few microspar. The skeletal grains include benthic foraminifera, dasycladacean green algae, ostracods, calcispheres, pelecypods, rare planktonic foraminifera and bryozoa in addition to bioclasts. Non-skeletal grains encompass peloids, oncoids, intraclasts and extraclasts with common monocrystalline quartz. Based on the field observation and petrographic analysis, three different lithostratigraphic units were identified. They are in ascending order: A-Thick bedded dolomitic marly limestone interbedded with shale. B- Bedded dolomitic limestone interbedded with shale and marl. C- Thin to medium bedded limestone interbedded with red mudstone. Depending on detailed microfacies analysis of carbonate rocks, three main microfacies and 12 submicrofacies are recognized. From the sum of all petrographic, facies, textural analyses, it is concluded that Avanah Formation in Gomaspan section, was deposited in shallow marine environment, semi restricted lagoon, in lower and upper parts and open lagoon environment in the middle part interval.


Author(s):  
Zagarzusem Ts ◽  
Baasanjav D ◽  
Sugir-Erdene N ◽  
Orgilbayar B ◽  
Sukhbat S ◽  
...  

This study investigated the effectiveness of the gravity beneficiation method based on gravitation and centrifugal forces for manganese ore. Manganese ores from Unagad deposit, samples powders were analyzed for their element and mineralogical composition using inductively coupled plasma mass spectrometry (ICP-MS) and X-ray diffractometer (XRD). Mineralogy and petrographic analysis are presented the mineralogical compositions are hydro goethite, manganese minerals and magnetite, the gangue minerals are quartz, albite, orthoclase, microcline in manganese ore. Manganese mineral occurs white, improper shape particles, weak grained-aggregates associated in gangue minerals. The most important minerals consist of manganese minerals are hausmannite, pyrolusite, rhodochrosite, and manganosite. The composite of feed containing 17.31 % Mn and 36.3 % SiO2 was produced by a centrifugal concentrator in combination with the shaking table. In the experiment, a concentrate assaying 41.37% Mn was obtained from this composite with 11.9 % yields. In the next experiment, f80=0.074mm particle size feed ore was used in the MGS concentration test. A concentrate containing 38.33 % Mn with 26.57 % yields was produced in this experiment. The results showed that it is possible to obtain concentrate on the gravity processing of manganese ore that economically significant and meet standard requirements. Манганы хүдрийг гравитацийн аргаар баяжуулах технологийн судалгаа Хураангуй:  Энэхүү судалгааны ажлаар манганы хүдрийг хүндийн хүч болон төвөөс зугтах хүчний үйлчлэл дээр үндэслэн гравитацийн аргаар баяжуулах туршилт явуулав. Унагад ордын манганы хүдрийн дээжийн элементийн найрлагыг индукцийн холбоост плазмын масс спектрометр (ICP-MS), эрдсийн найрлагыг рентген дифрактометрийн аргаар тодорхойлсон. Минералоги, петрографийн шинжилгээгээр чулуулагт гидрогётит, манганы эрдсүүд, магнетит гэсэн хүдрийн эрдсүүд, кварц, альбит, ортоклаз, микроклин зэрэг хүдрийн бус эрдсүүд тодорхойлогдлоо. Хүдрийн бус эрдэс дотор манганы эрдэс нь цагаан өнгөтэй, зөв бус хэлбэртэй мөхлөгүүд мөн сул шигтгээлэг байдлаар тааралдаж байна. Манганы эрдсүүд нь гаусманит, пиролюзит, родохрозит, манганизит хэлбэрээр агуулагдсан байна. Манганы 17.31%, цахиурын ислийн 36.3% агуулгатай анхдагч хүдрийг төвөөс зугтах хүчний сепаратор болон ширээний хосолсон аргаар баяжуулахад баяжмалын агуулга Mn-41.37%, гарц 11.9% байв. Харин -0.074 мм фракцийн агуулга 80%-тай анхдагч хүдрийг хүндийн хүчний сепаратор (MGS)–аар баяжуулж, 38.33% -ийн манган агуулсан, 26.57% -ийн гарцтай баяжмал гарган авсан. Иймд манганы хүдрийг гравитацийн аргаар баяжуулахад стандартын шаардлага хангасан эдийн засгийн ач холбогдолтой бүтээгдэхүүн гарган авах боломжтойг тогтоов. Түлхүүр үг: Манганы хүдэр, хүндийн хүчний сепаратор, төвөөс зугтах хүчний сепаратор, рентген - дифрактометр.


Author(s):  
Timothy Perttula ◽  
Kevin Stingley

In the summer of 2017, 21 ancestral Caddo ceramic vessels held since 1933 by the Gila Pueblo Museum and then by the Arizona State Museum were returned to the Texas Archeological Research Laboratory at The University of Texas at Austin (TARL). These vessels had not been properly or fully studied and documented when the University of Texas exchanged these vessels, so our purpose in documenting these vessels now is primarily concerned with determining the stylistic (i.e., decorative methods, motifs, and decorative elements) and technological (i.e., vessel form, temper, and vessel size) character of the vessels that are in the collection, and assessing their cultural relationships and stylistic associations, along with their likely age. In 1933, little was known about the cultural and temporal associations of ancestral Caddo ceramic vessels from East Texas, but that has changed considerably since that time.


Author(s):  
Timothy Perttula

In this article, I document 28 ancestral Caddo ceramic vessels from seven sites and one general collection in the whole vessel collections at the Texas Archeological Research Laboratory (TARL) at The University of Texas at Austin (UT). These sites and general collection are in Anderson and Cherokee counties in East Texas (Figure 1), specifically the: Rube Beard site (41AN18, n=2), the Edward W. Ellis site (41AN36, n=1), the Ray Lookabaugh site (41AN37, n=1), the R. E. Daly site (41AN39, n=9), the Jasper Tucker/Mrs. Joe Watkins Farm site (41AN44, n=11; see also Perttula and Selden [2015]), the W. T. Todd site (41AN52, n=1), the N. B. Ruggles site (41CE40, n=2), and one vessel from the Cherokee County general collections. The methods of ceramic vessel analysis follow those specified in Perttula (2018:2-4), among other publications on Caddo ceramic vessel documentation, methods consistently employed since the 1990s in the documentation of ancestral Caddo ceramic vessels in East Texas sites.


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