Zero Shear Viscosity Determination of Fracturing Fluids: An Essential Parameter In Proppant Transport Characterizations

Author(s):  
Mahmoud Asadi ◽  
Michael W. Conway ◽  
Robert D. Barree
SPE Journal ◽  
2020 ◽  
Vol 25 (06) ◽  
pp. 2962-2983 ◽  
Author(s):  
Zhengming Xu ◽  
Xianzhi Song ◽  
Zhaopeng Zhu

Summary Viscoelastic fluids are frequently used as drilling or fracturing fluids to enhance cuttings or proppant transport efficiency. The solid transport performance of these fluids largely depends on the settling behaviors of suspended particles. Different from viscoinelastic fluids, the elastic and viscous characteristics of viscoelastic fluids both affect particle settling behaviors. In this study, to separately quantify the contribution degrees of the shear viscosity and fluid elasticity on the terminal settling velocity, we decompose the total drag force into a viscous drag force and an elastic drag force. Based on the experimental data from the available literature, it is concluded that the elastic drag force is a function of the fluid elasticity, particle diameter, particle terminal settling velocity, and density difference between the fluid and particle. The formula for the elastic drag force is determined on the basis of the force analysis, and a relationship between the elastic drag coefficient and particle Reynolds number (Re) is developed. An explicit equation that directly predicts the terminal settling velocity in viscoelastic fluids is determined by correlating the dimensionless particle diameter and Re. To validate the proposed model, a total of 108 settling experiments in viscoelastic fluids are conducted. The absolute percentage error (APE) between the predicted and measured terminal settling velocities is 15.26%, which indicates that the proposed explicit terminal settling velocity equation can provide satisfactory prediction accuracy of the terminal settling velocity for particles in viscoelastic fluids. Furthermore, an illustrative example is provided to show that the proposed model can be used to calculate the required fluid elasticity to obtain the desired terminal settling velocity when the fluid shear viscosity is fixed. The proposed models are valid with a consistency index range of approximately 0.16 to 1.2 Pa⋅sn, flow behavior index range of approximately 0.282 to 0.579, an Re range of approximately 0.005 to 30, and a fluid relaxation time range of approximately 0.183 to 110 seconds. This study can help operators choose proper drilling/fracturing fluids to enhance the cuttings/proppant transport and maximize drilling/fracturing performance.


Polymers ◽  
2021 ◽  
Vol 13 (24) ◽  
pp. 4451
Author(s):  
Wangqing Wu ◽  
Ke Zeng ◽  
Baishun Zhao ◽  
Fengnan Duan ◽  
Fengze Jiang

Capillary rheometers have been widely used for the rheological measurement of polymer melts. However, when micro capillary dies are used, the results are usually neither accurate nor consistent, even under the same measurement conditions. In this work, theoretical modeling and experimental studies were conducted for a more profound understanding of the mechanism by which the initial and boundary conditions influence the inaccuracy in the apparent shear viscosity determination with micro capillary dies (diameters: 500 μm, 200 μm, 100 μm). The results indicate that the amount of polymer initially in the barrel, the pre-compaction pressure and the capillary die diameter have a significant influence on the development of the micro scale inlet pressure, which directly determines the accuracy of the measurement at low and medium shear rates. The varying melt compressibility was confirmed to be the main factor directly related to the inaccuracy in the micro scale apparent shear viscosity determination. It is suggested that measures such as reducing the amount of polymer initially in the barrel and increasing the pre-compaction pressure could be used to reduce the measurement inaccuracy.


1959 ◽  
Vol 32 (1) ◽  
pp. 97-98
Author(s):  
F. Bueche ◽  
S. W. Harding

Abstract It has been shown that the shear-rate dependence of the viscosity of concentrated polymer solutions can be explained in terms of known parameters of the solution. If the concentration, temperature, zero shear viscosity, and molecular weight of the polymer are known, the decrease in viscosity with increasing shear rate can be predicted. Conversely, if one measures the shear-rate dependence of the viscosity, the molecular weight may be computed. We believe this provides a convenient method for the absolute determination of molecular weights of linear, coiling, high polymers.


2009 ◽  
Vol 23 (5) ◽  
pp. 2080-2086 ◽  
Author(s):  
Szabolcs Biro ◽  
Tejash Gandhi ◽  
Serji Amirkhanian

2008 ◽  
Vol 34 (9) ◽  
pp. 923-929 ◽  
Author(s):  
Justin Pennington ◽  
Preetanshu Pandey ◽  
Henry Tat ◽  
Jennifer Willson ◽  
Brent Donovan

1988 ◽  
Vol 61 (5) ◽  
pp. 812-827 ◽  
Author(s):  
Ramesh R. Rahalkar ◽  
Henry Tang

Abstract Based upon the Doi-Edwards theory, a simple expression has been obtained for zero-shear viscosity in terms of the plateau modulus and the crossover frequency. There are no adjustable parameters in the expression. The model is in very good agreement with the zero-shear viscosity values for linear polybutadienes, the typical discrepancy being ∼5–10%. If the model can be validated for other linear amorphous polymers, it may become possible to estimate the zero-shear viscosity by measuring a single Theological parameter (the crossover frequency).


Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 3073
Author(s):  
Abbas Mukhtar Adnan ◽  
Chaofeng Lü ◽  
Xue Luo ◽  
Jinchang Wang

This study has investigated the impact of graphene oxide (GO) in enhancing the performance properties of an asphalt binder. The control asphalt binder (60/70 PEN) was blended with GO in contents of 0%, 0.5%, 1%, 1.5%, 2%, and 2.5%. The permanent deformation behavior of the modified asphalt binders was evaluated based on the zero shear viscosity (ZSV) parameter through a steady shear test approach. Superpave fatigue test and the linear amplitude sweep (LAS) method were used to evaluate the fatigue behavior of the binders. A bending beam rheometer (BBR) test was conducted to evaluate the low-temperature cracking behavior. Furthermore, the storage stability of the binders was investigated using a separation test. The results of the ZSV test showed that GO considerably enhanced the steady shear viscosity and ZSV value, showing a significant contribution of the GO to the deformation resistance; moreover, GO modification changed the asphalt binder’s behavior from Newtonian to shear-thinning flow. A notable improvement in fatigue life was observed with the addition of GO to the binder based on the LAS test results and Superpave fatigue parameter. The BBR test results revealed that compared to the control asphalt, the GO-modified binders showed lower creep stiffness (S) and higher creep rate (m-value), indicating increased cracking resistance at low temperatures. Finally, the GO-modified asphalt binders exhibited good storage stability under high temperatures.


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