scholarly journals The thermophysical properties of primary phase in lithium germanium phosphate glass

2021 ◽  
Vol 53 (3) ◽  
pp. 301-310
Author(s):  
Srdjan Matijasevic ◽  
Vladimir Topalovic ◽  
Snezana Grujic ◽  
Veljko Savic ◽  
Jelena Nikolic ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Differential Thermal Analysis ◽  
Phosphate Glass ◽  
Primary Phase ◽  
Melt Quenching ◽  
Scanning Calorimetry ◽  
Characteristic Temperatures ◽  
Xrd Method

The selected lithium germanium-phosphate glass was prepared by a conventional melt-quenching technique. The XRD method was employed to confirm the glass was obtained and to reveal crystalline phases during heat treatment. The dilatometry (DIL), differential thermal analysis (DTA), and differential scanning calorimetry (DSC) were used to determine the characteristic temperatures and enthalpies of crystallization and melting of the crystalline phase. The DTA and DIL were used to obtain the viscosity curves by applying the Vogel-Fulcher-Tammann (VFT) equation

scholarly journals A thermal degradation study of Y and La methanesulfonates

2006 ◽  
Vol 71 (8-9) ◽  
pp. 905-915
Author(s):  
Moura de ◽  
Jivaldo Matos ◽  
Farias de
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Differential Thermal Analysis ◽  
Thermal Degradation ◽  
Degradation Process ◽  
Oxide Formation ◽  
Scanning Calorimetry ◽  
Degradation Study ◽  
Thermogravimetric Data ◽  
Thermal Degradation Process

The synthesis, characterization and thermal degradation of yttrium and lanthanum methanesulfonates is reported. The prepared salts were characterized by elemental analysis and infrared spectroscopy. The thermal degradation study was performed using thermogravimetry (TG), differential thermal analysis (DTA) and differential scanning calorimetry (DSC).Using the thermogravimetric data, a kinetic study of the dehydration ofY and Lamethanesulfonates was performed employing the Coats-Redfern and Zsak?methods. It was verified that under heating, yttrium and lanthanum methanesulfonates undergo three main processes: dehydration, thermal degradation and oxide formation. Furthermore, depending on the nature of the atmosphere, i.e., inert or oxidant, the thermal degradation process could be endothermic (N2) or exothermic (air).

scholarly journals Thermal stability and thermal decomposition of sucralose

2018 ◽  
Vol 39 (4) ◽  
pp. 21
Author(s):  
Gilbert Bannach ◽  
Rafael R. Almeida ◽  
Luis G. Lacerda ◽  
Egon Schnitzler ◽  
Massao Ionashiro
Keyword(s):  
Thermal Stability ◽  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Thermal Decomposition ◽  
Differential Thermal Analysis ◽  
Infrared Spectroscopy ◽  
Scanning Calorimetry ◽  
Thermoanalytical Techniques ◽  
Thermal Stability Of

Several papers have been described on the thermal stability of the sweetener, C12H19Cl3O8 (Sucralose). Nevertheless no study using thermoanalytical techniques was found in the literature. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC) and infrared spectroscopy, have been used to study the thermal stability and thermal decomposition of sweetener.

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