scholarly journals Shear bond strength of orthodontic resins after caries infiltrant preconditioning

2012 ◽  
Vol 83 (2) ◽  
pp. 306-312 ◽  
Author(s):  
Ewelina Naidu ◽  
Bogna Stawarczyk ◽  
Pune Nina Tawakoli ◽  
Rengin Attin ◽  
Thomas Attin ◽  
...  

ABSTRACT Objective: To investigate the influence of caries infiltrant preconditioning on the shear bond strength of orthodontic resin cements on sound and demineralized enamel. Materials and Methods: Stainless-steel brackets were bonded to sound or artificially demineralized (14 d, acidic buffer, pH 5.0) bovine enamel specimens using a resin cement or a combination of caries infiltrant preconditioning (Icon, DMG) and the respective resin cement (light-curing composite: Heliosit Orthodontic, Transbond XT, using either Transbond XT Primer or Transbond Plus Self Etching Primer; light-curing resin-modified glass ionomer cement: Fuji Ortho; or self-curing composite: Concise Orthodontic Bonding System). Each group consisted of 15 specimens. Shear bond strength was evaluated after thermo-cycling (10,000×, 5°C to 55°C) at a crosshead speed of 1 mm/min, and data were statistically analyzed by analysis of variance, Mann-Whitney test, and Weibull statistics. Adhesive Remnant Index (ARI) scores and enamel fractures were determined at 25× magnification and were statistically analyzed by regression analyses (P < .05). Results: The caries infiltrant system significantly increased the shear bond strength of Transbond XT Primer, Transbond Plus Self Etching Primer, and Fuji Ortho in sound specimens, and of all resin cements except for the Concise Orthodontic Bonding System in demineralized enamel. Overall, caries infiltrant preconditioning decreased significantly the number of enamel fractures, but it did not affect ARI scores. Conclusion: Preconditioning of sound and demineralized enamel with the caries infiltrant system did not impair but rather increased the shear bond strength of most orthodontic resin cements while decreasing the risk of enamel fracture at debonding.

Materials ◽  
2018 ◽  
Vol 11 (11) ◽  
pp. 2216 ◽  
Author(s):  
Paulo Palma ◽  
Joana Marques ◽  
Rui Falacho ◽  
Alexandra Vinagre ◽  
João Santos ◽  
...  

The purpose of the present study was to assess the proper time to perform a restoration (immediately or delayed) after placement of two calcium silicate-based cements (CSCs) and to test the performance of two different restorative protocols regarding shear bond strength (SBS). Seventy-five acrylic blocks were randomly divided into five groups (n = 15). Specimens were filled with either ProRoot MTA (Dentsply Tulsa Dental) or Biodentine (Septodont). The restoration was performed at an immediate (12 min) or delayed (seven days) timeframe, using a resin-based flowable composite (SDR) (bonded to the CSC using a universal bonding system) or glass ionomer cement (GIC) as restorative materials. SBS was measured using a universal testing machine. Fractured surfaces were evaluated, and the pattern was registered. Statistical analysis was performed using the Dunn–Sidak post hoc test (P < 0.05). Biodentine/immediate SDR showed the highest mean SBS value (4.44 MPa), with statistically significant differences when compared to mineral trioxide aggregate (MTA)/GIC (1.14 MPa) and MTA/immediate SDR (1.33 MPa). MTA/GIC and MTA/immediate SDR did not present significant differences regarding SBS. No statistical differences were verified concerning mean SBS between both CSCs within the 7 day groups. MTA/delayed SDR (3.86 MPa) presented statistical differences compared to MTA/immediate SDR, whereas no differences were observed regarding Biodentine performance (Biodentine/immediate SDR and Biodentine/delayed SDR (3.09 MPa)). Bonding procedures directly on top of MTA might be preferably performed at a delayed timeframe, whereas Biodentine might allow for immediate restoration.


2017 ◽  
Vol 15 (4) ◽  
pp. 258
Author(s):  
Marcelo Giannini ◽  
Andreia Assis Carvalho ◽  
Ariovaldo Stefani ◽  
Wladimir Franco de Sá Barbosa ◽  
Lawrence Gonzaga Lopes

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.


2008 ◽  
Vol 78 (6) ◽  
pp. 1105-1109 ◽  
Author(s):  
Dong-Bum Ryou ◽  
Hyo-Sang Park ◽  
Kyo-Han Kim ◽  
Tae-Yub Kwon

Abstract Objective: To test the bonding characteristics of four flowable composites for orthodontic bracket bonding. Materials and Methods: Metal brackets were bonded to acid-etched human enamel using four flowable composites (Grandio Flow, GF; UniFil Flow, UF; UniFil LoFlo Plus, UL; and DenFil Flow, DF), an orthodontic bonding system (Transbond XT, TX), and a restorative composite (Filtek Z250, FZ). After 24 hours of storage in water at 37°C, a shear bond strength (SBS) test was performed. After debonding, the adhesive remnant index (ARI) was assessed. In addition, the flow and flexural strength of the materials were examined. Results: The SBS for the flowable composites ranged between 7.2 and 8.3 MPa, and TX showed a significantly higher value (mean 10.9 MPa). The flowable composites also demonstrated a significantly superior flowability, yet inferior flexural strength (except for DF) than TX and FZ. Two flowable composites (GF and UL) produced significantly higher ARI scores than TX and FZ, which represented a larger resin remnant on the enamel surfaces after debonding. Conclusion: When considering the SBS and ARI scores obtained in this study, flowable composites with no intermediate bonding resin could be conveniently applied for orthodontic bracket bonding.


2013 ◽  
Vol 38 (2) ◽  
pp. 186-196 ◽  
Author(s):  
Camila Sabatini ◽  
Manthan Patel ◽  
Eric D'Silva

SUMMARY Objective To evaluate the shear bond strength (SBS) of three self-adhesive resin cements and a resin-modified glass ionomer cement (RMGIC) to different prosthodontic substrates. Materials and Methods The substrates base metal, noble metal, zirconia, ceramic, and resin composite were used for bonding with different cements (n=12). Specimens were placed in a bonding jig, which was filled with one of four cements (RelyX Unicem, Multilink Automix, Maxcem Elite, and FujiCEM Automix). Both light-polymerizing (LP) and self-polymerizing (SP) setting reactions were tested. Shear bond strength was measured at 15 minutes and 24 hours in a testing device at a test speed of 1 mm/min and expressed in MPa. A Student t-test and a one-way analysis of variance (ANOVA) were used to evaluate differences between setting reactions, between testing times, and among cements irrespective of other factors. Generalized linear regression model and Tukey tests were used for multifactorial analysis. Results Significantly higher mean SBS were demonstrated for LP mode relative to SP mode (p&lt;0.001) and for 24 hours relative to 15 minutes (p&lt;0.001). Multifactorial analysis revealed that all factors (cement, substrate, and setting reaction) and all their interactions had a significant effect on the bond strength (p&lt;0.001). Resin showed significantly higher SBS than other substrates when bonded to RelyX Unicem and Multilink Automix in LP mode (p&lt;0.05). Overall, FujiCEM demonstrated significantly lower SBS than the three self-adhesive resin cements (p&lt;0.05). Conclusions Overall, higher bond strengths were demonstrated for LP relative to SP mode, 24 hours relative to 15 minutes and self-adhesive resin cements compared to the RMGICs. Bond strengths also varied depending on the substrate, indicating that selection of luting cement should be partially dictated by the substrate and the setting reaction.


2018 ◽  
Vol 6 (3) ◽  
pp. 548-553 ◽  
Author(s):  
Bandar M. A. Al–Makramani ◽  
Abdul A. A. Razak ◽  
Mohamed I. Abu–Hassan ◽  
Fuad A. Al–Sanabani ◽  
Fahad M. Albakri

BACKGROUND: The selection of the appropriate luting cement is a key factor for achieving a strong bond between prepared teeth and dental restorations.AIM: To evaluate the shear bond strength of Zinc phosphate cement Elite, glass ionomer cement Fuji I, resin-modified glass ionomer cement Fuji Plus and resin luting cement Panavia-F to Turkom-Cera all-ceramic material.MATERIALS AND METHODS: Turkom-Cera was used to form discs 10mm in diameter and 3 mm in thickness (n = 40). The ceramic discs were wet ground, air - particle abraded with 50 - μm aluminium oxide particles and randomly divided into four groups (n = 10). The luting cement was bonded to Turkom-Cera discs as per manufacturer instructions. The shear bond strengths were determined using the universal testing machine at a crosshead speed of 0.5 mm/min. The data were analysed using the tests One Way ANOVA, the nonparametric Kruskal - Wallis test and Mann - Whitney Post hoc test.RESULTS: The shear bond strength of the Elite, Fuji I, Fuji Plus and Panavia F groups were: 0.92 ± 0.42, 2.04 ± 0.78, 4.37 ± 1.18, and 16.42 ± 3.38 MPa, respectively. There was the statistically significant difference between the four luting cement tested (p < 0.05).CONCLUSION: the phosphate-containing resin cement Panavia-F exhibited shear bond strength value significantly higher than all materials tested.


2017 ◽  
Vol 16 ◽  
pp. 1-7
Author(s):  
Bruna Genari ◽  
Vicente Castelo Branco Leitune ◽  
João Henrique Macedo Saucedo ◽  
Susana Maria Werner Samuel ◽  
Fabrício Mezzomo Collares

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.


2013 ◽  
Vol 14 (1) ◽  
pp. 21-25 ◽  
Author(s):  
T Praveen Kumar Reddy ◽  
Kolasani Srinivasa Rao ◽  
Garlapati Yugandhar ◽  
B Sunil Kumar ◽  
SN Chandrasekhar Reddy ◽  
...  

ABSTRACT The acid pretreatment and use of composite resins as the bonding medium has disadvantages like scratching and loss of surface enamel, decalcification, etc. To overcome disadvantages of composite resins, glass ionomers and its modifications are being used for bonding. The study was conducted to evaluate the efficiency of resin reinforced glass ionomer as a direct bonding system with conventional glass ionomer cement and composite resin. The study showed that shear bond strength of composite resin has the higher value than both resin reinforced glass ionomer and conventional glass ionomer cement in both 1 and 24 hours duration and it increased from 1 to 24 hours in all groups. The shear bond strength of resin reinforced glass ionomer cement was higher than the conventional glass ionomer cement in both 1 and 24 hours duration. Conditioning with polyacrylic acid improved the bond strength of resin reinforced glass ionomer cement significantly but not statistically significant in the case of conventional glass ionomer cement. How to cite this article Rao KS, Reddy TPK, Yugandhar G, Kumar BS, Reddy SNC, Babu DA. Comparison of Shear Bond Strength of Resin Reinforced Chemical Cure Glass Ionomer, Conventional Chemical Cure Glass Ionomer and Chemical Cure Composite Resin in Direct Bonding Systems: An in vitro Study. J Contemp Dent Pract 2013;14(1):21-25.


Author(s):  
Ayman Mohammed Said

Purpose: To evaluate the effect of aging and different surface treatments on micro-shear bond strength of two resin cements to resin nano-ceramic composite blocks using an in-vitro study. Materials and methods: Blocks of resin nano-ceramic (Lava Ultimate, 3M, St Paul, Minnesota, USA) were used to prepare eight plates having the following dimensions: (14mm × 12mm × 2mm). After plates preparation they were assigned to two main groups according to the surface treatment applied, either hydrofluoric acid etching and silane or sandblasting and silane. Scanning electron microscope (SEM) was used to analyze the surface topography of the Lava-Ultimate plates before and after application of surface treatments. Two resin cements were used; dual cured adhesive resin cement (Bifix QM, VOCO, Cuxhafen, Germany) and dual cured self-adhesive resin cement (Bifix SE, VOCO, Cuxhafen, Germany) to create a five resin micro-cylinders received on each lava ultimate plate. Ten specimens from each subgroup were tested after 24 hours and the other ten specimens were tested after aging in saline for 6 months. Micro-shear bond strength test was applied until failure. . Multi-factorial ANOVA test and One-way ANOVA followed by pair-wise Tukey’s post-hoc tests were used to analyze the data. Results: Both resin cements showed statistically significant decrease on bond strength after aging. Before aging, both surface treatments with adhesive resin cement showed statistically significant higher micro-shear bond strength mean values than with self-adhesive resin cement. After aging sandblasting showed a statistically significant higher micro-shear bond strength mean values with adhesive resin cement, while hydrofluoric acid etching revealed a statistically non-significant higher values with adhesive resin cement than self-adhesive resin cement. Conclusion: For both surface treatments and resin cements aging had a detrimental effect on micro- shear bond strength.


2021 ◽  
pp. 232020682110502
Author(s):  
İdris Kavut ◽  
Mehmet Uğur

Aim: The aim of this study was to evaluate the effect of calcium phosphate based desensitizing agent on shear bond strength of self-etch/adhesive resin cements to dentin. Materials and Methods: Eighty dentin specimens were prepared from freshly extracted human third molar teeth and were classified, randomly ( n = 20). Half of groups were treated with calcium phosphate based Teethmate Desensitizer and then Panavia V5, RelyX Ultimate (containing self-etch primer), Panavia SA, and RelyX U200 self-adhesive resin cements were luted to all dentin surfaces. All specimens were stored in an incubator at 37°C for 24 h. Shear bond strength was tested by a universal test machine at a 0.5 mm/min crosshead speed. The data were analyzed with a statistical program. Two-way ANOVA was used for statistical differences ( P <.05). Dentin surfaces were examined with scanning electron microscopy (SEM) at x5000 and x10000 magnifications. Results: The higher shear bond values were observed in the groups with Teethmate Desensitizer applied and cemented with self-etch (16.05 ± 6.24 and 14.73 ± 4.75), whereas the lowest bonding values were observed in the groups with self-adhesive resin cement without Teethmate Desensitizer (3.73 ± 0.77 and 5.85 ± 4.19; P <.001). As the main effect of the treatment, the bond strength was 9.39 ± 6.04 in the control group, whereas it was 13.49 ± 5.44 in the Teethmate applied groups ( P <.05) Conclusions: Calcium phosphate desensitizer did not adversely effected shear bond strength of self-etch/adhesive resin cements to dentin. It even significantly increased the shear bond strength of self-adhesive resin cements.


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