scholarly journals Does surface treatment of demineralized dentin impact on shear bond strength?

2021 ◽  
Vol 6 (2) ◽  
pp. 023-028
Author(s):  
Fatemeh Rezaei ◽  
Atefeh Nemati-Karimooy ◽  
Horieh Moosavi

Aim: This study investigated the effect of various surface treatments on the bond strength of a universal adhesive to demineralized dentin. Materials and Methods: Human dentin surfaces of forty-eight carries-free maxillary premolars were prepared and demineralized by acidic solutions. Teeth were randomly distributed into four groups (n=12) getting different surface treatments. Three minutes application of a CPP‑ACP (group 1), Er: YAG laser irradiation (group 2), Er: YAG laser irradiation combined with three minutes application of CPP‑ACP (group 3), no treatment (group 4). Thereafter composite tube (Filtek TM Ultimate, 3M ESPE) bonded to the testing surfaces via universal adhesive; Single Bond Universal and the Shear Bond Strength (SBS) measured. Data were analyzed utilizing ANOVA and Tukey tests (P<0.05). Results: Only application of CPP-ACP and Er: YAG laser radiation, resulted in the highest and lowest SBS respectively (p<0.001). Bond strength after irradiation of Er: YAG laser combined with three minutes application of CPP‑ACP was a little more than laser alone. Conclusion: The application of CPP-ACP could increase the SBS of universal adhesives used to demineralized dentin. Laser irradiation application has an adverse effect on SBS.

2010 ◽  
Vol 04 (04) ◽  
pp. 367-373 ◽  
Author(s):  
Sevi Burcak Cehreli ◽  
Asli Guzey ◽  
Neslihan Arhun ◽  
Alev Cetinsahin ◽  
Bahtiyar Unver

Objectives: The aim of this in vitro study is to determine (1) shear bond strength (SBS) of brackets bonded with self-etch and total-etch adhesive after ozone treatment (2) bond failure interface using a modified Adhesive Remnant Index (ARI).Methods: 52 premolars were randomly assigned into four groups (n=13) and received the following treatments: Group 1: 30 s Ozone (Biozonix, Ozonytron, Vehos Medikal, Ankara, Turkey) application + Transbond Plus Self-Etching Primer (SEP) (3M) + Transbond XT (3M), Group 2: Transbond Plus SEP + Transbond XT, Group 3: 30 s Ozone application + 37% orthophosphoric acid + Transbond XT Primer (3M) + Transbond XT, Group 4: 37% orthophosphoric acid + Transbond XT Primer + Transbond XT. All samples were stored in deionised water at 37oC for 24 hours. Shear debonding test was performed by applying a vertical force to the base of the bracket at a cross-head speed of 1 mm/min.Results: The mean SBS results were Group 1: 10.48 MPa; Group 2: 8.89 MPa; Group 3: 9.41 MPa; Group 4: 9.82 MPa. One-Way Variance Test revealed that the difference between the groups was not statistically significant (P=0.267). Debonded brackets were examined by an optical microscope at X16 magnification to determine the bond failure interface using a modified ARI. The results were (mean) Group 1: 2.38; Group 2: 1.31; Group 3: 3.00; Group 4: 1.92. Multiple comparisons showed that Groups 1 and 2, 2 and 3, 3 and 4 were statistically different (P=0.014, P<.001 and P=0.025).Conclusions: Ozone treatment prior to bracket bonding does not affect the shear bond strength. (Eur J Dent 2010;4:367-373)


2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Zohreh Moradi ◽  
Farnoosh Akbari ◽  
Sara Valizadeh

Aim. This study aimed to assess shear bond strength (SBS) of resin cement to zirconia ceramic with different surface treatments by using Single Bond Universal. Methods. In this in vitro study, 50 zirconia discs (2 × 6 mm) were divided into 5 groups of (I) sandblasting with silica-coated alumina (CoJet)  + silane + Single Bond 2, (II) sandblasting with CoJet + Single Bond Universal, (III) sandblasting with alumina + Single Bond Universal, (IV) sandblasting with alumina + Z-Prime Plus, and (V) Single Bond Universal with no surface treatment. Resin cement was applied in plastic tubes (3 × 5 mm2), and after 10,000 thermal cycles, the SBS was measured by a universal testing machine. The mode of failure was determined under a stereomicroscope at × 40 magnification. Data were analyzed using one-way ANOVA. Results. The maximum (6.56 ± 4.29 MPa) and minimum (1.94 ± 1.96 MPa) SBS values were noted in groups III and I, respectively. Group III had the highest frequency of mixed failure (60%). Group V had the maximum frequency of adhesive failure (100%). Conclusion. Single Bond Universal + sandblasting with alumina or silica-coated alumina particles is an acceptable method to provide a strong SBS between resin cement and zirconia.


2003 ◽  
Vol 14 (2) ◽  
pp. 132-135 ◽  
Author(s):  
Claudia Minami Kussano ◽  
Gerson Bonfante ◽  
José Gilmar Batista ◽  
João Henrique Nogueira Pinto

This study evaluated the shear bond strength of porcelain/composite using 40 metal + porcelain + composite cylindrical specimens divided into 4 groups, according to porcelain surface treatment: 1) no treatment, 2) mechanical retentions performed with diamond burs, 3) etching with phosphoric acid+silane, and 4) etching with hydrofluoric acid+silane. After being stored in distilled water at room temperature for one week, the specimens were submitted to a shear force (load) and the data were analyzed statistically (ANOVA). The means (in Mpa) of the groups were: 4.71 (group 1); 4.81 (group 2); 11.76 (group 3); 11.07 (group 4). There were no statistically significant differences between groups 1 and 2 and between groups 3 and 4.


2017 ◽  
Vol 22 (4) ◽  
pp. 47-52 ◽  
Author(s):  
Marina Cumerlato ◽  
Eduardo Martinelli de Lima ◽  
Leandro Berni Osorio ◽  
Eduardo Gonçalves Mota ◽  
Luciane Macedo de Menezes ◽  
...  

ABSTRACT Objective: The aim of this in vitro study was to evaluate and compare the effects of grinding, drilling, sandblasting, and ageing prefabricated teeth (PfT) on the shear bond strength (SBS) of orthodontic brackets, as well as the effects of surface treatments on the adhesive remnant index (ARI). Methods: One-hundred-ninety-two PfT were divided into four groups (n = 48): Group 1, no surface treatment was done; Group 2, grinding was performed with a cylindrical diamond bur; Group 3, two drillings were done with a spherical diamond bur; Group 4, sandblasting was performed with 50-µm aluminum oxide. Before the experiment, half of the samples stayed immersed in distilled water at 37oC for 90 days. Brackets were bonded with Transbond XT and shear strength tests were carried out using a universal testing machine. SBS were compared by surface treatment and by ageing with two-way ANOVA, followed by Tukey’s test. ARI scores were compared between surface treatments with Kruskal-Wallis test followed by Dunn’s test. Results: Surface treatments on PfT enhanced SBS of brackets (p< 0.01), result not observed with ageing (p= 0.45). Groups II, III, and IV showed higher SBS and greater ARI than the Group 1 (p< 0.05). SBS was greater in the groups 3 and 4 (drilling, sandblasting) than in the Group 2 (grinding) (p< 0.05). SBS and ARI showed a positive correlation (Spearman’s R2= 0.57; p< 0.05). Conclusion: Surface treatment on PfT enhanced SBS of brackets, however ageing did not show any relevance. Sandblasting and drilling showed greater SBS than grinding. There was a positive correlation between SBS and ARI.


2015 ◽  
Vol 5 (2) ◽  
pp. 65-68
Author(s):  
Shruti Patil ◽  
Prajna Shetty

ABSTRACT Background The dentin desensitizers available for in-office application for prevention and/or treatment of post restorative dentinal hypersensitivity, act by blocking the open dentinal tubules. In doing so, they may influence the bond strength of the restorative resins. Thus, the aim of the study was to evaluate the effect of desensitizers on the shear bond strength of dentin adhesives and to check the extent of dentinal tubule occlusion caused by these desensitizers. Materials and Methods Sixty-four premolars were randomly divided into four groups of sixteen each. The middle depth dentin was exposed by on the buccal surface and was etched using 37% phosphoric acid and rinsed. They were assigned to, Group 1: Gluma desensitizer, Group 2: Vivasens desensitizer, Group 3: Gluma Comfort Bond and desensitizer, and Group 4: Adper Single Bond 2. Composite resin post of 2 mm in height and width were built on these specimens. The samples were then mounted in acrylic resin blocks. Universal testing machine was used to test the shear bond strength. The data were analyzed using one-way analysis of variance (ANOVA) and post hoc Tukey's test. Results The mean values of the shear bond strength were for: Group 1—18.61 ± 1.03 MPa, Group 2—17.53 ± 1.36 MPa, Group 3—22.63 ± 1.61 MPa and Group 4—23.12 ± 1.02 MPa. There was a statistically significant difference (p < 0.05) among the groups. Conclusion The use of dentin desensitizers’ influences bond strength between the tooth and the adhesive. Among the various agents, the single bottle system containing Gluma comfort bond and desensitizer had the best adhesion among the desensitizer groups. How to cite this article Patil S, Naik B, Shetty P. A Comparative Evaluation of Three Commercially Available Dentin Desensitizers on the Shear Bond Strength of Composite Resins: An in vitro Study. J Contemp Dent 2015;5(2):65-68.


2015 ◽  
Vol 63 (4) ◽  
pp. 376-382
Author(s):  
Chaiane Emilia DALAZEN ◽  
Mario Alexandre Coelho SINHORETI ◽  
Margareth COUTINHO

Objective: To evaluate the effects of different surface treatments, in repair bond strength of an aged silorane-based composite. Methods: Specimens were made of a silorane-based composite (P90, 3M/ESPE), aged with thermal-cycling (10,000 cycles; 5-55ºC) and randomly submitted to different surface treatments (each group n = 24): control group (no repair); group 1 (only application of P90 adhesive); group 2 (diamond bur asperization + P90 adhesive); group 3 (aluminum oxide sandblasting + P90 adhesive) and group 4 (asperization + sandblasting + P90 adhesive). Then, the specimens were repaired with the same silorane-based composite and each group randomly subdivided into 2 subgroups: stored in distilled water at 37 °C for 7 days or submitted to thermal-cycling (5,000 cycles). After aging, the tensile test was carried out. The data was submitted to 2-way analysis of variance (2-way ANOVA). Results: The repaired groups aged with oven storage for 7 days did not statistically differ (p>0.05) from the corresponding groups aged with thermal-cycling. The bond strength of the specimens was significantly influenced by the superficial treatment (p<0.01). The highest values of tensile bond strength were found in groups 3 (20.76 ± 4.51 MPa) and 4 (20.67± 3.96 MPa), regardless of aging and repair. Conclusion: The repair of silorane-based composite showed to be stable after aging, and the superficial treatment with aluminum oxide sandblasting was the most effective.


Author(s):  
Elahe Soltanmohamadi Borujeni ◽  
Javad Chalipa ◽  
Ardavan Etemadi ◽  
Maryam Nasiri ◽  
Mohammad Javad Kharrazifard ◽  
...  

Objectives: The aim of the present study was to compare shear bond strength (SBS), adhesive remnant index and enamel cracks in bonding and rebonding of brackets to enamel, conditioned with erbium-doped yttrium aluminium garnet (Er:YAG) laser and conventional acid-etching. Materials and Methods: Fifty-two bovine lower incisors were randomly divided into four groups consisting of group 1 (acid-conditioning in both bondings), group 2 (acid-conditioning in first and laser-conditioning in second bonding), group 3 (laser-conditioning in first- and acid-conditioning in second bonding), and group 4 (laser-conditioning in both bondings). After bracket placement, the samples were thermocycled and tested for SBS in both bonding procedures. Adhesive remnant index scores and enamel cracks were also determined. Tukey's test and one-way analysis of variance was used for statistical analysis (P<0.05). Results: Mean SBS in the first bonding was 23.59MPa in groups 1 and 2, and 6.9MPa in groups 3 and 4. (P<0.001). The acid-etched teeth had a significantly lower SBS in rebonding, regardless of the reconditioning method (P<0.001). The SBS of the teeth conditioned with Er:YAG laser in the first bonding did not show significant changes in rebonding, although mean SBS was higher compared to the first bonding (P=0.675). Bonding most often failed at the enamel-adhesive interface and enamel cracks were observed in a few teeth. Conclusion: The method of primary enamel preparation can affect SBS in rebonding. Based on our results, the mean SBS of Er:YAG-conditioned groups was clinically acceptable in bonding and rebonding, although it was lower compared to the acidetched samples.


2015 ◽  
Vol 39 (4) ◽  
pp. 348-357 ◽  
Author(s):  
RM Agarwal ◽  
R Yeluri ◽  
C Singh ◽  
AK Munshi

Objective: To suggest Papacarie® as a new deproteinizing agent in comparison with indigenously prepared 10% papain gel before and after acid etching that may enhance the quality of the bond between enamel surface and composite resin complex. Study design: One hundred and twenty five extracted human premolars were utilized and divided into five groups: In the group 1, enamel surface was etched and primer was applied. In group 2, treatment with papacarie® for 60 seconds followed by etching and primer application. In group 3, etching followed by treatment with papacarie® for 60 seconds and primer application. In group 4, treatment with 10% papain gel for 60 seconds followed by etching and primer application. In group 5, etching followed by treatment with 10% papain gel for 60 seconds and primer application . After bonding the brackets, the mechanical testing was performed using a Universal testing machine. The failure mode was analyzed using an adhesive remnant index. The etching patterns before and after application of papacarie® and 10% papain gel was also evaluated using SEM. The values obtained for shear bond strength were submitted to analysis of variance and Tukey test (p &lt; 0.05). Results: It was observed that group 2 and group 4 had the highest shear bond strength and was statistically significant from other groups (p=0.001). Regarding Adhesive remnant index no statistical difference was seen between the groups (p=0.538). Conclusion: Papacarie® or 10% papain gel can be used to deproteinize the enamel surface before acid etching to enhance the bond strength of orthodontic brackets.


2018 ◽  
Vol 2018 ◽  
pp. 1-7 ◽  
Author(s):  
Heloísa A. B. Guimarães ◽  
Paula C. Cardoso ◽  
Rafael A. Decurcio ◽  
Lúcio J. E. Monteiro ◽  
Letícia N. de Almeida ◽  
...  

The aim of this study was to evaluate the shear bond strength of resin cement and lithium disilicate ceramic after various surface treatments of the ceramic. Sixty blocks of ceramic (IPS e.max Press, Ivoclar Vivadent) were obtained. After cleaning, they were placed in polyvinyl chloride tubes with acrylic resin. The blocks were divided into six groups (n=10) depending on surface treatment: H/S/A - 10% Hydrofluoric Acid + Silane + Adhesive, H/S -10% Hydrofluoric Acid + Silane, H/S/UA - 10% Hydrofluoric Acid + Silane + Universal Adhesive, H/UA- 10% Hydrofluoric Acid + Universal Adhesive, MBEP/A - Monobond Etch & Prime + Adhesive, and MBEP - Monobond Etch & Prime. The light-cured resin cement (Variolink Esthetic LC, Ivoclar Vivadent) was inserted in a mold placed over the treated area of the ceramics and photocured with an LED for 20 s to produce cylinders (3 mm x 3 mm). The samples were subjected to a shear bond strength test in a universal test machine (Instron 5965) by 0.5 mm/min. ANOVA and Tukey tests showed a statistically significant difference between groups (p<0.05). The results of the shear strength test were H/S/A (9.61±2.50)A, H/S (10.22±3.28)A, H/S/UA (7.39±2.02)ABC, H/UA (4.28±1.32)C, MBEP/A (9.01±1.97)AB, and MBEP (6.18±2.75)BC. The H/S group showed cohesive failures, and the H/UA group was the only one that presented adhesive failures. The conventional treatment with hydrofluoric acid and silane showed the best bond strength. The use of a new ceramic primer associated with adhesive bonding obtained similar results to conventional surface treatment, being a satisfactory alternative to replace the use of hydrofluoric acid.


2017 ◽  
Vol 22 (4) ◽  
pp. 53-60 ◽  
Author(s):  
Nasrin Farhadian ◽  
Loghman Rezaei-Soufi ◽  
Seyed Farzad Jamalian ◽  
Maryam Farhadian ◽  
Shahrzad Tamasoki ◽  
...  

ABSTRACT Introduction: Many patients seeking orthodontic treatment already have incipient enamel lesions and should be placed under preventive treatments. The aim of this in vitro study was to evaluate the effect of CPP-ACP paste and CO2 laser irradiation on demineralized enamel microhardness and shear bond strength of orthodontic brackets. Methods: Eighty caries-free human premolars were subjected to a demineralization challenge using Streptococcus mutans. After demineralization, the samples were randomly divided into five equal experimental groups: Group 1 (control), the brackets were bonded without any surface treatment; Group 2, the enamel surfaces were treated with CPP-ACP paste for 4 minutes before bonding; Group 3, the teeth were irradiated with CO2 laser beams at a wavelength of 10.6 µm for 20 seconds. The samples in Groups 4 and 5 were treated with CO2 laser either before or through CPP-ACP application. SEM photomicrographs of a tooth from each group were taken to observe the enamel surface. The brackets were bonded to the buccal enamel using a conventional method. Shear bond strength of brackets and ARI scores were measured. Vickers microhardness was measured on the non-bonded enamel surface. Data were analyzed with ANOVA and Tukey test at the p< 0.05 level. Results: The mean shear bond strength and microhardness of the laser group were higher than those in the control group and this difference was statistically significant (p< 0.05). All groups showed a higher percentage of ARI score 4. Conclusion: CO2 laser at a wavelength of 10.6 µm significantly increased demineralized enamel microhardness and enhanced bonding to demineralized enamel.


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