Enamel Deproteinization using Papacarie and 10% Papain Gel on Shear Bond Strength of Orthodontic Brackets Before and After Acid Etching

2015 ◽  
Vol 39 (4) ◽  
pp. 348-357 ◽  
Author(s):  
RM Agarwal ◽  
R Yeluri ◽  
C Singh ◽  
AK Munshi

Objective: To suggest Papacarie® as a new deproteinizing agent in comparison with indigenously prepared 10% papain gel before and after acid etching that may enhance the quality of the bond between enamel surface and composite resin complex. Study design: One hundred and twenty five extracted human premolars were utilized and divided into five groups: In the group 1, enamel surface was etched and primer was applied. In group 2, treatment with papacarie® for 60 seconds followed by etching and primer application. In group 3, etching followed by treatment with papacarie® for 60 seconds and primer application. In group 4, treatment with 10% papain gel for 60 seconds followed by etching and primer application. In group 5, etching followed by treatment with 10% papain gel for 60 seconds and primer application . After bonding the brackets, the mechanical testing was performed using a Universal testing machine. The failure mode was analyzed using an adhesive remnant index. The etching patterns before and after application of papacarie® and 10% papain gel was also evaluated using SEM. The values obtained for shear bond strength were submitted to analysis of variance and Tukey test (p < 0.05). Results: It was observed that group 2 and group 4 had the highest shear bond strength and was statistically significant from other groups (p=0.001). Regarding Adhesive remnant index no statistical difference was seen between the groups (p=0.538). Conclusion: Papacarie® or 10% papain gel can be used to deproteinize the enamel surface before acid etching to enhance the bond strength of orthodontic brackets.

Author(s):  
Elahe Soltanmohamadi Borujeni ◽  
Javad Chalipa ◽  
Ardavan Etemadi ◽  
Maryam Nasiri ◽  
Mohammad Javad Kharrazifard ◽  
...  

Objectives: The aim of the present study was to compare shear bond strength (SBS), adhesive remnant index and enamel cracks in bonding and rebonding of brackets to enamel, conditioned with erbium-doped yttrium aluminium garnet (Er:YAG) laser and conventional acid-etching. Materials and Methods: Fifty-two bovine lower incisors were randomly divided into four groups consisting of group 1 (acid-conditioning in both bondings), group 2 (acid-conditioning in first and laser-conditioning in second bonding), group 3 (laser-conditioning in first- and acid-conditioning in second bonding), and group 4 (laser-conditioning in both bondings). After bracket placement, the samples were thermocycled and tested for SBS in both bonding procedures. Adhesive remnant index scores and enamel cracks were also determined. Tukey's test and one-way analysis of variance was used for statistical analysis (P<0.05). Results: Mean SBS in the first bonding was 23.59MPa in groups 1 and 2, and 6.9MPa in groups 3 and 4. (P<0.001). The acid-etched teeth had a significantly lower SBS in rebonding, regardless of the reconditioning method (P<0.001). The SBS of the teeth conditioned with Er:YAG laser in the first bonding did not show significant changes in rebonding, although mean SBS was higher compared to the first bonding (P=0.675). Bonding most often failed at the enamel-adhesive interface and enamel cracks were observed in a few teeth. Conclusion: The method of primary enamel preparation can affect SBS in rebonding. Based on our results, the mean SBS of Er:YAG-conditioned groups was clinically acceptable in bonding and rebonding, although it was lower compared to the acidetched samples.


2007 ◽  
Vol 77 (1) ◽  
pp. 117-124 ◽  
Author(s):  
Güvenç Basaran ◽  
Törün Özer ◽  
Nükhet Berk ◽  
Orhan Hamamcı

Abstract Objective: To test the shear bond strength, surface characteristics, and fracture mode of brackets that are bonded to enamel etched with an erbium, chromium:yttrium-scandium-gallium-garnet (Er,Cr:YSGG) laser operated at different power outputs: 0.5 W, 1 W, and 2 W. Materials and Methods: Human premolars that had been extracted for orthodontic purposes were used. Enamel was etched with an Er,Cr:YSGG laser system operated at one of three power outputs or with orthophosphoric acid. Results: The shear bond strength associated with the 0.5-W laser irradiation was significantly less than the strengths obtained with the other irradiations. Both the 1-W and 2-W laser irradiations were capable of etching enamel in the same manner. This finding was confirmed by scanning electron microscopy examination. The evaluation of adhesive-remnant-index scores demonstrated no statistically significant difference in bond failure site among the groups, except for the 0.5-W laser–etched group. Generally, more adhesive was left on the enamel surface with laser irradiation than with acid etching. Conclusion: The mean shear bond strength and enamel surface etching obtained with an Er,Cr: YSGG laser (operated at 1 W or 2 W for 15 seconds) is comparable to that obtained with acid etching.


2017 ◽  
Vol 22 (4) ◽  
pp. 47-52 ◽  
Author(s):  
Marina Cumerlato ◽  
Eduardo Martinelli de Lima ◽  
Leandro Berni Osorio ◽  
Eduardo Gonçalves Mota ◽  
Luciane Macedo de Menezes ◽  
...  

ABSTRACT Objective: The aim of this in vitro study was to evaluate and compare the effects of grinding, drilling, sandblasting, and ageing prefabricated teeth (PfT) on the shear bond strength (SBS) of orthodontic brackets, as well as the effects of surface treatments on the adhesive remnant index (ARI). Methods: One-hundred-ninety-two PfT were divided into four groups (n = 48): Group 1, no surface treatment was done; Group 2, grinding was performed with a cylindrical diamond bur; Group 3, two drillings were done with a spherical diamond bur; Group 4, sandblasting was performed with 50-µm aluminum oxide. Before the experiment, half of the samples stayed immersed in distilled water at 37oC for 90 days. Brackets were bonded with Transbond XT and shear strength tests were carried out using a universal testing machine. SBS were compared by surface treatment and by ageing with two-way ANOVA, followed by Tukey’s test. ARI scores were compared between surface treatments with Kruskal-Wallis test followed by Dunn’s test. Results: Surface treatments on PfT enhanced SBS of brackets (p< 0.01), result not observed with ageing (p= 0.45). Groups II, III, and IV showed higher SBS and greater ARI than the Group 1 (p< 0.05). SBS was greater in the groups 3 and 4 (drilling, sandblasting) than in the Group 2 (grinding) (p< 0.05). SBS and ARI showed a positive correlation (Spearman’s R2= 0.57; p< 0.05). Conclusion: Surface treatment on PfT enhanced SBS of brackets, however ageing did not show any relevance. Sandblasting and drilling showed greater SBS than grinding. There was a positive correlation between SBS and ARI.


2021 ◽  
Vol 21 (1) ◽  
Author(s):  
Yomna A. Nabawy ◽  
Tarek N. Yousry ◽  
Nadia M. El-Harouni

Abstract Background Increased risk of enamel demineralization during and after orthodontic treatment raises the demand for better preventive measures including combinations of laser, CPP-ACP, and fluoride. The combination of Er,Cr:YSGG laser with CPP-ACP was proved to have a synergetic effect compared to each of them alone. Shear bond strength (SBS) of orthodontic brackets bonded to the enamel surface after being treated with preventive measures is critical. The aim of this study was to compare the SBS and failure mode of metallic brackets bonded to teeth with no pretreatment and pretreated enamel surface, either with Er,Cr:YSGG laser alone or combined with CPP-ACP. Methods Sixty sound extracted human premolar teeth were allocated randomly to 3 groups: In Group 1 (control), teeth were etched and bonded directly; in Group 2, laser pretreatment of the enamel surface was done followed by etching and bonding as in the control group; in Group 3, the enamel surface was lased then CPP-ACP was applied according to the manufacturer instructions, etched and bonded. SBS and Adhesive remnant index (ARI) were evaluated. Results No significant differences were found between the 3 groups neither in the SBS nor in the ARI scores. Conclusions The use of combined Er,Cr:YSGG laser with CPP-ACP as a preventive measure before bonding orthodontic brackets does not endanger the bracket’s bonding strength.


2013 ◽  
Vol 2013 ◽  
pp. 1-6 ◽  
Author(s):  
Maria Francesca Sfondrini ◽  
Danilo Fraticelli ◽  
Paola Gandini ◽  
Andrea Scribante

Purpose. The aim of this study was to assess the effect of water and saliva contamination on the shear bond strength and failure site of orthodontic brackets and lingual buttons.Materials and Methods. 120 bovine permanent mandibular incisors were randomly divided into 6 groups of 20 specimens each. Both orthodontic brackets and disinclusion buttons were tested under three different enamel surface conditions: (a) dry, (b) water contamination, and (c) saliva contamination. Brackets and buttons were bonded to the teeth and subsequently tested using a Instron universal testing machine. Shear bond strength values and adhesive failure rate were recorded. Statistical analysis was performed using ANOVA and Tukey tests (strength values) and Chi squared test (ARI Scores).Results. Noncontaminated enamel surfaces showed the highest bond strengths for both brackets and buttons. Under water and saliva contamination orthodontic brackets groups showed significantly lower shear strengths than disinclusion buttons groups. Significant differences in debond locations were found among the groups under the various enamel surface conditions.Conclusions. Water and saliva contamination of enamel during the bonding procedure lowers bond strength values, more with orthodontic brackets than with disinclusion buttons.


2017 ◽  
Vol 41 (4) ◽  
pp. 280-283 ◽  
Author(s):  
Pallavi Hasija ◽  
Vinod Sachdev ◽  
Shivani Mathur ◽  
Rishi Rath

Objective: The aim of this study was to compare the effect of different deproteinizing agents on shear bond strength of composite to primary teeth enamel. Study Design: Forty sound primary molars divided in 4 groups of 10 teeth each. In control group 1, enamel was etched for 60 seconds with 37% phosphoric acid and rinsed with water. Group 2: after acid etching deproteinizing agent 5 % sodium hypochlorite was applied for 60 seconds and rinsed. Group 3: after acid etching deproteinizing agent papain gel was applied for 60 seconds and rinsed. Group 4: after acid etching deproteinizing agent bromelain gel applied for 60 seconds and rinsed. Following this, bonding agent was applied to treated enamel surface and composite resin disc were build. Samples were then tested for shear bond strength using Universal Testing Machine. Results: Mean SBS was highest for group 4 and lowest for group 1. No statistically significant difference (p value &gt;0.05) was found between all the four groups. Conclusion: Among deproteinizing agents, deproteinization when carried out with bromelain gel and sodium hypochlorite showed effective bond strength as compared to papain.


2009 ◽  
Vol 56 (3) ◽  
pp. 117-122 ◽  
Author(s):  
Vladimir Mitic

Introduction. A great number of techniques have been used for bonding orthodontic brackets to the tooth surfaces. Glass ionomer cements are frequently used material for this purpose. The aim of this study was to measure the shear bond strength of orthodontic brackets bonded with glass ionomer cement Ortho Fuji LC and remained adhesive on the enamel surface after brackets debonding. Material and methods. A total of 40 extracted premolars for orthodontic reasons in different gender patients, 10-16 years old, were randomly divided into four groups. Using glass ionomer cement Ortho Fuji LC (Tokyo, Japan) stainless steel brackets were bonded to the teeth with the average surface area of the bracket base of 14.7 mm2. The shear bond strengths were measured at a crosshead speed of 1 mm per minute, and the load applied at the time of fracture was recorded using electronic dynamometer. Remained adhesive on the enamel after bracket debonding was evaluated using the adhesive remnant index (ARI). Results. Shear bond strength had the highest value for the group where enamel was etched right before bonding bracket (9.14 MPa), than in the group 2 (7.43 MPa), while in the groups 1 (6.72 MPa) and 3 (6.22 MPa), where etching was not performed, bond strength was lower. Conclusion. Shear bond strength of orthodontic brackets bonded with glass ionomer cement Ortho Fuji LC had higher values when the enamel was etched than without etching.


2017 ◽  
Vol 22 (1) ◽  
pp. 82-88 ◽  
Author(s):  
Jéssika Lagni Tonus ◽  
Fernanda Borguetti Manfroi ◽  
Gilberto Antonio Borges ◽  
Eduardo Correa Grigolo ◽  
Sérgio Helegda ◽  
...  

ABSTRACT Introduction: Material biodegradation that occurs in the mouth may interfere in the bonding strength between the bracket and the enamel, causing lower bond strength values in vivo, in comparison with in vitro studies. Objective: To develop a prototype to measure bracket debonding force in vivo and to evaluate, in vitro, the bond strength obtained with the prototype. Methods: A original plier (3M Unitek) was modified by adding one strain gauge directly connected to its claw. An electronic circuit performed the reading of the strain gauge, and the software installed in a computer recorded the values of the bracket debonding force, in kgf. Orthodontic brackets were bonded to the facial surface of 30 bovine incisors with adhesive materials. In Group 1 (n = 15), debonding was carried out with the prototype, while tensile bond strength testing was performed in Group 2 (n = 15). A universal testing machine was used for the second group. The adhesive remnant index (ARI) was recorded. Results: According to Student’s t test (α = 0.05), Group 1 (2.96 MPa) and Group 2 (3.08 MPa) were not significantly different. ARI score of 3 was predominant in the two groups. Conclusion: The prototype proved to be reliable for obtaining in vivo bond strength values for orthodontic brackets.


2013 ◽  
Vol 2013 ◽  
pp. 1-6 ◽  
Author(s):  
Andrea Scribante ◽  
Maria Francesca Sfondrini ◽  
Danilo Fraticelli ◽  
Paola Daina ◽  
Alessandra Tamagnone ◽  
...  

Objective. The aim of this study was to compare the shear bond strength (SBS) and adhesive remnant index (ARI) scores of no-primer adhesives tested with two different bracket bases.Materials and Methods. 120 bovine permanent mandibular incisors were divided into 6 groups of 20 specimens. Two brackets (ODP) with different bracket bases (anchor pylons and 80-gauge mesh) were bonded to the teeth using a conventional adhesive (Transbond XT) and two different no-primer adhesive (Ortho Cem; Heliosit) systems. Groups were tested using an instron universal testing machine. SBS values were recorded. ARI scores were measured. SEM microphotographs were taken to evaluate the pattern of bracket bases. Statistical analysis was performed. ANOVA and Tukey tests were carried out for SBS values, whereas a chi-squared test was applied for ARI scores.Results. Highest bond strength values were reported with Transbond XT (with both pad designs), Ortho Cem bonded on anchor pylons and Heliosit on 80-gauge mesh. A higher frequency of ARI score of “3” was reported for Transbond XT groups. Other groups showed a higher frequency of ARI score “2” and “1.”Conclusion. Transbond XT showed the highest shear bond strength values with both pad designs.


2020 ◽  
Author(s):  
Purna Prasad Khanal ◽  
Basanta Kumar Shrestha ◽  
Rajiv Yadav ◽  
Sanjay Prasad Gupta

Abstract Background: Recycling the old or debonded bracket is one possible alternative to the replacement with new bracket. The aim of this study was to evaluate and compare the effect of different methods of recycling stainless steel orthodontic brackets on shear bond strength.Methods: One hundred twenty human premolars extracted for orthodontic purpose were randomly divided into four groups. Standard MBT (0.022”) brackets, (Leone co., Sesto, Florentine, Florence, Italy) were bonded on buccal surface of all samples with light cured adhesive primer Orthosol (Enlight, Ormco corp., USA) using LED curing unit for 10 seconds. Group I was assigned as control and the brackets of Group II, Group III and Group IV were subjected to recycling by flaming (Gas microtorch: RS Pro, Nozzle, MT 790) ,flaming with sandblasting (Bio-Art sandblaster; Rua Teotônio Vilela, Brazil) and flaming with ultrasonic cleaning (Ultrasonic cleaning unit ,Confident dental equipments Ltd, India) respectively. The recycled brackets were rebonded and final debonding of all brackets was done with universal testing machine (AG-IC/100 KN, Shimadzu, Japan) at a crosshead speed of 0.5mm/min and shear bond strength (MPa) was determined. The adhesive remnant index was evaluated by stereomicroscope at 10X magnification (Olympus corp., Japan). Results: The highest shear bond strength was obtained with Group I (10.35 ± 0.46 MPa), followed by Group III (9.36 ± 0.55 MPa), Group IV (5.97 ± 0.66 MPa) and the least value was obtained with Group II (4.30 ± 0.55 Mpa). Significant differences among the groups were detected by analysis of variance. Tukey post hoc multiple comparison test showed that the shear bond strength of each group was significantly different from one another (p < 0.001). The Chi-square showed statistically significant differences in the adhesive remnant index of the 4 groups (p < 0.001). Conclusions: Shear bond strength of new brackets was significantly higher than that of the recycled brackets. Among recycled brackets, flaming with sandblasting provided adequate shear bond strength, flaming with ultrasonic cleaning provided borderline value for clinical use while flaming alone led to significantly lower value.


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