scholarly journals Organic waste removal from pharmaceutical and textile effluents using composite adsorbent

2020 ◽  
Vol 55 (3) ◽  
pp. 197-206
Author(s):  
M Khatun ◽  
G Mohammad ◽  
Mir T Rahman ◽  
SE Kabir
Keyword(s):  
Waste Water ◽  
High Performance ◽  
Organic Waste ◽  
Water Systems ◽  
High Concentration ◽  
Total Peak Area ◽  
Composite Adsorbent ◽  
Similar Chemical ◽  
Uv Visible ◽  
Textile Industries

Pharmaceutical and textile industries widely use inorganic and organic components which undergo different chemical and biochemical reactions with the ground water systems. The removal of organic wastes from effluents was carried out using a composite adsorbent. Four different samples were collected from the Gonoshasthaya Antibiotic Limted, Gonoshasthaya Pharmaceuticals Limited, Pakiza Dyeing and Printing Industries Limited and Bangladesh Dyeing and Finishing Industries Limited. Synthetic effluents of four types were prepared maintaining a similar chemical average of the collected samples. All the samples contained a high concentration of TDS, TSS, TS, COD and BOD5. The composite adsorbent performed excellently for all the samples. The concentrations of the components contained in the waste water were analyzed by UV-Visible spectrophotometer and High Performance Liquid Chromatography (HPLC). After the treatment, the decreasing trend of the absorbance and total peak area indicated that the significant amount of effluent materials were removed. Bangladesh J. Sci. Ind. Res.55(3), 197-206, 2020

Review of Treatment Methods for Fracturing Flowback Fluid

2014 ◽  
Vol 881-883 ◽  
pp. 659-662
Author(s):  
Fu Bao Li ◽  
Jun Jie Yang ◽  
Qin Li ◽  
Hao Wu
Keyword(s):  
Waste Water ◽  
Wastewater Treatment ◽  
Reaction Kinetics ◽  
Organic Waste ◽  
Reaction Rate ◽  
High Concentration ◽  
Fracturing Fluid ◽  
Treatment Methods ◽  
Organic Wastewater ◽  
At Home

Through analyzing and comparing the treatment of fracturing fluid flowback at home and abroad, it can be found that fluid derived organic waste water can be handled by micro electrolysis economically and efficiently. But there are also some shortages of traditional micro electrolysis. So this paper discusses a new micro-electrolysis technology, namely cavitation-impinging stream electrolysis technology which has several advantages in high concentration organic wastewater treatment. The technology can not only solve the problems that the passivation of process and the plugged equipment in the treatment of fracturing fluid flowback fluid by traditional micro electrolysis, but also can better promote the reaction from the reaction kinetics with the help of Coupling application about cavitation and impinging stream technology, so as to realize the purpose of improving the reaction rate and efficiency.

scholarly journals Determination of Catechin and Epicatechin Content in Chocolates by High-Performance Liquid Chromatography

2014 ◽  
Vol 2014 ◽  
pp. 1-5 ◽  
Author(s):  
Raju V. S. S. Gottumukkala ◽  
Nareshraju Nadimpalli ◽  
Kannababu Sukala ◽  
Gottumukkala V. Subbaraju
Keyword(s):  
High Performance ◽  
Gradient Elution ◽  
High Performance Liquid Chromatographic ◽  
Reversed Phase ◽  
Hplc Method ◽  
High Concentration ◽  
Uv Visible ◽  
Liquid Chromatographic ◽  
Interday Precision

A simple and sensitive reversed phase high-performance liquid chromatographic (HPLC) method has been developed for the determination of catechin and epicatechin in cocoa powder and chocolates. The separation was achieved on a reversed phase C 18 column (TARGA) 5 μm by gradient elution with a flow rate of 1.0 mL/minute with an operating temperature of 30°C and detection with a UV-Visible detector was at 280 nm. The method was validated for linearity, precision, intra- and interday precision, and accuracy. The developed method is successfully applied for the determination of catechin and epicatechin content in chocolates. The Godiva brand chocolate contains high concentration of epicatechin.

Quantitation of Δ8-THC, Δ9-THC, Cannabidiol and 10 Other Cannabinoids and Metabolites in Oral Fluid by HPLC–MS-MS

2020 ◽  
Author(s):  
Lin Lin ◽  
Piyadarsha Amaratunga ◽  
Jerome Reed ◽  
Pornkamol Huang ◽  
Bridget Lorenz Lemberg ◽  
...  
Keyword(s):  
Human Subject ◽  
High Performance ◽  
Oral Fluid ◽  
Solid Phase ◽  
Forensic Toxicology ◽  
High Concentration ◽  
Driving Impairment ◽  
Three Samples ◽  
Cannabidiolic Acid ◽  
Liquid Chromatography Tandem Mass

Abstract Quantitative analysis of Δ9-tetrahydrocannabinol (Δ9-THC) in oral fluid has gained increasing interest in clinical and forensic toxicology laboratories. New medicinal and/or recreational cannabinoid products require laboratories to distinguish different patterns of cannabinoid use. This study validated a high-performance liquid chromatography-tandem mass spectrometry method for 13 different cannabinoids, including (-)-trans-Δ8-tetrahydrocannabinol (Δ8-THC), (-)-trans-Δ9-tetrahydrocannabinol (Δ9-THC), cannabidiol (CBD), Δ9-tetrahydrocannabinolic acid-A (Δ9-THCA-A), cannabidiolic acid (CBDA), 11-hydroxy-Δ9-tetrahydrocannabinol (11-OH-Δ9-THC), 11-nor-9-carboxy-Δ9-tetrahydrocannabinol (Δ9-THCCOOH), tetrahydrocannabivarin (THCV), cannabidivarin (CBDV), cannabidiorcol (CBD-C1), cannabichromene (CBC), cannabinol (CBN) and cannabigerol (CBG), in oral fluid. Baseline separation was achieved in the entire quantitation range between Δ9-THC and its isomer Δ8-THC. The quantitation range of Δ9-THC, Δ8-THC and CBD was from 0.1 to 800 ng/mL. Two hundred human subject oral fluid samples were analyzed with this method after solid phase extraction. Among the 200 human subject oral fluid samples, all 13 cannabinoid analytes were confirmed in at least one sample. Δ8-THC was confirmed in 11 samples, with or without the presence of Δ9-THC. A high concentration of 11-OH-Δ9-THC or Δ9-THCCOOH (>400 ng/mL) was confirmed in three samples. CBD, Δ9-THCA-A, THCV, CBN and CBG were confirmed in 74, 39, 44, 107 and 112 of the 179 confirmed Δ9-THC-positive samples, respectively. The quantitation of multiple cannabinoids and metabolites in oral fluid simultaneously provides valuable information for revealing cannabinoid consumption and interpreting cannabinoid-induced driving impairment.

scholarly journals Concentration of Bioactive Phenolic Compounds in Olive Mill Wastewater by Direct Contact Membrane Distillation

Molecules ◽  
2021 ◽  
Vol 26 (6) ◽  
pp. 1808
Author(s):  
Rosa Tundis ◽  
Carmela Conidi ◽  
Monica R. Loizzo ◽  
Vincenzo Sicari ◽  
Rosa Romeo ◽  
...  
Keyword(s):  
Direct Contact ◽  
High Performance ◽  
Biological Properties ◽  
Membrane Distillation ◽  
Olive Mill Wastewater ◽  
High Concentration ◽  
Direct Contact Membrane Distillation ◽  
Reducing Activity ◽  
Β Carotene ◽  
Olive Mill

Olive mill wastewater (OMW), generated as a by-product of olive oil production, is considered one of the most polluting effluents produced by the agro-food industry, due to its high concentration of organic matter and nutrients. However, OMW is rich in several polyphenols, representing compounds with remarkable biological properties. This study aimed to analyze the chemical profile as well as the antioxidant and anti-obesity properties of concentrated fractions obtained from microfiltered OMW treated by direct contact membrane distillation (DCMD). Ultra-high performance liquid chromatography (UHPLC) analyses were applied to quantify some phenols selected as phytochemical markers. Moreover, α-Amylase, α-glucosidase, and lipase inhibitory activity were investigated together with the antioxidant activity by means of assays, namely β-carotene bleaching, 2,2′-azino-bis(3-ethylbenzothiazoline-6-sulphonic) acid (ABTS) diammonium salts, 2,2-diphenyl-1-picrylhydrazyl (DPPH) assay, and Ferric Reducing Activity Power (FRAP) tests. MD retentate—which has content of about five times greater of hydroxytyrosol and verbascoside and about 7 times greater of oleuropein than the feed—was more active as an antioxidant in all applied assays. Of interest is the result obtained in the DPPH test (an inhibitory concentration 50% (IC50) of 9.8 μg/mL in comparison to the feed (IC50 of 97.2 μg/mL)) and in the ABTS assay (an IC50 of 0.4 μg/mL in comparison to the feed (IC50 of 1.2 μg/mL)).

scholarly journals Elucidation of the Crystal Growth Characteristics of SnO2 Nanoaggregates Formed by Sequential Low-Temperature Sol-Gel Reaction and Freeze Drying

Nanomaterials ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1738
Author(s):  
Saeid Vafaei ◽  
Alexander Wolosz ◽  
Catlin Ethridge ◽  
Udo Schnupf ◽  
Nagisa Hattori ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Low Temperature ◽  
Photoelectron Spectroscopy ◽  
High Performance ◽  
Freeze Drying ◽  
Sno2 Nanoparticles ◽  
Sol Gel ◽  
Functional Materials ◽  
Cost Effective ◽  
High Concentration

SnO2 nanoparticles are regarded as attractive, functional materials because of their versatile applications. SnO2 nanoaggregates with single-nanometer-scale lumpy surfaces provide opportunities to enhance hetero-material interfacial areas, leading to the performance improvement of materials and devices. For the first time, we demonstrate that SnO2 nanoaggregates with oxygen vacancies can be produced by a simple, low-temperature sol-gel approach combined with freeze-drying. We characterize the initiation of the low-temperature crystal growth of the obtained SnO2 nanoaggregates using high-resolution transmission electron microscopy (HRTEM). The results indicate that Sn (II) hydroxide precursors are converted into submicrometer-scale nanoaggregates consisting of uniform SnO2 spherical nanocrystals (2~5 nm in size). As the sol-gel reaction time increases, further crystallization is observed through the neighboring particles in a confined part of the aggregates, while the specific surface areas of the SnO2 samples increase concomitantly. In addition, X-ray photoelectron spectroscopy (XPS) measurements suggest that Sn (II) ions exist in the SnO2 samples when the reactions are stopped after a short time or when a relatively high concentration of Sn (II) is involved in the corresponding sol-gel reactions. Understanding this low-temperature growth of 3D SnO2 will provide new avenues for developing and producing high-performance, photofunctional nanomaterials via a cost-effective and scalable method.

High performance UV–visible avalanche photodetector based on single α-MoO3 microbelt/p-Si heterostructure

2021 ◽  
Vol 44 (3) ◽  
Author(s):  
Yi Tian ◽  
Naisen Yu ◽  
Shiyu Du ◽  
Dedi Liu ◽  
Yunfeng Wu
Keyword(s):  
High Performance ◽  
Uv Visible
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