scholarly journals Recovery and Characterization Studies of Post-Production Alloy Waste from the Automotive Industry

Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5600
Author(s):  
Sylwester Żelazny ◽  
Witold Żukowski ◽  
Dariusz Bogdał ◽  
Szczepan Bednarz ◽  
Wiktor Kasprzyk ◽  
...  

Superalloys provide high corrosion resistance and are widely used as high-performance materials in aerospace, automotive, chemical, and other industries. Herein, the investigation into the characteristics and properties of alloy waste; Inconel 625, Inconel 718, and Titanium Grade 5, from the automotive industry, was introduced as a result of a recovery in various processes. For this reason, the following procedures were carried as follows; the washing process to remove oil from the swarf was evaluated using several commercial agents and for the process of thermal disposal of processing fluids, a temperature of 900 °C was used in a muffle furnace without air access. The presented studies show that the commercially available series of washing agents did not modify the composition of the surface. However, the high temperatures during the calcination of oil residues are affecting the elemental composition of the alloys. According to the results of the analyses, it is not possible to remove 100% of the oil residues from alloy waste using washing agents based on light organic fractions; however, the effectiveness of this method reaches 99%. In this report, accurate SEM-EDS analyses show changes that occur on the surface after machining and removal of processing fluids. The NMR and GC/MS investigations indicate contaminants as a mixture of aliphatic and cycloaliphatic hydrocarbons with carbon numbers from C8–C30.

1996 ◽  
Vol 6 (3) ◽  
pp. 137 ◽  
Author(s):  
RR Blank ◽  
FL Allen ◽  
JA Young

We evaluated the influence of temperature and heating time on water-soluble anions and cations of soil-litters of low sagebrush (Artemisia arbuscula ssp. longicaulis), squirreltail (Elymus elymoides), cheatgrass (Bromus tectorum), and medusahead (Taeniatherum caputmeduase ssp. asperum). Soil-litters were collected from volcanic tablelands north of Honey Lake, California. These high clay, montmorillonitic, soils have rarely experienced wildfires. Soil-litter samples, in a 50 mt crucible, were placed in a preheated muffle furnace using a time-temperature matrix of 150, 250, 350, and 450°C at 1, 5,and 15 min. High performance ion-exchange chromatography was used to quantify water-soluble cations and anions. For most measured solutes, there was either a significant (P less than or equal to 0.05) burn time × temperature or a significant burn time × temperature × soil-litter type interaction. As compared to pre-burn values, heating of soil generally increased the concentration of the water-soluble solutes measured; nitrate was the exception. Maximum solute values were generally obtained at a temperature of 350°C at 5 and 15 min heating time. A temperature of 450°C at 15 min heating time resulted in the significant reduction of solute concentration below the maximum values. Nitrate was significantly higher in squirreltail soil-litter than the other soil-litters when the burn time was 1 min. Heating, in general, fostered an increase in water-soluble ammonium. For most solutes, heat-induced increases were greatest for the low sagebrush soil-litter.


2020 ◽  
Vol 142 (9) ◽  
Author(s):  
I. Valiente-Blanco ◽  
J. L. Perez-Diaz ◽  
J. L. Perez-del-Alamo ◽  
E. Diez-Jimenez

Abstract Linear bushings are a compact and reliable solution for mechanisms requiring relative linear displacement between moving parts. In this paper, we report the dependence of the coefficient of friction (COF) of polytetrafluoroethylene (PTFE) grease-lubricated bushings against a Ti6Al4 V (grade 5) alloy shaft at high temperatures up to 200 °C, for a motion speed of up to 0.47 m/s and a load pressure of 0.8 MPa. A proportional sensitivity of the COF with temperature is observed due to the change in the viscosity of the grease lubricant. Results of survival tests are also reported demonstrating a total sliding distance of 3200 m without maintenance and a total a total sliding distance of 10,200 m without critical failure.


Materials ◽  
2019 ◽  
Vol 12 (3) ◽  
pp. 544 ◽  
Author(s):  
Maider Muro ◽  
Josu Leunda ◽  
Garikoitz Artola ◽  
Carlos Soriano

The aim of this work is to evaluate the microstructural evolutions developed by mixing a corrosion-resistant and high-performance material with a high-hardness material in a coating obtained by laser-cladding technology. In this paper, five different mixtures of Inconel 625 alloy and AISI H13 steel powders have been deposited on a plate of 42CrMo4 steel using a 2.2 kW diode pumped Nd:YAG laser. The effect of adding tool steel to a Ni-based superalloy has been analyzed by the characterization of each cladded sample using optical microscopy and scanning electron microscopy (SEM). The precipitates observed in the samples have been analyzed by energy dispersive X-ray spectroscopy (EDS X-ray). SEM micrographs and EDS analysis indicate the existence of Laves phase. It has been observed that the presence of these precipitates is stabilized in a certain range of AISI H13 addition.


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